Metallic Additive Manufacturing Process and Materials Development at the University of Sheffield

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Metallic Additive Manufacturing Process and Materials Development at the University of Sheffield 3 rd June 2015 2 nd Mexican Workshop on Additive Manufacturing 3D Printing Queretaro Mexico Dr Kamran Mumtaz Centre for Advanced Additive Manufacturing 19

Presentation Overview 1) About Me 2) University of Sheffield 3) Advanced Additive Manufacturing (AdAM) Centre -Facilities -Academic Staff/Research Team 4) Snapshot of Non Metallic Activities - Polymer, inkjet and composite technologies 5) Overview of Metallic AM Research Areas 6) Detail into specific process and materials development projects - Topology Optimisation - Stress Reduction - Novel Processes Development - Multi-Materials - Materials Development

Background -DrKamran Mumtaz Involved in Additive Manufacturing research activities since 2005 2004 BEng (Hons) Aeronautical Engineering - Manchester 2005 MSc Manufacturing Management - Loughborough 2008 PhD laser powder bed fusion of Nickel alloys -Loughborough 2008-2011- Research associate - Loughborough University/Industrial Secondments 2011 Lecturer in Additive Manufacturing - The University of Sheffield 2012- Co-founded AdAM Centre at the University of Sheffield Process and Materials Development for Metallic AM Understand limitations of current AM process/materials, develop more efficient processes, improved capability, novel processes, multi-materials, process simulation etc.

- Russell Group University - Top 5 in UK for Mechanical Engineering - Top 100 University 2014 world QS Rankings - 7000 Staff and more than 26,000 students from around the world University of Sheffield

University of Sheffield - 86% of our research assessed as world-leading or internationally excellent - 2014 Research Excellence Framework top 10% of all UK Universities - Advanced Manufacturing Research Centre (AMRC) with Boeing, includes Nuclear & Medical AMRC

Advanced Additive Manufacturing Centre - World leading AM research activities - Multi-disciplinary approach, AM research activities and facilities spread across multiple departments, encouraging innovation in research - Employs over 40 staff and researchers - Over 20 commercial and bespoke additive manufacturing technologies - Industrial work - Siemens, Rolls Royce, Philips, GKN etc.

AdAMCentre Academics Polymer Technologies Metal Technologies Design for AM Prof N Hopkinson (Head of Centre) Dr C Majewski Prof I Todd Dr K Mumtaz Prof M Gilbert Jetting Technologies Bio-Printing Dental AM Applications Prof R Noort DrI Ortega DrP Smith Dr F Claeyssens

AdAMCentre Facilities Polymers - X2 Object polymer jetting - EOS Formiga Laser Sintering - X2 custom High Speed Sintering - Custom multi-laser sintering system - X4 custom desktop 3D printers - X2 custom micro stereolithography - Custom Ink Jetting system - Custom extrusion based 4-axis robot Metals - X3 Arcam Electron Beam Melting (customised) - X2 Renishaw Selective Laser Melting (customised) - ExOne Binder Jetting - Optomec Aerosol Jet - Custom multi-laser melting system - Custom extrusion based system Other Advanced Manufacturing - Metal Injection Moulding - Spark Plasma Sintering - ProBeam Welder (electron beam) - Post Treatment (HIP, Vacuum Furnace, shot blast etc.)

Snapshot of Non-metallic AM activities High Speed Sintering Polymers Development driven by need to increase AM productivity and reduce the cost per part Replaces conventional scanning lasers with a print head infra-red lamp to significantly increase build speed and increase build volume

Snapshot of Non-metallic AM activities Inkjet Technologies Effect of inkjet printed polymer on mechanical performance of Carbon FibreReinforced Polymers (CFRP) Toughening CFRP by printing thermoplastic polymers between laminate sheets before curing Polymer phases ease/arrest crack propagation. Minimise weight gain After Printing After Heating A highly controllable size and geometrical distribution of the thermoplastic inkjet printed microphasesare believed to be the contribution to the enhanced mechanical properties. Polymer phase

Snapshot of Non-metallic AM activities Bio-printing with Stereolithography Restoring damaged nerve function Nerve guidance conduit (NGC) Create scaffolds from a photopolymerizable liquid that bio-degrades once nerve as been repaired Non-Conventional AM Materials (often requiring process development) Ceramic processing Various composite materials (i.e SFRC) Sustainable materials (i.ewood waste feedstock to create large structures, shelters)

Overview of Metallic Activities Understanding of existing processes (repeatability, process simulation etc.) Tackle common issues (i.estress development, surface finish, speed, material variety etc.) Design Optimisation(i.elightweight structures) New Materials (AM specific alloys) Novel Processes (faster, more efficient, introduce further capability advantage) Multi-materials Large list of materials processed/attempted. Steel, Nickel, Cobalt Chrome, Aluminium, Copper, Magnesium, Titanium alloys, graded materials etc.

Understanding and Development of Process Rolls Royce Engine Stator Vanes for Ring of Vanes - Build orientation and support structures - Process optimisation-build quicker, eliminate defects - Support to down stream processes e.g. machining, finishing & welding - Pre-production repeatability - Key process variables identified and controlled - Increase in build process speed

Understanding and Development of Process Process Simulation - Numerical modeling used extensively in casting industry, nothing yet developed for powder bed AM - Can assist with understanding of process and prediction of resultant microstructures, customisation, single crystal structure etc. - Assists process parameter optimisation 3D Single Spot Temperature profile at the powder bed (SLM) developed with FEM. Powder Layer Solidified Track 120 μm 250 μm Argon Flux Liquid Mushy Zone Substrate 3D Single Spot Solidification front tracking on melt pool (SLM) developed with FEM. 2D FEM Single Layer Solidification front tracking on melt pool (SLM).

Understanding and Development of Process Process Simulation

Topology Optimisation Lightweight Structures - Minimal mass structures - 69% weight saving achieved using structural topology optimisationfor bracket/hinge Topology Optimised Design Original Design

Topology Optimisation Lightweight Structures - Bloodhound land speed record

Topology Optimisation Lightweight Structures - Lattice structures for testing impact loads - Lattice like structures have high surface area making them ideal for thermal management applications - Meta-material behaviours!

Stress Reduction Methods to Reduce Residual Stress - Parameter optimisationto reduce thermal variations across build - Examine effects on mechanical properties

Stress Reduction & Requirement for Supports

Stress Reduction & Requirement for Supports

Novel method to reduce stress and remove requirement for support structures - Anchorless Selective Laser Melting - Maintain material is semisolid state throughout build, similar to SLS - Combine careful custom elevated powder bed preheat with specially prepared elemental mix of materials Stress Reduction using Anchoress SLM

Stress Reduction using ASLM Novel method to reduce stress and remove requirement for support structures

Stress Reduction using ASLM Novel Method to Reduce stress and remove requirement for support structures Large flat geometries impossible to build without support structures/anchors using conventional SLM/EM x50 100µm layers 40mm

Novel Method to Reduce stress and remove requirement for support structures Large flat geometries impossible to build without support Stress Reduction using ASLM

Novel Method to Reduce stress and remove the requirement for support structures Geometries within geometries Stress Reduction using ASLM

Novel Method to Reduce stress and remove the requirement for support structures Aluminium alloys, AlSi12, Al339, AlCu Future work seeks to expand materials available Stress Reduction using ASLM

Enhance properties through grading of materials Prevent/design failure Mechanical property control Thermal management etc. Multi-Materials AM

Custom Alloys for AM Custom Materials Designed for AM - Better Materials (improved performance, reduced processing issues) - Growing research area - Example of work -certain aerospace nickel alloys suffer from high crack susceptibility Ultimate Tensile Strength Custom SLM? EBM Elongation % 50 μm 10 μm Rickenbacher, L. (2013) Rapid Prototyping Journal 19(4): 282-290.

Alloys for AM Reduce crack susceptability in Nickel alloy - Calculated composition manipulation of existing alloy Alloy Ni Cr Fe Mo Co Mn Si W C MHX wt% 46.55 21.80 18.6 9.4 1.77 0.22 0.31 1.05 0.054 OHX wt% 47.87 21.3 19.5 9.0 1.04 0.48 0.32 0.56 0.057 Δc(At. Frac) -0.01 0.007 0.0004 0.003 0.007-0.003-0.0002 0.0016-0.0001 k (MPa At. Fraction- 1/2) - 337 153 1015 39.4 448 275 997 1061 8.31

Custom Alloys for AM Cracks per mm 2 Cracks per mm 2 50 45 40 35 30 OHX H 25 20 MHX H 15 10 Average reduction 5 0 0.2 0.25 0.3 0.35 0.4 0.45 0.5 0.55 0.6 of 65% 40 35 30 25 20 15 10 5 0 0.2 0.25 0.3 0.35 0.4 0.45 0.5 0.55 0.6 OHX V MHX V As observed in the horizontal section As observed in the vertical section 1D energy density (J/mm)

Working with Mexico - Currently supervise PhD students from Mexico (CONACYT) Simulation of Microstructure within laser powder bed Stress free Aluminium AM components Machining of Ti64 AM components - University of Sheffiedalready hasa good relationship with Mexican research institutions and Universities - Many Mexican students registered on our Advanced Mechanical MSc with AMRC/Boeing Omar Lopez Botello Novel multi-laser metallic powder bed processing Rafael A M Ramos Stress reduced Ti64 AM processing Marco A Galindo Bespoke nickel alloys for metallic AM - Initiated AM related collaboration with UANL, Mexico. If funded 18 month project will start in September 2015 Miguel A Z Arredondo Haider Ali Neil J Harrison

And Finally Visit www.adamcentre.co.uk Contact Dr Kamran Mumtaz k.mumtaz@sheffield.ac.uk