Detection of Thermal Cracks in Early-Age Concrete by AE

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www.crl.issres.net Vol. 2 (3) Sep. 211 Detection of Thermal Cracks in Early-Age Concrete by AE T. Watanabe 1c, T. Ohno 2, and C. Hashimoto 1 1 Department of Civil and Environmental Engineering The University of Tokushima, JAPAN 2 Tekken Corporation, JAPAN Abstract Early-age cracking after casting is a fundamental problem for the durability of concrete structures. Recently, thermal cracks and early-age cracks have been observed in concrete containing Portland cement with blast-furnace slag in Japan. In order to reduce the number of these cracks, fly ash is substituted for cement or sand. Fly ash is one of the popular admixtures as a waste material from coal-fired power plants. To evaluate the effect of fly ash on early-age cracks, experimental studies were performed. In order to detect microcracking in concrete, acoustic emission (AE) measurement was applied. In experiments, two types of fly ash, typeⅡ and Ⅳ categorized by JIS were employed. The ratio to substitute cement and sand was 1% and 2%. As a result, micro-cracks in concrete were detected by the AE method. Results show that substitution of fly ash for cement and sand is effective to reduce micro-cracking due to thermal changes which occurs from 2 to 3 hours elapsed after casting of concrete. Keywords: Thermal cracks; AE method; Blast-furnace slag; Fly ash, Early-age cracks. 1. Introduction Early-age cracking after casting is considered to be an essential problem for the durability of concrete structures. In Japan, Portland cement mixed with blast-furnace is widely employed to prevent concrete from thermal cracking by reducing heat of hydration. Recently, however, thermal cracks and early-age cracks have been observed in concrete containing Portland cement with blastfurnace slag. This is because the function to reduce heat of hydration becomes weak in order to improve the early-age strength. As a remedy to reduce the occurrence of early-age cracks in concrete of Portland cement with blast-furnace slag, fly ash is known to be applicable to substitute for cement and sand. Previously, it was observed that the number of settlement cracks and the averaged crack-widths decreased with the substitution of fly ash for sand [1]. The settlement crack is one example of the early-age cracks. In order to evaluate the effect of fly ash on preventing from early-age cracks, experiments on c Corresponding Author: Takeshi Watanabe Email: watanabe@ce.tokushima-u.ac.jp Telephone: +81 88-656-732 Fax: +81 88-656-7351 29-212 All rights reserved. ISSR Journals 29

Takeshi Watanabe & Tomonori Ohno Concrete Research Letters Vol. 2 (3) Sep. 211 thermal cracks are performed. To detect micro-cracking readily, acoustic emission (AE) method is applied in the measurement. 2. Experiments 2.1. Mixture proportion and physical properties of materials Governing equations Four kinds of concrete mixes; BBFA, BBFA2, BBFA1, NFA2 are shown in Table 1. Physical properties of materials are given in Table 2. In this study two types of fly ash, type Ⅱ and Ⅳ categorized by JIS are used. BBFA1 is a control concrete without fly ash, using Portland cement with blast-furnace slag. BBFA2 is a concrete using fly ash of type Ⅱ by substituting 2% Portland cement with blast-furnace slag. BBFA1 is concrete using fly ash of type Ⅳ by substituting 1% sand. NFA2 is a concrete using fly ash of type Ⅱ by substituting 2% ordinary Portland cement. Specimens BBFA G max () TABLE 1: MIXTURE PROPORTION OF CONCRETE SPECIMENS Slump Air W/C s/a Unit wait (kg/m 3 ) (cm) (%) (%) (%) W C FA S G AD AE 54 46.5 166 38-822 946 3.8 1.54 BBFA2 1± 4.5± 46 44.5 162 282 71 766 953 3.53 4.59 2 BBFA1 2. 1.5 54 45.5 164 34 68 727 969 3.4 5.32 NFA2 46 44.5 164 286 71 766 953 3.57 3.93 W: water, C: cement, FA: fly ash, S: sand, G: gravel, AD: super plasticizer, AE: air-entrained agent Material Cement Fly ash Sand TABLE 2: PHYSICAL PROPERTIES OF MATERIAL. Properties Portland blast-furnace slag cement, Type B (JIS Category) ρ=3.4g/cm 3 Ordinal Portland cement, ρ=3.15g/cm 3 Fly ash Ⅱ (JIS Category) ρ=2.28g/cm 3 Fly ash Ⅳ(JIS Category) ρ=2.2g/cm 3 Crushed sand, ρ=2.57g/cm 3, F.M. 2.95 Sea sand, ρ=2.57g/cm 3, F.M. 2. Coarse aggregate Crushed stone (15-5), ρ=2.57g/cm 3 Admixture Super plasticizer (polycarboxylic acid type) and AE 2.2. Detection and Evaluation of Cracks A sketch of a specimen tested to evaluate thermal cracks is shown in Fig.1, of which dimensions are 18 x 9 x 4. A deformed steel bar with 22 diameter is set at a height of 5 from the bottom of the specimen. This bar served as a waveguide of AE detection in addition to reinforcement. Gauges to detect strain and temperature are also set as denoted in the figure. Measurement of AE activity, strain and temperature started right after casting of concrete. AE phenomenon is defined as elastic-wave emission produced by micro-fracturing in a solid [2]. Time history of AE hits is useful for detection of cracking in concrete. In most cases, abrupt increase of AE hits is associated with failure in concrete. This is because AE activity is physically correlated with nucleation of cracks in concrete. 291

Detection of Thermal Cracks in Early-Age Concrete by AE 18 4 9 AE sensor Strain and temperature gauge 1 35 35 D22 Deformed bar 5 5 Base concrete Figure 1. Sketch of specimen for evaluation of thermal cracks. Compressive strength (N/²) 45 4 35 3 25 2 15 1 5 3days 7days 28days 91days BBFA BBFA2 BBFA1 NFA2 Spesimens Figure 2. Results of compressive tests. 3. Results and discussion Results of the compression tests based on JIS A 118 are shown in Fig. 2. Compressive strengths of all specimens are about 3 N/ 2 at 28days. This is because mixture proportions in Table 1 are controlled to keep the compressive strengths around 3 N/ 2. In order to detect thermal cracks, AE sensors were attached to both ends of rebar in the specimen as shown in Fig. 1. Relationships between cumulative AE hits and temperature in concrete are presented in Fig. 3. Here, AE hits which were detected by both sensors are only plotted. Since AE activity is different in each specimen, evaluation is conducted qualitatively in the relationship with temperature. Concerning temperature variations, reduction of the maximum temperate with addition of fly ash is not clearly observed. of all specimens increase between 2 and 3 hours elapsed. It is considered that concrete temperature increases from to 2 hours elapsed due to hydration of cement, and then temperature decreases. A similar trend is observed in strain changes. In a laboratory test, it was observed that AE hits were actively detected until when temperature started decreasing [3]. Comparing AE activity between BBFA and BBFA1, it is found that almost of all AE hits are observed from 2 to 5 hours elapsed in BBFA. AE hits in BBFA1 also occur from 2 to 5 hours elapsed, although AE activity is fairly low in this period and AE hits are continuously observed until 15 hours. In BBFA2 and NFA2, AE activities have two highly active periods at 2 hours and after 1hours. These results imply that fly ash acts effectively to reduce micro- 292

Takeshi Watanabe & Tomonori Ohno Concrete Research Letters Vol. 2 (3) Sep. 211 cracking due to thermal changes in the early stage (the first active period) from 2 to 3 hours after casting concrete. Based on visual inspection, the second active period could be associated with drying shrinkage of concrete. Results of visual inspection on crack widths are suarized in Table 3. These cracks were not recognized right after casting, but found within a week after casting. This implies that a driving force for these cracks could be not only thermal change but also drying shrinkage. According to experimental observation, it seems that micro-cracks due to thermal change occur fast, and then cracks grow due to drying shrinkage. In Table 3, it is observed that averaged crack widths of specimens are almost similar except NFA2, where cracks are not observed. BBFA 8 7 6 5 4 3 2 1 Temperature 外気温 Concrete コンクリート温度 temperature ( 上部 (top) ) Concrete コンクリート温度 temperature ( 中部 (mid.) ) Concrete コンクリート温度 temperature ( 下部 (bottom) ) 6 2 4 6 8 1 12 14 16 5 4 3 2 1 BBFA2 18 16 14 12 1 8 6 4 2 Temperature 外気温 Concrete コンクリート温度 temperature ( 上部 (top) ) Concrete コンクリート温度 temperature ( 中部 (mid.) ) Concrete コンクリート温度 temperature ( 下部 (bottom) ) 6 2 4 6 8 1 12 14 16 5 4 3 2 1 Cumulativi AE hits BBFA1 8 7 6 5 4 3 2 1 外気温 Temperature コンクリート温度 Temperature ( 上部 ) コンクリート温度 Concrete temperature ( 中部 (mid.) ) コンクリート温度 Concrete temperature ( 下部 )(mid.) 6 2 4 6 8 1 12 14 16 5 4 3 2 1 NFA2 14 12 1 8 6 4 2 外気温 Temperature コンクリート温度 Concrete temperature ( 中部 (mid.) ) Concrete コンクリート温度 temperature ( 下部 ) 6 2 4 6 8 1 12 14 16 Figure 3. Relationship between cumulative AE hits and temperature in concrete. 5 4 3 2 1 TABLE 3: CRACK WIDTHS IN SPECIMENS () number of cracks BBFA BBFA2 BBFA1 NFA2 1.96.77.93-2.17.75.85-3.75.78.79-4 -.89 - - Average.93.8.86-4. Conclusion Experiments were performed to evaluate the effect of fly ash on early-age cracking in concrete made of Portland cement with blast-furnace slag. Thermal cracking was detected by AE method. As a result, micro-cracking due to thermal change was observed, prior to drying shrinkage. AE activity detected implies that fly ash serves to reduce micro-cracking due to thermal change which occurred from 2 to 3 hours after casting concrete. 293

Detection of Thermal Cracks in Early-Age Concrete by AE References [1] Hashimoto, S., Hashimoto, C., Watanabe, T. and Mizuguchi, H. Study on Evaluation on Settlement Cracks occurring on the Concrete Surface above Steel Bars of Reinforced Concrete Slab by Nondestructive Testing, Proceedings of the 1th International Conference on Structural Faults and Repair, 23, CD-ROM. [2] Ohtsu, M., Acoustic Emission Theory for Moment Tensor Analysis, Research in Non- Destructive Evaluation, ASNT, 1995, 6: pp.169-184. [3] Son, H. N., Hosoda, A. and Watanabe, T. Characterization of Microcracking in Very Early Age Concrete subjected to Elevated Temperature by AE, Proceedings of The Japan Concrete Institute, 21, 31: pp. 323-328 294