ATT- 16/04 ASPHALT RUBBER BLENDING EQUIPMENT INSPECTION, PRODUCTION RATE and PLANT CHECK. Part V, Drum Mix/Asphalt Rubber Plant

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ATT- 16, Part V 1.0 Scope ATT- 16/04 ASPHALT RUBBER BLENDING EQUIPMENT INSPECTION, PRODUCTION RATE and PLANT CHECK Part V, Drum Mix/Asphalt Rubber Plant 1.0 SCOPE Part A - This method describes the procedure for taking temperatures of the asphalt cement and asphalt rubber binder, recording times at various stages of the blend and reaction process, testing the asphalt rubber binder viscosity in the field using a hand held viscometer and verifying the asphalt rubber crumb content on a batch and daily basis to verify the rubber blending equipment calibration. Part B - This method describes the procedures for verifying the drum mix asphalt rubber plant calibration while the plant is operating and for determining the test series and daily totalizer asphalt rubber contents. 2.0 EQUIPMENT 2.1 Asphalt Rubber Blending Equipment Inspection Hand Held Viscometer (Calibrated to the Manufacturer s Specifications and frequencies) 4 litre, round, wide mouth, metal can (clean and dry) Calibrated Long stem thermometer Stirring rod Hot plate Form: Asphalt Rubber Blending Equipment Inspection, ARCP1 2.2 Asphalt Rubber Drum Plant Inspection calculator tachometer stop-watch Form: Asphalt Rubber Drum Plant Inspection, ARCP2 3.0 PROCEDURE (Part A - Asphalt Rubber Blending Equipment Inspection) 3.1 Temperatures 1. Record the following temperatures from the calibrated tank thermometer, for each batch of asphalt rubber binder: The temperature readings of the Asphalt Cement prior to Rubber Crumb addition in Line A, temperature readings of the Asphalt Rubber Binder at start time in reaction tank in Line B and temperature readings of the Asphalt Rubber Binder at end time in reaction tank in Line C of the form as shown in Figure 1. 3.2 Asphalt Rubber Reaction Times 1. Record the following times of the asphalt-rubber reaction process for each batch of asphalt rubber binder.

ATT 16, Part V ASPHALT RUBBER BLENDING EQUIPMENT INSPECTION ARCP1 Form SHEET of CONTRACT NO. PROJECT NO. CONTRACTOR PRIME CONSULTANT AC GRADE DESIGN VISCOSITY RANGE(cP) 9999/99 Hw 99:12 Good Road Builder Good Consultant 150-200A 1500-5000 LOT NO. DATE QC CONSULTANT TECHNOLOGIST(S) TYPE OF VISOMETER RUBBER CRUMB SOURCE & GRADE 1 Sept.2 Good Consultant B. Good Haake Model 5000CP Alberta Environment Products Edmonton BATCH NO. 1 2 3 4 5 6 7 ASPHALT CEMENT AND ASPHALT-RUBBER TEMPERATURES A. TEMPERATURE OF ASPHALT CEMENT PRIOR TO RUBBER CRUMB ADDITION o C 178 185 190 200 202 B. TEMPERATURE OF ASPHALT RUBBER IN REACTION TANK AT START o C 176 180 185 194 198 C. TEMPERATURE OF ASPHALT RUBBER IN REACTION TANK AT END o C 174 178 182 190 195 ASPHALT RUBBER BLEND REACTION TIMES D. ASPHALT RUBBER BLEND REACTION START TIME Hr-min 8:30 9:30 10:30 11:30 1:02 E. ASPHALT RUBBER BLEND REACTION END TIME Hr-min 9:22 10:32 11:45 12:56 2:12 F. ASPHALT RUBBER BLEND TOTAL REACTION TIME (D - E) Hr-min 0:52 1:02 1:15 1:26 1:10 ASPHALT RUBBER VISCOSITY TESTING G. TIME OF VISCOSIY TEST Hr-min 9:22 10:32 11:45 12:56 2:12 H. TEMPERATURE AT TIME OF VISCOSIY TEST o C 175 175 176 174 176 I. FIRST READING cp 2200 2330 3000 3400 2500 VISCOSITY J. SECOND READING cp 2210 2310 3100 3350 2610 TESTS K. THIRD READING cp 2230 2300 3120 3360 2630 L. AVERAGE READING ((I+J+K)/3) cp 2213 2313 3073 3370 2580 M. WT. OF ASPHALT CEMENT DELIVIERED FROM CALIBRATION TOTALIZER RUBBER CRUMB CONTENT REVOLUTION OF PUMP kg/rev. UNIT VOLUME kg/l MASS FOW COUNT 1.023 kg/cnt REVOLUTION, N. FINAL READING 29450 55012 80256 105420 130952 FLOW METER O. INITIAL READING 4379 29450 55012 80256 105420 OR MASS FLOW COUNT P. COUNT O-N 25071 25562 25244 25164 25532 Q. WT OF ASPHALT CEMENT PUMPED INTO MIXING VESSEL PM / 1000 t 25.65 26.15 25.82 25.74 26.12 R. WT. OF CRUMB RUBBER FROM CALIBRATED HOPPER SCALE READING t 6.02 6.12 6.01 6.03 6.08 S. DESIGN OR TARGET RUBBER CRUMB CONTENT % 19 19 19 19 19 T. ACTUAL RUBBER CRUMB CONTENT ((100 R) /( Q + R )) % 19.01 18.97 18.88 18.98 18.88 DAILY RUBBER CRUMB CONTENT U. DAILY TOTAL WEIGHT OF RUBBER CRUMB( SUM of R ) t 30.26 V. DAILY TOTAL WEIGHT OF ASPHALT CEMENT ( SUM of Q ) t 129.48 W. DAILY RUBBER CRUMB CONTENT 100 U / (U + V ) % 18.94 REMARKS: ARCP1/04 FIGURE 1

ATT- 16, Part V 3.3 Asphalt Rubber Sampling The time at the start of the Asphalt Rubber reaction Line D, the time at the end of the Asphalt Rubber reaction Line E as shown in Figure 1. 2. Determine the Asphalt Rubber Blend Total Reaction Time in Line F using the formula D - E" of the form as shown in Figure 1. 3.3 Asphalt Rubber Sampling 1. Obtain a 4 litre sample of the reacted asphalt rubber binder as outlined in ATT - 42 SAMPLING, Asphalt, using the tank mounted sampling valve as outlined in 3.4 Sampling Asphalt Using the Sampling Valve. Bleed off about four litres of asphalt rubber into a separate container to clean out the line before taking a 3/4 full sample for testing. 2. Stir the sample thoroughly and place the calibrated long stem thermometer into the centre of the asphalt rubber binder. 3. Allow approximately one minute for the temperature to stabilize, then take a reading. 4. The temperature of the asphalt rubber binder shall be 175 C +/- 2 C during the viscosity testing. 5. Allow the sample to cool if required. 6. If the sample requires heating before testing, the open asphalt rubber binder sample container should be set on or over the hot plate as appropriate and the sample brought up to the required temperature while being stirred to prevent scorching or burning. 7. Repeat steps 2 and 3 prior to performing the viscosity testing to verify the temperature requirements. 4.0 Equipment Preparation and Viscosity Testing 1. Record the type of viscometer in heading area of the form. 2. Insert the appropriate viscometer spindle in the viscometer. The spindle size should be appropriate for taking measurements within the design viscosity range. 3. The viscosity spindle shall be inserted in the level hot binder sample near the edge of the can for about one minute to acclimatize, without plugging the vent holes. 4. The probe should then be moved to the center of sample to make the viscosity measurements. 5. Ensure the viscometer is level and at the proper immersion depth. The hand held viscometers should have a level bubble for proper orientation (probe shaft perpendicular to binder surface and viscometer level) and an immersion depth mark on the shaft. 6. Once level, begin probe rotation. The peak viscosity value is read from the scale with the corresponding spindle number. 7. Record the time the viscosity tests are taken in Line G, as shown in Figure 1. 8. Record the temperature of the asphalt rubber binder at the time of the viscosity test in Line H, as shown in Figure 1.

ATT- 16, Part V 5.0 Totalizer Rubber Crumb Content 9. Take three measurements and record each peak viscosity value measured on Lines I, J and K of the form, as shown in Figure 1. 10. Between measurements, the viscometer probe should be moved away from the center, without removing it from the sample and the sample thoroughly stirred again. 11. Determine the average viscometer reading of the Asphalt Rubber Blend, and record on Lines L of the form as shown in Figure 1. 5.0 Totalizer Rubber Crumb Content 1. Obtain from the rubber blending equipment calibration data the weight of asphalt delivered per revolution of pump, the weight of asphalt per unit volume or the weight of asphalt delivered per mass flow and record it where applicable in line "M". 2. Record the initial reading on the flow meter, revolution or mass flow counter and record it in line "O". 3. Record the final reading on the flow meter, revolution or mass flow counter and record it in line "N". 4. Determine the flow meter, revolution or mass flow total count using the formula O - N" of the form and record on line P, as shown in Figure 1. 5. Calculate the weight in tonnes of asphalt pumped into the mixing vessel (line "Q") in Tonnes using the following formula, ((PM )/ 1000)". 6. Obtain from the total weight of rubber crumb added to the batch from the calibrated hopper scale reading and record it in line of "R". 7. Record the Design or Target Rubber Crumb Content by total weight of rubber asphalt binder in Line "S". 8. Calculate the Actual Rubber Crumb Content by total weight of asphalt rubber binder (line "T") using the formula ((100R)/(Q+R)). 9. The Design or Target Rubber Crumb Content and Actual Rubber Crumb Content should be within ±1%. 6.0 Daily Rubber Crumb Content 1. Determine the Daily Total Weight of Rubber Crumb used in the production day using the following formula, (SUM of R) and record in Line "U". 2. Determine the Daily Total W eight of Asphalt Cement used in the production day using the following formula, (SUM of Q) and record in Line "V". 3. Calculate the Daily Rubber Crumb Content (line "W") using the formula ((100U)/(U+V)).

ATT- 16, Part V 7.0 Procedure(Part B) 7.0 PROCEDURE (Part B, Asphalt Rubber Drum Plant Inspection) The methods and procedures in ATT-17, PLANT CALIBRATION and ATT-16, PRODUCTION RATE AND PLANT CHECK for Drum Mix Asphalt Plants is followed except the calibration of the asphalt system is done with asphalt rubber binder instead of virgin asphalt cement. The drum plant system checks are done with a weight of asphalt rubber binder delivered into the plant as established during the calibration. An example Asphalt Rubber Drum Plant Inspection form ARCP2 is shown in figure 2. 8.0 HINTS AND PRECAUTIONS 1. Observe and follow the safety precautions outlined in ATT - 42, when sampling and handling asphalt and asphalt rubber binder. 2. Calibrate the thermometers as directed by the equipment manufacturer.

ATT 16, Part V ASPHALT RUBBER DRUM PLANT INSPECTION ARCP2 Form SHEET of CONTRACT NO. PROJECT NO. CONTRACTOR PRIME CONSULTANT 9999/99 Hw 99:12 Good Road Builder Good Consultant LOT NO. DATE QC CONSULTANT TECHNOLOGIST(S) PLANT TYPE 1 Sept.2 Good Consultant B. Good Boeing 400 A WT. OF ASPHALT-RUBBER DELIVIERED FROM CALIBRATION REVOLUTION OF PUMP 2.27 kg/rev. UNIT VOLUME kg/l MASS FOW COUNT kg/cnt TIME 7:30 9:55 13:15 16:05 TEST NO. 1 2 3 4 5 B RELATIVE DENSITY DIAL SETTING C TEMPERATURES D TOTALIZER SPAN SETTING E TOTALIZER ZERO SETTING ASPHALT RUBBER BINDER PLANT MIX o C o C PLANT SETTINGS 9.44 9.44 9.44 9.44 198 205 202 195 164 160 155 148 544 544 544 544 505 505 505 505 F REVOLUTION OR FLOW COUNTER CALIBRATION FACTOR 0.2187 0.2187 0.2187 0.2187 G ELAPSED TIME AGGREGATE H FINAL READING t TOTALIZER I INITIAL READING t J COUNT (H-I) K AGGREGATE MOISTURE CONTENT DIAL SETTING % L DRY AGGREGATE TOTALIZER COUNT 100J/(100 + K) DRY AGGREGATE M METER READING t/h PRODUCTION RATE N ACTUAL 3600 L/G t/h REVOLUTION, FLOW METER O FINAL READING P INITIAL READING AGGREGATE TOTALIZER SYSTEM s t t DAILY 178 180 182 180 DAILY AVERAGE TOTALIZER 37589 38332 39377 40254 40320 37569 38312 39357 40234 37475 20 20 20 20 2845 5.6 5.6 5.6 5.6 5.6 5.6 18.94 18.94 18.94 18.94 2694.13 382 378 376 380 379 383 379 375 379 379 ASPHALT RUBBER TOTALIZER SYSTEM 11847 30132 56541 78875 110000 11100 29380 55800 78130 8974 OR MASS FLOW COUNT Q COUNT O-P 747 752 741 745 101026 SPEED OF R METER READING r/m ASPHALT RUBBER PUMP S ACTUAL 60Q/G r/m T WT OF ASPHALT RUBBER PUMPED QA\1000 t ASPHALT RUBBER U METER READING t/h PRODUCTION RATE V ACTUAL 3600T\G t/h ASPHALT RUBBER W DIAL SETTING % CONTENT X ACT. SETTING(FROM GRAPH) % Y ACTUAL 100T\L % 252 251 245 248 248 251.8 250.7 244.3 248.3 248 1.69569 1.70704 1.68207 1.69115 229.33 34 34 33 34 34 34.3 34.1 33.3 33.8 34 8.5 8.5 8.5 8.5 8.5 8.5 8.5 8.5 8.5 8.5 8.5 8.5 8.4 8.5 8.5 DAILY TOTALIZER ASPHALT RUBBER CONTENT AA TRUCK SCALE TOTAL WEIGHT OF MOIST MIX t 2940 BB MIX MOISTURE CONTENT % 0.4 CC WEIGHT OF DRY MIX 100AA / (100 + BB) t 2928.29 DD WEIGHT OF DRY AGGREGATE CC - T t 2698.96 EE BELT SCALE ERROR 100(DD - L) / DD % 0.2 FF DAILY TOTALIZER ASPHALT RUBBER CONTENT 100 T / DD % 8.50 GG BIN NUMBER 1 r/m BIN MOTOR SPEED HH BIN NUMBER 2 r/m II BIN NUMBER 3 r/m AGGREGATE BIN PROPORTIONING SYSTEM 1410 1400 1390 1420 MATERIAL TYPE BIN NO. 690 680 720 730 510 560 530 540 JJ BIN NUMBER 4 r/m 400 390 430 400 M. F. DRY AGGREGATE KK BIN NUMBER 1 t/h 210 209 207 212 PRODUCTION RATE LL BIN NUMBER 2 t/h 84 82 86 87 Other NA (FROM CALIBRATION GRAPH) MM BIN NUMBER 3 t/h 56 56 52 53 NN BIN NUMBER 4 t/h 30 29 33 30 OO TOTAL BIN DRY AGG. PROD. RATE KK+LL+MM+NN t/h REMARKS: PP BIN NUMBER 1 100KK/OO PERCENT SPLIT QQ BIN NUMBER 2 100LL/OO RR BIN NUMBER 3 100MM/OO 380 376 378 382 Coarse N. F. B.S. DAILY AVERAGE 1 2 3 4 DESIGN OR TARGET 55.3 55.3 54.8 55.5 55.3 56 22.1 21.8 22.8 22.8 22.4 22 14.7 14.9 13.7 13.9 14.3 14 SS BIN NUMBER 4 100NN/OO 7.9 7.7 8.7 7.8 8 8 FIGURE 2 ARCP2/04