Araldite MY pbw Hardener HY pbw

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Vantico Ltd Electronic Polymers Heavy Electrical Araldite Impregnating Resin System Araldite MY 750 100 pbw Liquid, impregnating resin system with low glass transition temperature for coils with excellent mechanical end-properties. Large coils for magnets and/or rotating machines Super-conductive magnets Applications Vacuum Impregnation Processing methods High thermal shock resistance Properties Slg Edition: July 2000 Replaces Edition: June 1999

Product data Araldite MY 750 Liquid, unmodified, solvent-free Bisphenol A epoxy resin Viscosity at 25 C ISO 12058-1 mpa s Epoxy content ISO 3001 equiv/kg Density at 25 C ISO 1675 g/cm³ Flash point DIN 51758 C Vapour pressure at 20 C (Knudsen) Pa at 50 C (Knudsen) Pa 12000-16000 5.20-5.40 1.15-1.20 > 200 < 1.10-2 5.10-3 Hardener HY 5922 Liquid, aliphatic polyamine hardener Viscosity at 20 C ISO 9371 mpa s Density at 20 C ISO 1675 g/cm³ Flash point DIN 51758 C Vapour pressure at 20 C (Knudsen) Pa at 50 C (Knudsen) Pa < 10 0.95-1.00 160-170 < 0.1 c. 1 Remark The hardener HY 5922 is a corrosive product. Storage Store the components at 18-25 C, in tightly sealed and dry original containers. Under these conditions, the shelf life will correspond to the expiry date stated on the label. Product specific advise regarding storage can be found on product label. After this date, the product may be processed only following reanalysis. Partly emptied containers should be closed tightly immediately after use. For information on waste disposal and hazardous products of decomposition in the event of fire, refer to the Material Safety Data Sheets (MSDS) for these particular products 2 Vantico Ltd. July 2000 Araldite MY 750/ HY5922

Processing properties System: Araldite MY 750 100 pbw 50 [Pa s] 40 30 40 C Processing Viscosity 20 30 C 10 0 [min] 0 50 100 150 200 250 300 350 400 450 500 Fig.3.1: Viscosity increase at 30 and 40 C in function of the time (measurements with Rheomat 115A, MS DIN 125, D =10 s -1 ) Viscosity increase at 30 C 40 C (time until 1500 mpa s) 4h 30 min 3h 25 min 1000 [mpa s] 100 10 20 30 40 [ C] 50 Fig.3.2: Viscosity increase at 30 and 40 C in function of the time (measurements with Rheomat 115A, MS DIN 125, D =10 s -1 ) 1000 [min] Fig.3.3: Initial viscosity in function of temperature (measurements with Rheomat 115A, MS DIN 125, D =10 s -1 ) Gelation-/Cure Times 100 20 30 40 50 60 [ C] 70 Fig.3.4: Geltime in function of temperature (measured with Gelnorm Instrument, ISO 9396) Vantico Ltd. July 2000 Araldite MY 750/ HY 5922 3

Mechanical and Physical properties System: Araldite MY 750 100 pbw Determined on standard test specimen at 23 C Curing Cycle: 6h at 40 C + 3h at 80 C Flexural strength ISO 178 MPa Surface strain ISO 178 % E modulus from flexural strength ISO 178 MPa Tensile strength ISO R 527 MPa Elongation at break ISO R 527 % E modulus from tensile strength ISO R 527 MPa Impact strength ISO 179 kj/m² Glass transition temperature (DSC) IEC 1006 C Heat Distortion Temperature ISO 75 C Bend Notch Critical Stress Intensity Factor K IC ISO/ DIN 1358 MPa.m 1/2 Specific Energy at break G IC IEC 1006 C Water absorption (specimen: 50x50x4 mm) ISO 62 4 days at 23 C % 10 days at 23 C % Storage under tropical conditions CG 75 % after 10 days at 40 C / 92% rel. humidity 95-105 3.5-4.5 2700-3100 55-65 6-9 2800-3200 60-70 40-45 40-45 4.2-4.4 5100-5500 0.35-0.45 0.55-0.65 1.1-1.4 4 Vantico Ltd. July 2000 Araldite MY 750/ HY 5922

Electrical properties System: Araldite MY 750 100 pbw Determined on standard test specimen at 23 C Curing Cycle: 6h at 40 C + 3h at 80 C Breakdown strength IEC 60243-1 kv/mm Loss factor IEC 250/ DIN 53483 tan δ > 1% % tan δ > 5% % Dielectric constant IEC 250/ DIN 53483 ε r at 25 C 25-30 35-40 40-45 3.7 Volume resistivity IEC 93/ DIN 53482 at 25 C ohm.cm 7.70E + 15 14 12 tg δ [%] 10 8 6 ε 4 r 2 0 0 50 100 150 1.0E+16 [Ω cm] 1.0E+14 1.0E+12 1.0E+10 1.0E+08 1.0E+06 0 50 100 150 200 [ C] 250 Fig.6.1: Loss factor (tan δ) and dielectric constant (εr) in function of temperature (measurement frequency: 50 Hz) (IEC 250/ DIN 53483) Fig.6.2: Volume resistivity (ρ) in function of temperature (measurement voltage: 1000 V) (IEC 93/ DIN 53482) Vantico Ltd. July 2000 Araldite MY 750/ HY 5922 5

Industrial hygiene Mandatory and recommended industrial hygiene procedures should be followed whenever our products are being handled and processed. For additional information please consult the corresponding Safety Data Sheets and the brochure "Hygienic precautions for handling plastics products of Ciba Specialty Chemicals " (Publ. No. 24264/e). Handling precautions Safety precautions at workplace: protective clothing gloves arm protectors goggels/safety glasses respirator/dust mask Skin protection before starting work after washing Cleansing of contaminated skin Clean shop requirements Disposal of spillage Ventilation: of workshop of workplace yes essential recommended when skin contact likely yes recommended Apply barrier cream to exposed skin Apply barrier or nourishing cream Dab off with absorbent paper, wash with warm water and alkali-free soap, then dry with disposable towels. Do not use solvents Cover workbenches, etc. with light coloured paper Use disposable breakers, etc. Soak up with sawdust or cotton waste and deposit in plastic-lined bin Renew air 3 to 5 times an hour Exhaust fans. Operatives should avoid inhaling vapours. First Aid Contamination of the eyes by resin, hardener or casting mix should be treated immediately by flushing with clean, running water for 10 to 15 minutes. A doctor should then be consulted. Material smeared or splashed on the skin should be dabbed off, and the contaminated area then washed and treated with a cleansing cream (see above). A doctor should be consulted in the event of severe irritation or burns. Contaminated clothing should be changed immediately. Anyone taken ill after inhaling vapours should be moved out of doors immediately. In all cases of doubt call for medical assistance. Vantico Ltd. Electronic Polymers Registered trademark APPROVED TO ISO 9000 ff All recommendations for use of our products, whether given by us in writing, verbally, or to be implied from results of tests carried out by us are based on the current state of our knowledge. Notwithstanding any such recommendations the Buyer shall remain responsible for satisfying himself that the products as supplied by us are suitable for his intended process or purpose. Since we cannot control the application, use or processing of the products, we cannot accept responsibility therefore. The Buyer shall ensure that the intended use of the products will not infringe any third party's intellectual property rights. We warrant that our products are free from defects in accordance with and subject to our general conditions of supply. 25 July, 2000