Technical Report PolymerMetall

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Technical Report PolymerMetall TEC-# 006 Microscope photographs, direct-mm-bonding, bonding on contaminated surfaces, pressure tight tests Used products MM-metal ol-steelceramic Description MM-metal ol-steelceramic is a PolymerMetal tested and certified for the repair of oily, greasy or fuel contaminated metals and alloys in case of stress due to cracks, corrosion, abrasion, impact or chemicals. The degree of soiling does not in any way affect the bonding with the structure of the soiled metal surface. High technical data and also the chemical resistance and bonding with the structure on a dirty metallic surface are remarkable features of MM-metal ol-steelceramic. This technology is approved by Lloyd s Register of Shipping. Microscope photographs / direct-mm-bonding The following pictures show microscopic photographs of the fully cured PolymerMetal MMmetal ol-steelceramic magnified by a factor of 100 and 500. Here the bonding between MMmetal ol-steelceramic and metallic surfaces (steel or casting), which have been contaminated by various applied oils before, has been analyzed. on industry gear oil / steel on petroleum / casting

on diesel / steel on compression oil KSL 68 / casting on hydraulic oil T 29-50 / steel on gear oil / machine oil 55 (Magnification 500) MM-metal ol-steelceramic penetrates and absorbs oil, grease and fuel. The direct-mmbonding technology secures the direct and high solid bonding on contaminated surfaces. Bonding on oily surfaces Tests have been carried out to evaluate the quality of the bonding on different surfaces. At the reference test MM-metal ol-steelceramic and Hardener yellow have been applied to a cleaned (that means oil free) and roughened metal surface. The reference value of 100% stands for the quality of the various determined technical data during bending, shearing & hydraulic tests after total curing time. Other values have been determined by applying MM-metal ol-steelceramic on different contaminated metal surfaces. The test results demonstrate that sometimes better technical values were reached after application on oily metal surfaces than on clean metal surfaces.

120 100 Quality of the bonding in % 80 60 40 20 0 clean surface (=reference sample) compression oil KSL 68 pneumatic oil CHX 4400 hydraulic oil T29-50 bed track oil K35/SO68 industry gear oil EP1 industry gear oil EP6 machinery oil 55 Multi Plus 15 40HD SAE diesel motor oil VSL-8 SAE 10W30 petroleum storage grease petrol Type of contamination Testing of pressure tightness To be able to evaluate the quality of the application of MM-metal ol-steelceramic on oily surfaces, tests have been carried out at company M.A.N. under supervision of the classification society Lloyds Register of Shipping. Here special test pipes made off steel have been created according to the following drawing. Around a leakage of a size of diameter 5 mm the metallic shiny surface (Rz 65 μm) of the test cylinder was contaminated with oil. Then the cold-curing MM-metal ol-steelceramic with Hardener yellow was applied around the leakage with a layer thickness of up to max. 8 mm. After full curing of the PolymerMetal the test cylinder has been filled with a liquid and pressure was built up. Then the system was checked against pressure tightness.

Pressure Temperature of Auxiliaries Result test cylinder 100 bar 20 C - pressure tight 150 bar 20 C - pressure tight 200 bar 20 C - after 8 hours small leakage In the course of the time the research and development division of MultiMetall was successful to continue optimising the material MM-metal ol-steelceramic and new tests with same conditions have been carried out at MultiMetall. The following results were achieved: Pressure Temperature of Auxiliaries Result test cylinder 200 bar 20 C - pressure tight 300 bar 20 C - pressure tight 350 bar 20 C - after 2 hours small leakage 150 bar 75 C pipe clip pressure tight 400 bar 75 C pipe clip pressure tight The pipe clip was fixed around the test cylinder in the area of the leakage. Reinforcing elements as e.g. fibres or mats consisting of glass or carbon have not been used. These would have increased the physical strength essentially. The tests have been carried out at M.A.N. (test report No. 1731/82) under supervision of Lloyds Register of Shipping (certificate No. 301954) in 1982, the test at MultiMetall in 1995. Extract of the certificate: The test results of MM-metal ol-steelceramic may be classed as ranging from good to exceptionally good. All test results were in support of the maker s claim that MM-metal ol-steelceramic will bond on oily surfaces with a high degree of reliability. Practical example At Weatherford pressure tests have been carried out with MM-metal ol-steelceramic. The test piece was pressure tight up to a tested pressure load of 4.000 psi (~ 275 bar). Here are some photographs incl. test records:

Further information can be provided upon request. MultiMetall the MetalExistenceCompany The product information and instructions provided in this leaflet were prepared to the best of our knowledge and serve information purposes only. We recommend that appropriate tests are carried out prior to application in order to ensure that the products and methods fulfil the purpose desired by the user. In this procedure, the given data may serve as a basis. Application and processing of the products lie outside our possible control and are therefore the sole responsibility of the user.