Ytterbium-doped Aluminum-codoped Sol-Sel Silica Glass Fiber Laser

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Ytterbium-doped Aluminum-codoped Sol-Sel Silica Glass Fiber Laser Urs Pedrazza 1,2, Valerio Romano 2, Willy Lüthy 2, Christian Ban 1, Julien Sauvet 1, Florian Dürr 1, Hans G. Limberger 1, René P. Salathé 1, Thomas Feurer 2 1 Laboratoire d'optique appliquée, Ecole polytechnique fédérale de Lausanne, Switzerland 2 Institute of Applied Physics, University of Bern, Switzerland

Outline Yb-doped Al-codoped Sol-Sel Silica Glass Fiber Laser Motivation Production Optical Characterization Mechanical Characterization

Ytterbium-doped Aluminum-codoped Sol-Sel Silica Glass Fiber Laser Motivation Sol-Gel Technique Ytterbium Production Optical Characterization Mechanical Characterization

Sol-Gel Technique Flexibility for photonic research purposes... Flexibility of the products (thin films, powders, bulk) Flexibility of dopant content any water or ethanol soluble dopant can be dissolved homogeneously Flexibility of covering any shape by wetting the surfaces multi-core fibers, microstructures fibers (photonic crystals) Flexibility of choosing processing temperatures (200 C 2000 C) Very cost-effective Starting summer 2002 building to tower Ytterbium fiber laser

Ytterbium Yb ¾ High quantum efficiency No cross-relaxation No excited state absorption No up-conversion ¾ ¾ ¾ Absorption fits InGaAs diodes Broad emission band - short pulses Tunability (re-absorption) Rare-Earth-Doped Fiber Lasers and Amplifiers, M.J.F. Digonnet, Editor (Marcel Dekker Inc., New York 2001)

Ytterbium-doped Aluminum-codoped Sol-Sel Silica Glass Fiber Laser Motivation Production Sol-Gel Route Reduction of OH - -Group Content Optical Characterization Mechanical Characterization

Production by the Sol-Gel Route Wet chemistry process hydrolysis and polycondensation H 3 C CH 3 Si-OR + H 2 O Si-OH + ROH Si-OH + HO-Si Si-O-Si + H 2 O O O Si O O H 3 C CH 3 Wetting of surface, evaporation xerogel Thermal post-treatment (densification, reduction of OH - -groups)

Reduction of OH - - Group Content He, O 2 Oven Tube Collapsing Drawing Lathe Yb 1 :Al 10 :(SiO 2 ) 89 High viscosity 2.7 µm each layer, total 3 layers Vitrification layer-by-layer 1800 C OH - 3600 2800 2000 Wavenumber Wellenzahl [cm [cm -1 ] -1 ] Transmission (bel. [%] Einh.) IR Spectra OH - Quartz (for comparison) Silica @ 950 C Silica @ 500 C Silica @ 250 C SiO 1200 400 B. Wilhelm, IAP

Ytterbium-doped Aluminum-codoped Sol-Sel Silica Glass Fiber Laser Motivation Production Optical Characterization Monomode-Fiber Laser Spectral Characteristics Laser Performance Mechanical Characterization

Monomode-Fiber Laser Difference index of refraction between core and cladding: 0.00345 Numerical aperture: 0.099 Diameter fiber 140 µm Diameter core 6.3 µm Lifetime 764 ± 4 µs (20 cm, 908 nm) Losses 0.53 dbm -1 @ 632.8 nm Losses < 0.1 dbm -1 @ laser wavelengths IT ultra low OH - 1.5 dbkm -1 (0.8 dbkm -1 ) IT high OH - 50-200 dbkm -1

Spectral Characteristics 1037 nm (20 cm) saturation - 1091 nm (65 cm)

Laser Performance 5 P out (mw) 4 3 2 1 2 nd band 2 nd line starting 1080 nm 1088 nm 65 cm long fiber 64 % slope eff. 0 46 48 50 52 54 56 P in (mw)

Ytterbium-doped Aluminum-codoped Sol-Sel Silica Glass Fiber Laser Motivation Production Optical Characterization Mechanical Characterization Tomographic Measurements

Tomographic measurements 3.0 core axial stress [kg/mm2] 2.5 2.0 1.5 1.0 0.5 0.0 Yb 1 at.-% Al 10 at.-% Ge 9 at.-% -0.5-100 -80-60 -40-20 0 20 40 60 80 100 radial position [um]

Thank you for your attention! Acknowledgements: Markus Pollnau, University of Twente, NL