DUCTILITY PERFORMANCE OF HIGH STRENGTH LIGHTWEIGHT CONCRETE PRODUCED FROM A MIXTURE OF OIL PALM SHELL AND PALM OIL CLINKER

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CICM 2015 First International Conference on Advances in Civil Infrastructure and Construction Materials MIST, Dhaka, Bangladesh, 14 15 December 2015 DUCTILITY PERFORMANCE OF HIGH STRENGTH LIGHTWEIGHT CONCRETE PRODUCED FROM A MIXTURE OF OIL PALM SHELL AND PALM OIL CLINKER Md. N. HUDA 1, Mohd Z. B.Jumaat 2, A.B.M. Saiful Islam 3 and Mahmudur R. Soeb 4 1, 2, 3, 4 University of Malaya, Kuala Lumpur, Malaysia. Email: 1 nazmulhuda.128@gmail.com, 2 zamin@um.edu.my, 3 abm.saiful@gmail.com and 4 soeb_buet@yahoo.com Abstract. Due to environmental issues, the use of waste materials in concrete is gaining popularity. Waste materials, such as oil palm shell (OPS) and palm oil clinker (POC) from the Malaysian palm oil industry are being used in various researches to produce lightweight concrete. Concrete containing only OPS shows more ductility and less compressive strength, while POC concrete shows less ductility but higher compressive strength. Combination of OPS and POC may exhibit improved compressive strength and ductility behaviour. In this experimental study, normal coarse aggregate is replaced by a mixture of OPS and POC aggregates in the lightweight concrete. The proportion of OPS and POC in the concrete mix varies from 40% to 70%. The results indicate that if a mixture of OPS and POC are used in producing lightweight aggregate concrete, better performance in terms of compressive strength and ductility can be achieved. Furthermore, through the utilization of waste materials, the proposed lightweight concrete helps to mitigate the negative impact on the environment. Keywords: Oil palm shell, Palm oil clinker, Lightweight concrete, Compressive strength, Displacement ductility. 311

Md. N. Huda, Mohd. Zamin B. Jumaat, A.B.M. Saiful Islam and Mahmudur R. Soeb 1 INTRODUCTION Nowadays, lightweight concrete is a popular choice in the construction industries. The use of lightweight concrete (LWC) has many advantages over normal weight concrete, such as a reduction in the size of the structural elements, increase in building height and a greater span-depth ratio for beams in pre-stressed concrete construction [1]. In designing a structural element, the compressive strength is desirable along with acceptable ductility under heavy loading to ensure adequate deflection [2]. Satisfactory ductility is a very important factor for reinforced concrete structures in high seismic areas because less ductile reinforced concrete experiences many serious complications when subjected to compression and torsion. Currently several researchers have worked on lightweight concrete using waste materials, as recycling the solid wastes from the agricultural and manufacturing industries is long overdue [3-5]. Malaysia is the second largest palm oil producing country in the world producing more than half of the world s palm oil [6]. The residue of palm oil industry includes OPS and POC. Several investigations have shown that lightweight concrete with OPS or POC aggregate can be produced with a compressive strength ranging from 17 to 53 MPa [7, 8].LWC is still not a common material in the construction industry and there has been some reticence concerning its use in concrete structures. Even the displacement ductility of lightweight concrete has rarely been studied in the earlier literature. The objective of this study is to produce lightweight concrete from a mixture of OPS and POC aggregates. This lightweight concrete is named as palm shell and clinker concrete (PSCC). This research also investigates the compressive strength, stress-strain curves and ductility behaviour of PSCC. The ductility characteristics have been studied by the displacement ductility index. 2 MATERIALS 2.1 Cement In this study, ordinary Portland cement with a specific gravity of 3.14 g/cm3 and fineness of 3510 cm2/g was used as the binder material in the concrete. This cement was collected from a local Malaysian company named Tasek Corporation Berhad. The compressive strengths of the cement were 34.2 and 45.9 MPa, at 7 and 28 days, respectively. 2.2 Fine Aggregate Local mining sand with specific gravity, fineness modulus, water absorption and maximum grain size of 2.68, 2.65, 1.17% and 4.75 mm, respectively, was selected as the fine aggregate in the concrete mix. 312

2.3 Coarse Aggregate Ductility performance of high strength OPS and POC lightweight concrete Two types of coarse aggregates were used in the concrete mix for this study, which were collected from the local palm oil factory in Malaysia as waste materials. Figure 1 shows the selected coarse aggregates for producing lightweight concrete. The OPS aggregate is shown in Figure 1 (a). After collecting the OPS from the local palm oil industry, it was washed and crushed using a stonecrushing machine in the laboratory. The flakiness of OPS decreases significantly upon crushing, which improves the performance of the coarse aggregate and yields higher compressive strength[9]. Subsequently, crushed OPS aggregate was sieved using a 5 mm-sieve to remove the aggregate less than 5 mm in size. Fig.1. Coarse aggregate (a) OPS aggregate (b) POC aggregate Another type of coarse aggregate, POC aggregate is presented in Fig. 1 (b). This POC was also collected from the local palm oil industry in Malaysia. In a similar fashion to OPS, the clinker was crushed and sieved using a 5 mm-sieve. As the larger size aggregate has a greater value under the abrasion test, POC retained on the 5 mm sieve was considered to be coarse aggregate. 2.4 Superplasticizer (SP) For this experimental program, SikaViscocrete 2199, which was collected from Sika Kimia, Malaysia, was employed as the chloride free Super plasticizer, in accordance with EN 934-2, and mixed in the concrete at 2.0% of cement weight to facilitate the workability. 3 TEST METHODS 3.1 Mix Proportions By and large, the LWAC mix design is determined by trial mixes [10]. Most of the previous studies used 480-550 kg/m 3 cement with a water cement ratio of 0.3-313

Md. N. Huda, Mohd. Zamin B. Jumaat, A.B.M. Saiful Islam and Mahmudur R. Soeb 0.4 to obtain concrete with a compressive strength of 30-44 MPa [11]. In this study, to obtain concrete with a compressive strength of 45 MPa, 450 kg/m 3 cement content with a water cement ratio of 0.35 was selected for the trial mix. Therefore, unlike some previous studies, this study designed the trial mixes with the less cement content to get high strength lightweight concrete (LWC) Four trial mixes were conducted in the laboratory to obtain grade 45 concrete with a moderate workability. Each and every mix had an identical water/cement ratio. To achieve workability, SP was added to all the mixes. Sieved local mining sand fills the place of fine aggregate. To attain the high strength ductile concrete, a mixture of OPS and POC was used as coarse aggregate in different proportions in the four trial mixes. In mix TM-1, the total volume of coarse aggregate was divided into two parts: 70% for the OPS and 30% for the POC. The corresponding quantities of OPS and POC in the TM-2, TM-3 and TM-4 mix were 60% & 40%; 50% & 50%; and 40% & 60%, respectively. The details of the concrete mixes with the proportions of ingredients are shown in Table 1. Mix ID Cement Water Table 1: Concrete mix proportions in kg/m3 W/C ratio SP Sand OPS (% by vol.) POC (% by vol.) Slump (mm) TM - 1 450 158 0.35 2% 1013 248 (70%) 141 (30%) 60 TM - 2 450 158 0.35 2% 1025 212 (60%) 187 (40%) 65 TM - 3 450 158 0.35 2% 1158 148 (50%) 195 (50%) 40 TM - 4 450 158 0.35 2% 1048 142 (40%) 281 0%) 70 3.2 Samples Preparation and Data Collection During preparation of the concrete mixing procedure, cement, sand, OPS and POC were blended into a pan mixer for 5 min. Subsequently, the mixture of SP and about 80% of the water were added into the pan mixture. After 5 minutes of mixing, the remaining 20% of the water was added into the pan mixture and the mixing continued for a further 10 min. The concrete specimens were cast in steel moulds, and the specimens were compacted using the vibration table. The casting of all the specimens followed BS 1881 [12]. The specimens were remoulded after 24 hours and cured in water at 30 ± 2 C until the test days. Three specimens from each category were prepared for obtaining the average value. Initially the slump tests were carried out for the selected mixes. The compressive strengths of the specimens were determined on the 1 st, 3 rd, 7 th and 28 th day. In addition, the modulus of elasticity was measured on the 28 th day. The tests were carried out in accordance with BS 1881: Part 116 [12] using a univer- 314

Ductility performance of high strength OPS and POC lightweight concrete sal compression testing machine of 3000 KN capacity with a rate of loading controller. 4 RESULTS AND DISCUSSION 4.1 Compressive Strength Table 2 shows the 28 days compressive strength development for all the trial mixes. The test results show that if the percentage of OPS increases in the combination of coarse aggregate, the 28 days compressive strength decreases. Again, having a POC content of more than 50% also decreases the compressive strength. With the largest proportion of OPS content, TM-1 exhibits the lowest value for the 28-day compressive strength. TM-3, with a POC content of 50% in the mixture of coarse aggregate, shows the highest value for the 28-day compressive strength. In TM-4, the POC content was increased to 60%, resulting in a 9% fall in the compressive strength from TM-3. This weakening can be attributed to the round and plain surface texture of OPS, which imparts poor bondage to the concrete if its presence is excessive. On the other hand, the POC aggregate, which is rough and porous, imparts strong bonding with the cement paste. Furthermore, if OPS and POC coarse aggregate are mixed in a 50% ratio (TM-3), the 28-days compressive strength increases to 46.5 MPa, which is the maximum among all the mixes. However, POC aggregate is porous in nature, which enables some of the cementing material to enter the pores, that, eventually, decreases the overall bonding strength [13]. Table 2: Development of the compressive strength of PSCC Mix ID Compressive Strength (MPa) 1 day 3 day 7 day 28 day TM-1 18.44 31.39 35.43 38.28 TM-2 29.46 33.7 36.01 38.57 TM-3 28.9 39.95 44.64 46.47 TM-4 30.7 36.23 40.13 42.35 4.2 Stress-Strain Behavior Fig. 2 shows the stress-strain curves of all the tested samples containing different percentages of OPS and POC. Both vertical and lateral strains are plotted against the increase in the compressive load applied. The vertical displacement is shown in the positive X-axis and the lateral displacement in the negative X-axis in Fig. 2. The stress-strain curves of the PSCC samples softens towards a rounded peak in the post-yield stage with a very slow dropping tendency after the post yield, which is mainly because the PSCC concrete has a good interlocking [13] and bi- 315

Md. N. Huda, Mohd. Zamin B. Jumaat, A.B.M. Saiful Islam and Mahmudur R. Soeb linear ductile [14] stress-strain behaviour. The experimental results show that the PSCC concrete specimen can undergo larger deformation before failure, and that such a failure is ductile and gives warning of the impending failure similar to steel. For TM-3 and TM-4, the strains at maximum stress were measured in the range of 0.0028 and 0.0034, respectively showing less value than that for TM-1 and TM-2, which were 0.0035 and 0.004, respectively; this is close to the range for lightweight concrete elements [15], 0.026 0.003. With the increase in the POC aggregate in the concrete, the strain at maximum stress exhibits a lower value, and, vice versa, with an increase in OPS aggregate. It is also observed that concrete with POC aggregate only shows brittle behaviour with the maximum stress value whereas OPS concrete reveals the maximum ductile behaviour with the minimum stress value. After combining the OPS and POC in the concrete, a higher stress value is found with moderate ductile behaviour. 316 Fig.2. Stress-strain curves for vertical and lateral displacement 4.3 Displacement Ductility The mechanical properties (compressive strength and modulus of elasticity) and ductility indices of PSCC obtained from the laboratory results are presented in Table 3. The ductility of any structural element is usually specified as the capacity of the structural element to undergo load still experiencing extra distortion beyond the maximum load stage [2]. This definition is qualitative and to measure the displacement ductility of compression critical elements. The ratio of the area under the stress-strain curve up to 5ε o to the area up to ε o for displacement is defined as the ductility index (μ). The displacement ductility values stated in this study are the strain ductility of the compression-critical member. Here, ε o is the strain at peak stress (σ max ) for the concrete element. The evaluation of the structural parameters of the displacement ductility index is illustrated in Table 3 for the different mix ratios. Existing literature shows that POC concrete exhibits little ductility [13]. After mixing OPS with POC in this study, all the trial mixes show

Ductility performance of high strength OPS and POC lightweight concrete an adequate ductility index. TM-3 shows the maximum ductility among the trial mixes. Table 3: Displacement ductility indices of PSCC for different mixture 5 CONCLUSIONS Elastic Displacement ductility Mix ID modulus (GPa) Stress Strain μ TM - 1 6.8 24.00 0.00408 3.02 TM - 2 6.9 24.57 0.00422 2.87 TM - 3 10.16 28.92 0.00338 3.56 TM - 4 10.38 26.60 0.00324 2.96 The PSCC samples show ductile behaviour. The ductility index decreases with the increase of porous POC aggregate content in the concrete mixes. The strains at maximum stress of the PSCC samples are in good agreement with the recent study of lightweight aggregate concrete. PSCC can be produced with a 28-day compressive strength of 46 MPa, which is higher than the structural requirement of 15MPa. In this study, the use of 50% OPS and 50% POC coarse aggregate seems to give the optimum mix, which produces grade 45 concrete with adequate ductility. It requires 450 kg/m3 cement to produce grade 45 concrete, which is the lowest among the recent studies. ACKNOWLEDGEMENTS The authors gratefully acknowledge the support given by University of Malaya (UM) for funding the study through the University of Malaya Research Grant (UMRG)RP018-2012A. REFERENCES [1] M. J. Shannag, "High strength concrete containing natural pozzolan and silica fume," Cement and Concrete Composites, vol. 22, pp. 399-406, 12// 2000. [2] S. H. Ahmad, Y. Xie, and T. Yu, "Shear ductility of reinforced lightweight concrete beams of normal strength and high strength concrete," Cement and Concrete Composites, vol. 17, pp. 147-159, // 1995. 317

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