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This document is downloaded from the Digital Open Access Repository of VTT Title Foam forming - potential production technology for building materials Author(s) Jetsu, Petri; Pöhler, Tiina Citation 12th Global Insulation Conference and Exhibition 2017, 25-26 September 2016, Krakow, Poland Date 2017 Rights This presentation may be downloaded for personal use only. VTT http://www.vtt.fi P.O. box 1000 FI-02044 VTT Finland By using VTT Digital Open Access Repository you are bound by the following Terms & Conditions. I have read and I understand the following statement: This document is protected by copyright and other intellectual property rights, and duplication or sale of all or part of any of this document is not permitted, except duplication for research use or educational purposes in electronic or print form. You must obtain permission for any other use. Electronic or print copies may not be offered for sale.

Foam forming - potential production technology for building materials Petri Jetsu, Tiina Pöhler VTT Technical Research Centre of Finland Ltd

Outline Why foam technology? Introduction to foam forming technology Foam formed thermal insulation materials based on wood fibres - the effect of fibre type Benchmarking of wood based foam formed building materials against commercial materials Future actions

Why foam technology? Foam forming is an enabling technology with six major benefits 1. Material uniformity is excellent high quality and raw material savings 2. Possibility to produce highly porous as well as dense structures - wide product window with the one technology 3. Possibility to utilize different kinds of raw materials from nanofibers to several centimeter long fibres as well as high and low density particles 4. Possibility to produce layered products with excellent layer purity 5. Technology can be a resource efficient and cost competitive compared to many other manufacturing methods 6. Sustainable products can be produced by this technology

History Background Foam forming technology has been studied already in 1970 s, but implemented in some extent only in nonwoven and tissue industry at the moment. Foam forming research at VTT First laboratory scale projects started in the mid of 2000 Technology has up-scaled to the pilot scale in 2012 Wide variety of raw materials have be used; wood and natural fibres, residues from wood industry (bark, saw dust etc.), man-made fibres, polymer powders Wide variety of applications like printing papers, packaging boards, hygienic nonwovens, filters, thermal insulation materials, acoustic panels, building boards, cushioning materials, fibre/plastic composites etc. has been studied. New pilot line will be started during autumn 2017

Basics of foam forming Foam is generated by intensive mixing of water and foaming agent Typical air content is 40 70 % Typical bubble diameter is ~100 µm Foam stability can be controlled Fibres and other raw materials are mixed with aqueous foam Material is located in bubble pockets preventing flocculation, which leads to uniform material distribution

Main process phases and features of foam forming Generation of aqueous foam and mixing of raw materials in the foam: In tank or on-line in tube Web forming: Spreading the foam on a wire through a nozzle and removing wet foam with vacuums, typical dry solid content of web is 10-25 % after this phase Wet pressing: Increase dry solid content of web to 40-50 % (Not used if aiming to highly porous structures) Drying: With contact or non-contact techniques Process can be batch or continuous process

Pilot scale foam forming environment at VTT Technical specifications: Design speed 2000 m/min Sampling speed <1000 m/min Roll width 250 mm Several forming geometry options Multilayer forming possibilities Two foam generation options (tank mixing & tube generation) Single nip press section Off-line dryer For paper-like products

Foam formed thermal insulation materials based on wood fibres the effect of fibre type

Preparation of foam formed materials in laboratory scale Phases: Fibre foam generation: Mixing of pulp suspension and foaming agent Sheet forming: Fibre foam is poured into a mould and drained by gravity Drying in the oven Rewetting to dsc. 50 % and pressing to targeted thicknesses Drying in the oven

Fiber dimensions Fibre length, mm Fibre width, µm SW 2.00 29 HW 0.87 21 TMP 1.36 33 Glass 3-10 8-10 PLA 12 10-12 Optical microscope images SW: Chemical softwood pulp HW: Chemical hardwood pulp TMP: Thermomechanical pulp Glass: Glass fibres PLA: Polylactid acid fibres SW, HW, TMP average fibre dimensions by Fibermaster analyzer Glass and PLA fibre dimensions estimated from optical microscope images SW Glass PLA This result is part of WOTIM project funded by the WoodWisdom-Net Research Programme under the Seventh Framework Programme (FP7)

Thermal conductivity SW: Chemical softwood pulp ΔT +20 C HW: Chemical hardwood pulp TMP: Thermomechanical pulp EN 12667 This result is part of WOTIM project funded by the WoodWisdom-Net Research Programme under the Seventh Framework Programme (FP7)

Air flow resistance SW: Chemical softwood pulp HW: Chemical hardwood pulp TMP: Thermomechanical pulp ISO 9053 This result is part of WOTIM project funded by the WoodWisdom-Net Research Programme under the Seventh Framework Programme (FP7)

Compression strength SW: Chemical softwood pulp 10 % compression HW: Chemical hardwood pulp TMP: Thermomechanical pulp EN 826 This result is part of WOTIM project funded by the WoodWisdom-Net Research Programme under the Seventh Framework Programme (FP7)

Thermal conductivity of material mixtures SW: Chemical softwood pulp Glass: Glass fibres PLA: Polylactid acid fibres Man-made fibre proportion 20 % This result is part of WOTIM project funded by the WoodWisdom-Net Research Programme under the Seventh Framework Programme (FP7)

Benchmarking of wood based foam formed building materials against commercial materials

Thermal insulation materials thermal conductivity This result is part of WOTIM project funded by the WoodWisdom-Net Research Programme under the Seventh Framework Programme (FP7) EN 12667

Acoustic panels - sound absorption Material Thickness Density Grammage Flow resistivity Commercial glass wool Foam formed pine pulp mm kg/m 3 g/m 2 Ns/m 4 30 53 1585 27300 30 42 1260 23600 Glass wool product Foam formed pine pulp ISO 10534-2 This result is part of FOAMSOUD project funded by the Finnish Funding Agency for Innovation (TEKES)

Building boards bending strength NBSK: Northern bleached softwood kraft Internal wall element Surfaces: Foam formed boards Middle layer: Foam formed thermal insulation material Foam formed fibre board This result is part of OSIRYS project funded under the Seventh Framework Programme (FP7) EN 12089

Status and future actions

Status and next steps Status Technical performance of foam formed building materials is proved in laboratory scale However there is still a need for the development/optimization work that all required properties can be achieved (varying with applications) Preliminary cost evaluations are promising in many cases Next steps Up-scale the manufacturing of building materials in pilot scale technical proof of concept Evaluate the cost and resource effectiveness of manufacturing based on pilot data Material production to demo buildings

New pilot line at VTT Layout and technical specifications Design speed 1000 m/min Sampling speed < 200 m/min Sample width 600 mm (rolls or sheets) Two forming geometry options Multilayer forming possibilities Foam generation in tank For thick products (thickness 1 20 mm)

Foam forming - potential production technology for building materials Petri Jetsu, Tiina Pöhler VTT Technical Research Centre of Finland Ltd