Wood potential use of Acacia melanoxylon growing in pure or mixed stands with Pinus pinaster by the Portuguese forest industry

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Wood potential use of Acacia melanoxylon growing in pure or mixed stands with Pinus pinaster by the Portuguese forest industry Utilização potencial do lenho de Acacia melanoxylon a crescer em povoamentos puros ou mistos com Pinus pinaster pela indústria florestal portuguesa A. Santos A. Teixeira O. Anjos R. Simões L. Nunes J. Machado M. Tavares Estação Florestal Nacional Projecto AGRO 283 Medida 8 Universidade da Beira Interior Laboratório Nacional de Engenharia Civil Projecto AGR/42594/2001 Programa POCTI 3º Simpósio Ibero-Americano de Gestão e Economia Florestal / 11º Simpósio de Análise de Sistemas em Recursos Florestais Brasil, Ubatuba,, 18-22 September 2005

Objective Acacia potential analysis as a raw material source for Portuguese industry (solid wood and pulp and paper), using information from forest management, wood properties and fiber quality for paper. Wood growth of Pinus pinaster Eucalyptus globulus Acacia melanoxylon Mechanical Properties Pinus pinaster Acacia melanoxylon Papermaking evaluation Eucalyptus globulus Acacia melanoxylon

Acacia sampling (similar for pine in Macão; different for the others) North & Center Regions of Portugal (pré-selection) 22 sites Pure austrália or mixed dominants stands with P. pinaster Installation of diameter growth study - Edaphic and sylvicultural characteristics of sites. - Diametric range evaluation (selection of dbh classes); (Selection of 4 sites) 2 sites dune sandy soils 2 sites granite soils National Forest of Camarido MNC Forest Perimeter of Ovar - PFDO Forest Perimeter of Rebordões/Sta. Maria, Ponte de Lima PFRSM Forest Perimeter of Serra do Crasto, Viseu - PFC

Sampling (cont.) For the 4 sites acacia acacia (pré-selection) 200 trees - 10 trees per dbh classes of 10, 20, 30, 40, e 50 cm acacia pine pine acacia pine pine pine pine 5 trees 40 cm dbh class per site Base, 5, 15, 35, 65% total height and top 100 trees - 5 trees per dbh classes Papermaking evaluation discs Solid wood study logs Diameter growth study trees

Material and methods Wood growth (origin of dendrometric information ) (previous outlined) Acacia melanoxylon Center/north pine forest Pine forest of center of Country - Municipality of Mação Pinus pinaster Model GLOBULUS 2.1 (Tomé et al., 2001) Eucalyptus globulus Estação Florestal Nacional

Wood growth Results and discussion Mean values of dbh growth (maritime( pine main stand) from littoral to interior of Portugal Site Soil/ region t (years) dg (cm) ami dg (cm.year -1 ) cmi dg (cm.year -1 ) M. Nacional Valado Frades, Nazaré Sand littoral 22 12.8 0.58 0.50 Vila Velha de Ródão Sandstone center 29 22.9 0.79 0.85 Serra Lousã, Castanheira de Pêra Schist center 25 21.8 0.87 0.90 Serra S. Mamede, Portalegre Schist interior 24 17.5 0.73 1.05 Serra da Estrela, Covilhã Granite interior 30 20.7 0.69 0.65 t age; dg mean dbh; ami annual mean increment; cmi current mean increment. In: : Tavares et al., 2004. Estação Florestal Nacional

Results and discussion (cont.) Wood growth Mean values of dbh growth (maritime( pine main stand) in Municipality of Mação ão,, center of Portugal Cl. dbh t (years) start of study Study duration (years) t (years) final study dg(cm) initial dg (cm) final ami dg (cm.year -1 ) cmi dg (cm.year -1 ) 5 22.4 1.9 24.3 5.6 6.3 0.26 0.34 10 24.4 1.9 26.3 10.2 10.5 0.40 0.17 15 30.6 1.9 32.5 15.0 16.0 0.49 0.49 20 30.6 1.9 32.5 19.8 20.8 0.64 0.49 25 32.6 1.9 34.5 25.5 26.6 0.77 0.61 30 32.6 1.9 34.5 29.5 30.6 0.89 0.56 Cl.dbh dbh class; t age; dg mean dbh; ami annual mean increment; cmi current mean increment. Estação Florestal Nacional

Results and discussion (cont.) Wood growth Estimated values for E. globulus in Portugal by Model GLOGULUS 2.1 (Tom( Tomé et al.,, 2001) Region (N.ha -1 =1250, 4x2m) Mean SI III (m) N.ha -1 at 12 years old dg (cm) ami dg (cm.ano -1 ) G (m 2.ha -1 ) ami G (m 2.ha -1.ano - 1 ) ami V (m 3.ha -1.ano -1 ) N / C Littoral 22, 20, 19, 14 1090 11.6 0.96 18.78 1.57 13.73 N/C Interior 17. 16 1061 10.7 0.89 15.24 1.27 9.54 S Littoral 18 1093 11.2 0.93 17.35 1.45 11.87 S Interior 15 850 10.1 0.84 10.97 0.91 6.20 N/ha stand density; ami annual mean increment in dg (mean dbh), in G (basal area per hectare) and in V (total volume ) Estação Florestal Nacional

Wood growth Results and discussion (cont.) Mean values of dbh growth of acacia in sands and granites in Portugal Site dbh class t estimated at the beginning of study (years) duration of study (years) t estimate d at the end of study (years) dg (cm) initial dg (cm) final ami dg cm.ano -1 cmi dg cm.ano -1 Mean values for North Region 10 20 30 40 11.3 22.6 33.9 45.3 2.6 2.6 2.6 2.6 13.9 25.2 36.5 47.9 10.6 21.3 29.1 41.0 11.5 22.4 30.5 42.5 0.83 0.89 0.83 0.89 0.36 0.44 0.52 0.60 50 56.6 2.6 59.2 49.9 51.4 0.87 0.56 t age; dg mean dbh; ami annual mean increment; cmi current mean increment. Estação Florestal Nacional

Material and methods Mechanical properties Mechanical experiments were done at 3 levels (15, 35 and 65% of stem total high). From each level were collected 3 cores from 3 different positions on stem cross section, defined by the relative distance to pith (10, 50 and 90% of radius length). Mechanical experiments Mechanical experiment Standard Cores size (width x thickness x length) (mm) Number of cores Static bending (3 points) ISO3133 20x20x340 223 Modulus of elasticity in bending ISO3133 20x20x340 198 Compression parallel to the fibers ISO3787 20x20x60 254 Tension perpendicular to the fibers ISO3346 20x20x60 246 Laboratório Nacional de Engenharia Civil

Results and discussion Mechanical properties Mean physical-mechanical properties of defects clean wood of maritime pine and d acacia-austr austrália Species/ origin Maritime pine / Different regions a) Maritime pine / Leiria National Forest a) Maritime pine / Leiria National Forest b) Acacia/ Different regions c) Acacia/ Different regions d) Average density (kg.m -3 ) 530 600 630 650 614 Average bending strength (N.mm -2 ) 9800 a) Mateus (1961) b) Machado e Cruz (2005) c) Preliminary data from project Upgrading of Portuguese wattle wood. Potential uses d) Tavares et al. (1999) - 96 130 146 142 Average modulus of elasticity (N.mm -2 ) - 13500 10500 14200 Average axial compression strength (N.mm -2 ) 46 52 47 61 - Laboratório Nacional de Engenharia Civil

Results and discussion (cont.) Mechanical properties Variation (%) 20 10 0 DP10 DP50 DP90 Variation (%) 16 12 8 4 65% 35% 5% -10 5% 35% 65% Stem high 0 DP10 DP50 DP90 Distance from pith Variation (in median) vertical (referring to 5% stem total high) and horizontal (referring to distance to pith of 10% of radius) of density in the tree. Laboratório Nacional de Engenharia Civil

Material and methods Papermaking evaluation White liquor Black liquor Wood chips (Acacia melanoxylon Eucalyptus globulus) Screening Screened chips Cooking Cooked chips 6 + 2 samples Effective alkali NaOH (%) Sulfidity index (%) Liquor/wood ratio Time to temperature (min.) Time at temperature (min.) Temperature (ºC) Acacia melanoxylon 19.6-21.3 30 4:1 90 80-90 160 Eucalyptus globulus 16.2-18.1 25 4:1 90 70-90 158-160

Material and methods (cont.) Papermaking evaluation Cooked chips Disintegrated and washed Unbleached kraft pulps Rejects Bleaching (ECF) Refining (0, 500, 2500 e 4500 revolutions) Morphological properties Paper handsheets Papermaking evaluation

Material and methods Papermaking evaluation White liquor Black liquor Wood chips (Acacia melanoxylon Eucalyptus globulus) Screening Screened chips Cooking Cooked chips 6 + 2 samples Effective alkali NaOH (%) Acacia melanoxylon 19.6-21.3 Eucalyptus globulus 16.2 18.1 Disintegrated and washed Sulfidity index (%) Liquor/wood ratio 30 4:1 25 4:1 Unbleached kraft pulps Rejects Time to temperature (min.) Time at temperature (min.) 90 80-90 90 70-90 Bleaching (ECF) Temperature (ºC) 160 158-160 Refining (0, 500, 2500 e 4500 revolutions) Morphological properties Paper handsheets Papermaking evaluation

Results and discussion Papermaking evaluation Cooking results Pulp yield (%) Rejects (%) Effective alkali consumption (as NaOH) (%) Kappa number Pulp viscosity - unbleached (cm 3 /g) Pulp viscosity - bleached (cm 3 /g) A. melanoxylon (n=6) 52.3 ± 3.6 1.1 ± 0.6 17.0 ± 1.1 15.1 ± 1.3 882 ± 127 783 ± 71 E. globulus (n=2) 52.5 ± 3.3 1.3 ± 0.6 14.8 ± 1.8 14.4 ± 3.7 1002 ± 144 897 ± 136

R.D. Morphological properties Papermaking evaluation Acacia melanoxylon Eucalyptus globulus Refining (revolutions) Fiber width (µm) Length weighted in length (mm) Coarseness (mg/m) 0 18.6 0.85 0.055 500 18.6 0.86 0.055 2500 18.6 0.85 0.055 4500 18.8 0.85 0.056 0 16.5 0.73 0.091 500 16.4 0.73 0.088 2500 16.7 0.73 0.088 4500 16.6 0.71 0.090 A. melanoxylon versus E. globulus Fibers with higher width Fibers with higher length Lower coarseness

Papermaking evaluation R.D. Suspension - properties 90 Acacia melanoxylon Eucalyptus globulus 70 0,95 SRº 50 0,85 30 10 0 1000 2000 3000 4000 5000 Number of revolutions - PFI Density (g/cm 3 ) 0,75 0,65 Acacia melanoxylon Eucalyptus globulus 0,55 11 21 31 41 51 61 71 81 SRº R.D Structural properties

R.D Mechanical properties Papermaking evaluation Tear index (mn.m 2 /g) 14,0 12,0 10,0 8,0 6,0 4,0 2,0 Acacia melanoxylon Eucalyptus globulus 40,0 60,0 80,0 100,0 Tensile index (N.m/g) Light scattering coefficient (m 2 /kg) 49,0 39,0 29,0 19,0 Acacia melanoxylon Eucalyptus globulus 0,58 0,65 0,72 0,79 0,86 Density (g/cm 3 ) R.D. Optical properties

Conclusions Growth pattern of acacia is higher (ami dg=0.89 cm.year -1 ) then m. pine (0.71) and just a little lower then blue gum (0.90). It can be an alternative wood producer. Mechanical properties (determined in small cores without defects) allows to qualify the wood of austrália as a source of wood for sawing and construction national industry. Concerning resistance and stiffness, must be noticed a considerable variability intra and inter trees. Acacia austrália versus Eucalypt - Bigger smoothness of papers. - Less resistance to tear and tensile. - Bigger light scattering coefficient. Acacia fiber presents real potential to be combined with eucalypt in writing & printing paper.

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