Melting and casting technologies for the production of tool steels Dr. Harald Holzgruber, CEO DI Alexander Scheriau, CSO

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Tool 2016, Bratislava, October 5 th 2016 Melting and casting technologies for the production of tool steels Dr. Harald Holzgruber, CEO DI Alexander Scheriau, CSO

Global Alloy Tool Steel Products 2015 [ 000 metric tonnes] TOTAL Total World: 1,930 NAFTA: 250 Other America: 60 Europe: 600 Asia: 900 Others: 120 Total ATS Total HSS Total World: 1,780 Total World: 150 TOTAL BARS Other Products TOTAL 1,320 TOTAL 460 Forged Bars* 690 Flat Products 300 Hot Rolled Bars 210 Others 160 Cold Finished Bars 420 *incl. die blocks Picture credits: Böhler Edelstahl GmbH & Co KG Picture credits: Böhler Bleche GmbH & Co KG Picture credits: Deutsche Edelstahlwerke Data provided by

Alloy Tool Steel Structure 2015 Europe Rest of the World PM 42% HSS 7% PM 38% HSS 9% CW 24% HW 27% CW 26% HW 27% Data provided by Tool steel grades: Hot work steel (HW) Cold work steel (CW) Plastic mould steel (PM) High speed steel (HSS)

[ 000 tonnes] TOP 20 tool steel producers 275 250 225 200 175 150 125 100 75 50 25 - High Speed Steel Alloy Tool Steel * excluding trade volumes (externally sourced) Data provided by

Properties and influence factors Chemistry Heat/surface treatment Forging Hardness Red hardness Wear resistance Polishability Low levels of inclusion Cleanliness Hot toughness Retention of hardness Hot strength Thermal shock resistance Thermal conductivity Melting Refining Remelting Casting

Typical process route for tool steels

Typical process route for tool steels

EAF Electric Arc Furnace

EAF Main tasks and trend Primary melting unit in alloy steel making process Melting of various kinds of scraps and ferro-alloys Dephosphorisation and decarburisation using oxygen and lime Trend towards Improved productivity Decreased energy consumption Increased flexibility

EAF Melting optimisation The EAF Melting Process requires the combination of 2 main energy sources: CHEMICAL ENERGY (burners, oxygen lances, carbon injectors) ELECTRICAL ENERGY (electric arc) PROCESS TOOLS AUTOMATION TOOLS The optimum control of the two power input together with all the activities needed for process and turnaround is the KEY for EAF process optimization

EAF Melting optimisation Case study of 55t EAF for Tool Steels: Upgrade of existing EAF to decrease energy consumption and tap-to-tap-time Installation of SwingDoor and chemical energy Package

Power On Time (min) Specific Electric Energy (kwh/t) EAF Achived savings 700 Specific Electric Energy Consumption 600 500 400 OLD; 582.0 Target; 507.0 Average; 488.0 Electric energy reduction: - 94 kwh/t (-16.2 %) 300 200 90 Power ON Time (all heats) - power OFF < 62 min 100 80 OLD; 74.0 August September October November December January February 0 70 64 264 464 664 864 1064 1264 1464 1664 1864 Heats 60 Average; 64.0 Target; 64.0 Specific Electric Energy (LS) Target Average OLD 10 per. Mov. Avg. (Specific Electric Energy (LS)) 50 40 30 20 10 Power ON reduction: - 10 min (-13.5 %) 0 64 264 464 664 864 1064 1264 1464 1664 1864 Heats Power ON Target Average OLD 10 per. Mov. Avg. (Power ON)

EAF Telescopic Furnace Increased yield due to low oxidation Increased productivity due to one scrap bucket charging High flexibility (one bucket is one steel grade)

Typical process route for tool steels

Refining - Typical units Ladle Furnace Heating Trimming Desulphurisation VD/VOD Degassing Decarburisation

Refining - Tasks Final adjustment of chemical composition Decreasing gas content in the melt Improved steel cleanliness

Refining - Challenges Many steelgrades with challenging target values Various combination of different process units requires clever process modelling

Level 2 Process model Metallurgical Order Management Models Temperature Mass and Chemical Composition of Steel Bath Mass and Chemical Composition of Slag The integrated metallurgical models dynamically (cyclic) calculate the temperature, the mass and the chemical composition of the steel bath and the slag along the whole process route.

Typical results of degassing model Hydrogen content Results presented at AISTech2016 together with

Typical process route for tool steels

Casting

Casting - Trends Bottom pouring is still the dominant process Two major trends can be observed: 1. Mechanisation / automation of ingot casting 2. Continuous casting

ATS advanced teeming system

Segment Casting Tool steels usually cannot be cast on a bow typecaster. Vertical CC have enourmous investment cost. Therefore new plant concepts have to be developed. Features Semi-continuous vertical casting process Combination of advantages of vertical ingot casting with continuous casting Casting steel grades that cannot be cast on a conventional bow-type caster (i.e. alloyed and special steels) Suited for all casting shapes (round, square, rectangular, slab) Up to 1200 mm diameter

Segment Casting Client (Europe)

Typical process route for tool steels

ESR

Why remelting? Cleanliness Level Ingot Structure Forging Operation Reduced content of nonmetallic inclusions Lower size of remaining inclusions Close control of chemical analysis from bottom to top Slow directional solidification Minimization of segregations Minimization of pores Higher Yield Lower forging ratio Cylindrical Ingot with uniform diameter Less Forging Steps Higher ductility, less anisotropy Improved mechanical properties

Ingot structure of ESR material Comparison: left: conventional cast ingot right: remelted condition Microstructure evolution in the annealed condition: Above: conventionally cast ingot Below: ESR remelted ingot

Comparison NMI conventional route VS remelted material Source: G. Reiter (Böhler special steel), LMPC 2013, Austin Texas

Typical Melt Trend in ESR One main objective in ESR is a constant stable remelting rate (given in orange) in order to achieve consistent product quality

Surface quality ESR ø1000mm ESR ingot 1.2083

1963 1967 2016

1985 2004 2013 250.000 tons remelted

1979 2012

Typical process route for tool steels

World Market This document contains INTECO proprietary information and may not be used or disclosed to others without the expressed written permission of INTECO. Data provided by

HSS Powder Production - History Traditional Method 1st Generation 2nd Generation 3rd Generation In the traditional method, pre- The 1st generation is a The 2nd generation is applied The 3rd generation is applied alloyed metal is poured into a development of the traditional for the ERASTEEL ASP and for the BÖHLER UDDEHOLM funnel, acting as a fairly small method to produce powder in DvalinTM process, where a microclean process, where a tundish; no temperature control an atomizing chamber utilizing larger tundish (7 t and 14 t) is larger tundish (approx. 8 t) in and high risks of entrainment of a tundish (approx. 1 t), requiring utilized in combination with combination with INTECO s slag. frequent refilling which leads to Argon stirring and INTECO s ESH and electromagnetic entrainment of slag. electro-slag heating (ESH) stirring system is used, leading system, leading to higher to extremely high powder powder cleanliness with cleanliness, optimized atomi- reduced slag entrainment. zation and closed powder handling.

HSS Powder Production - Today MicroClean Process 8 t Tundish & Electromagnetic Stirring & ESH INTECO IHEC Source: Böhler Edelstahl

Source: ERASTEEL HSS Powder Production - Today Dvalin TM Process 14 t Tundish & Argon Stirring & ESH with ESH

Outlook: General trends in tool steel melting and casting Productivity & yield C C Production costs Automation & mechanisation Product quality Introduce completely new alloy concepts

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