SCOPE OF ACCREDITATION TO ISO/IEC 17025:2005

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SCOPE OF ACCREDITATION TO ISO/IEC 17025:2005 MICROBAC LABORATORIES, INC., KTL DIVISION 3323 Gilmore Industrial Blvd. Louisville, KY 40213 Megan Rothgerber Phone: 502 962 6400 CHEMICAL Valid To: December 31, 2019 Certificate Number: 0085.04 In recognition of the successful completion of the A2LA evaluation process, accreditation is granted to this laboratory to perform recognized EPA methods using the following testing on non-potable water, soil, stillage, coating, paper, polymers, petroleum (oil, tar, lubricants) and metals: Testing Technologies: ICP AES Spectrometry, ICP-MS, Discrete Analyzer, Gas Chromatography, Gas Chromatography/Mass Spectrometry, Gravimetry, Ion Chromatography, Methylene Blue Active Substances, Microbiology, Misc.- Electronic Probes (ph, O2, Redox), Oxygen Demand, Hazardous Waste Characteristics Tests, Spectrophotometry (Visible), Titrimetry, Turbidity, TKN Gas Dispersion Skalar. Parameter/Analyte Metals Aluminum EPA 200.7 Antimony EPA 200.7 Arsenic EPA 200.7 Barium EPA 200.7 Beryllium EPA 200.7 Boron EPA 200.7 Cadmium EPA 200.7 Calcium EPA 200.7 Chromium EPA 200.7 (A2LA Cert. No. 0085.04) 12/28/2017 Page 1 of 7

Cobalt EPA 200.7 Copper EPA 200.7 Iron EPA 200.7 Lead EPA 200.7 Magnesium EPA 200.7 Manganese EPA 200.7 Molybdenum EPA 200.7 Nickel EPA 200.7 Phosphorous EPA 200.7 Potassium EPA 200.7 Selenium EPA 200.7 Silver EPA 200.7 Sodium EPA 200.7 Strontium EPA 200.7 Thallium EPA 200.7 Tin EPA 200.7 Titanium EPA 200.7 Vanadium EPA 200.7 Zinc EPA 200.7 Nutrients Ammonia (as N) SM 4500-NH3 G Nitrogen (Kjeldahl) SM 4500-NH3 G Nitrate (as N) EPA 300.0 (A2LA Cert. No. 0085.04) 12/28/2017 Page 2 of 7

Nitrite (as N) EPA 300.0 Nitrate-Nitrite (as N) EPA 300.0 Orthophosphate (as P) EPA 300.0 EPA 365.1 Total Phosphorus EPA 365.1 Demands Biochemical Oxygen Demand Carbonaceous BOD Chemical Oxygen Demand Total Organic Carbon SM 5210B SM 5210B SM 5220D SM 5310C Wet Chemistry Acidity SM 2310B Alkalinity SM 2320B Bromide EPA 300.0 Chloride EPA 300.0 SM 4500-Cl G Chromium, hexavalent SM 3500-Cr B Color, ADMI SM 2120C Conductivity (Specific Conductance) SM 2510B Fluoride EPA 300.0 Hardness SM 2340B ph EPA 9040C EPA 9045D SM 4500-H+ B MBAS (Surfactants) SM 5540C Oil & Grease EPA 1664B Solids, total USGS I-3750-85 Solids, total suspended USGS I-3765-85 Solids, dissolved SM 2540C Solids, settleable SM 2540F Solids, volatile USGS I-3753-85 Sulfate EPA 300.0 Sulfide SM 4500-S 2 D Sulfite SM 4500-SO3 2 B Turbidity SM 2130B (A2LA Cert. No. 0085.04) 12/28/2017 Page 3 of 7

Microbiology Coliforms, total SM 9223B (Colilert and Colilert 18) Escherichia coli SM 9223B (Colilert and Colilert 18) Coliforms, fecal SM 9222D (Colilert and Colilert 18) Enterococci ASTM D6503-99 Pseudomonas SM 9213E Pureable Organics (Volatiles) Acetone EPA 624 Acrolein EPA 624 Benzene EPA 624 Bromobenzene EPA 624 Bromochloromethane EPA 624 Bromodichloromethane EPA 624 Bromoform EPA 624 Bromomethane EPA 624 2-Butanone EPA 624 n-butylbenzene EPA 624 sec-butylbenzene EPA 624 tert-butylbenzene EPA 624 Carbon disulfide EPA 624 Carbon tetrachloride EPA 624 Chlorobenzene EPA 624 Chloroethane EPA 624 2-Chloroethyl vinyl ether EPA 624 Chloroform EPA 624 (A2LA Cert. No. 0085.04) 12/28/2017 Page 4 of 7

Chloromethane EPA 624 2-Chlorotoluene EPA 624 4-Chlorotoluene EPA 624 Dibromochloromethane EPA 624 1,2-Dibromo-3-chloropropane (DBCP) EPA 624 Dibromomethane EPA 624 1,2 Dibromomethane (EDB) EPA 624 1,2-Dichlorobenzene EPA 624 1,3-Dichlorobenzene EPA 624 1,4-Dichlorobenzene EPA 624 Dichlorodifluoromethane EPA 624 1,1-Dichloroethane EPA 624 1,2-Dichloroethane EPA 624 1,1-Dichloroethene EPA 624 cis-1,2-dichloroethene EPA 624 trans-1,2-dichloroethene EPA 624 1,2-Dichloropropane EPA 624 1,3-Dichloropropane EPA 624 2,2-Dichloropropane EPA 624 1,1-Dichloropropene EPA 624 cis-1,3-dichloropropene EPA 624 trans-1,3-dichloropropene EPA 624 (A2LA Cert. No. 0085.04) 12/28/2017 Page 5 of 7

trans-1,4-dichloro-2-butene EPA 624 Ethyl benzene EPA 624 2-Hexanone EPA 624 Hexachlorobutadiene EPA 624 Isopropylbenzene EPA 624 p-isopropyltoluene EPA 624 Iodomethane EPA 624 Methylene chloride EPA 624 Methyl ethyl ketone (MEK) EPA 624 Methyl isobutyl ketone EPA 624 Methyl-t-butylether (MTBE) EPA 624 4-Methyl-2-pentanone EPA 624 Naphthalene EPA 624 n-propylbenzene EPA 624 Styrene EPA 624 1,1,1,2-Tetrachloroethane EPA 624 1,1,2,2-Tetrachloroethane EPA 624 Tetrachloroethene EPA 624 Toluene EPA 624 Total Petroleum Hydrocarbons (TPH) EPA 624 1,1,1-Trichloroethane EPA 624 1,1,2-Trichloroethane EPA 624 (A2LA Cert. No. 0085.04) 12/28/2017 Page 6 of 7

1,2,3-Trichlorobenzene EPA 624 1,2,4-Trichlorobenzene EPA 624 1,3,5-Trichlorobenzene EPA 624 Trichloroethene EPA 624 Trichlorofluoromethane EPA 624 1,2,4-Trimethylbenzene EPA 624 1,3,5-Trimethylbenzene EPA 624 Vinyl acetate EPA 624 Vinyl chloride EPA 624 Xylenes, total EPA 624 1,2-Xylene EPA 624 1,3-Xylene EPA 624 1,4 Xylene EPA 624 Sample Preparation/Extraction Methods Metals EPA 3005 EPA 3050B Nutrients SM 4500 NH-B Ignitability EPA 1010A Synthetic Precipitation Leaching Procedure EPA 1312 ASTM D3987 Toxicity Characteristic Leaching Procedure EPA 1311 Paint Filter Liquids Test EPA 9095 (A2LA Cert. No. 0085.04) 12/28/2017 Page 7 of 7

Accredited Laboratory A2LA has accredited MICROBAC LABORATORIES, INC., KTL DIVISION Louisville, KY for technical competence in the field of Chemical Testing This laboratory is accredited in accordance with the recognized International Standard ISO/IEC 17025:2005 General requirements for the competence of testing and calibration laboratories. This accreditation demonstrates technical competence for a defined scope and the operation of a laboratory quality management system (refer to joint ISO-ILAC-IAF Communiqué dated 8 January 2009). Presented this 28 th day of December 2017. President and CEO For the Accreditation Council Certificate Number 0085.04 Valid to December 31, 2019 For the tests to which this accreditation applies, please refer to the laboratory s Chemical Scope of Accreditation.