Rev. 2 Crprate Presentatin
Clant Out (H 2 O) Cndenser Clant In (H 2 O) Sxhlet Uses cld slvent, and takes a lng time; the slvent passes thrugh the thimble. (Gldfish, similar methd but with lwer slvent cnsumptin than Sxhlet); Immersin Washing Recvery Twisselman Ht extractin with the slvent flwing thrugh the sample in the thimble; Sxhlet Extractin Randall Extractin Randall Ht extractin by immersing the thimble int the biling slvent t ptimize speed and slvent used. Als knwn as «Ht Slvent Extractin». 2
Slvent extractin is a methd fr the separatin f mixtures by using the differences in the slubilities f the cmpnents. The sample is immersed in the ht, biling slvent. Later n, the sample needs t be washed ff with fresh slvent. In autmated systems, as urs, this happens either by pulling ut the sample r by reducing the level f slvent. It is a «slid-liquid extractin», allwing sluble cmpnents t be remved frm slids using a slvent. 3
The use f slvent extractrs can be divided in tw grups f applicatin: Fat Determinatin Fr bth «crude» and «ttal» fats. Mst f the fd prducts cntain fat, but als nn-fd samples can be prcessed Sample Preparatin When slvent extractin cmes befre further tests t extract pllutants and cntaminatin elements, mainly frm envirnmental testing 4
«Crude» methds invlve disslving the material in a slvent such as ether r hexane and then evaprate the slvent. What remains, is called «crude fat». 5
The «ttal fat» test invlves analytical instruments that separate the fat cmpnents int varius fatty acids. Ttal fat analysis cnsists f tw steps: Hydrlysis In rder t determine encased fat the cell matrix needs t be brken up. When heat is applied, the hydrchlric acid breaks fatty acids frm ther elements. Extractin The dried mass cntaining fat is extracted with slvents (e.g. petrleum ether), the slvent evaprated and the residue weighed. 6
Acid Hydrlysis Meat, seafd, cca, cereal meals, eggs, nuts, bread derived prducts, pasta, seeds and related prducts. Animal feed Basic Hydrlysis Milk and related prducts like cheese, fresh cheese, mzzarella, cndensed milk, sugar lactse, etc. HU6 Hydrlysis Unit 7
Use SER 158 Series fr quick, simple, precise and reliable fat determinatin in Fd & Feed Testing Dairy Prducts and Baby Fd Cereals & Bakery Prducts Meat and Derived Prducts Chclate and Caca Prducts Oil and Oil Seeds Fried Ptates Creams, Sauces and Dressings Fruits and Vegetables Eggs and Derived Prducts Feeds and many mre 8
It is als suitable fr ther relevant tests in nn-fd samples, like: Oil and Fat in Water and Waste Water Hydrcarbns frm Sil Oil in Sludges Paraffin in Wd Chips Fat Cating f Artificial Fertilizers Oil frm Textiles & Synthetic Fibres Insulating Wl Residue f Resin in Paper Unsapnified & Unsapnifiable Fat Oil in Leather and many mre 9
Its real applicatins are extendable als t Sample Prep fr additinal tests: Rcks Oil and Lubricants Pesticides Phenls PCB - Ply Chlrinated Biphenyls Dixins Sfteners/Additives in Plastic & Rubber Clrant n Textile Fibers Catings f Fertilizers PAH - Ply Armatic Hydrcarbns EOX - Extractable rganic halides and many mre 10
THE STATE-OF-THE-ART SOLUTION FOR RELIABLE EXTRACTIONS WITH A SCALABLE & AUTOMATED SYSTEM Fully autmated 3 r 6 psitins, with slvent additin, immersin, remval, washing, recvery & safety peratin; Select hw many & which psitins t use. Up t 4 SER units can be cnnected, allwing vernight peratin with the autmatic stand-by mde: lad & g; Autmatic calculatin and visualizatin f the results, then saved n the n-bard archive. 11
DRASTIC REDUCTION IN THE COST PER ANALYSIS WITH UNMATCHED PERFORMANCE Patented titanium cndensers, n need fr external cler: titanium can be up t 20x mre efficient than glass; High recvery rate (> 90%) thanks t titanium cndensers, efficient seals and internal tank; This brings t reduced cnsumptin f slvent and the lwest cling water need thanks t cling water flw cntrl. 12
TAILORED SOLUTION TO VIRTUALLY SUIT ANY CUSTOMER REQUIREMENT Feel free t use different slvents fr extractin and t chse amng several thimbles and cups ; Vafln seal is able t stand several types f slvent and it is ideal fr diversified applicatins; Ultra-fast glass ceramic heating plate with aut-lift after the recvery t prevent sample burning/verheating. 13
OUTSTANDING SAFETY STANDARD TO PREVENT ANY INCONVENIENCE TO THE END USER N expsure t slvent, thanks t a smart dispsing system fr easy and secure prcedure in slvent additin; Visual recvery tank (n the back) with ptical sensr fr a maximum safety; Overtemp. prtectin n each heater, with individual n/ff switches; Prtectin screen fr extractin chamber 14
THE MOST MODERN EXTRACTOR EQUIPPED WITH A REAL, YET INTUITIVE POWERHOUSE Prgrammable cntrl pad with 7 tuch screen and intuitive settings fr clear cmmunicatin and ease f use; Pre-installed methds library & custmizable prgrams; Smart features, like easy menu navigatin, quick-start Analysis buttn, recall f favrite methds, result calculatin, and much mre. 15
TIME SAVING» intuitive and quick setting» rapid, fully-aut slvent additin ENERGY SAVING» titanium cndensers fr unmatched efficiency» limited water cnsumptin, frm 1.0 L/min MONEY SAVING» substantial cst reductin» mre than 90% recvery means lwer OPEX SPACE SAVING» extremely cmpact ftprint saves bench space 16
With SER 148/3 and SER 148/6 With SER 158/3 and SER 158/6 Immersin The thimble with the sample is immersed int the ht biling slvent and remains there fr a certain perid f time Washing (als knwn as Rinsing) The slvent flws thrugh the thimble, after this has been lifted ut frm the slvent Recvery Slvent is recvered by clsing the stpcck and the extracted slutin is cllected in the glass cup Immersin Same as n SER 148 Series Remval Slvent vlume is autmatically reduced Washing (als knwn as Rinsing) The slvent flws thrugh the thimble Recvery Autmatic slvent recvery. The glass cup with the extracted slutin lifted t prevent sample burning Safety Operatin Cndensatin with water cntinues t ensure cmplete safety 17