Measurement of penetration and cycle time of jets from an industrial fluid coking spray nozzle

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Engineering Conferences International ECI Digital Archives Fluidization XV Proceedings 5-24-2016 Measurement of penetration and cycle time of jets from an industrial fluid coking spray nozzle Francisco Sanchez Careaga Institute for Chemicals and Fuels from Alternative Resources (ICFAR), Western University, Canada Cedric Briens Institute for Chemicals and Fuels from Alternative Resources (ICFAR), Western University, Canada, cbriens@uwo.ca Franco Berruti Institute for Chemicals and Fuels from Alternative Resources (ICFAR), Western University, Canada Follow this and additional works at: http://dc.engconfintl.org/fluidization_xv Part of the Chemical Engineering Commons Recommended Citation Francisco Sanchez Careaga, Cedric Briens, and Franco Berruti, "Measurement of penetration and cycle time of jets from an industrial fluid coking spray nozzle" in "Fluidization XV", Jamal Chaouki, Ecole Polytechnique de Montreal, Canada Franco Berruti, Wewstern University, Canada Xiaotao Bi, UBC, Canada Ray Cocco, PSRI Inc. USA Eds, ECI Symposium Series, (2016). http://dc.engconfintl.org/fluidization_xv/77 This Abstract and Presentation is brought to you for free and open access by the Proceedings at ECI Digital Archives. It has been accepted for inclusion in Fluidization XV by an authorized administrator of ECI Digital Archives. For more information, please contact franco@bepress.com.

Measurement of penetration and cycle time of jets from an industrial Fluid Coking spray nozzle Francisco Sanchez, Cedric Briens, and Franco Berruti May 24 th, 2016

Feed Liquid Background Agglomerate Impact Lower Liquid Yield Fouling of Internals Mass and Heat Transfer Limitations Operating Problems (Bogging) Feed Nozzle Jet Cavity Jet Penetration Atomization Gas Fluidization Gas 2

Feed Liquid Background Feed Nozzle Atomization Gas 3

Background From Ben Li s work bed hydrodynamics in region where agglomerates are released is important. In Fluid Cokers large radial and vertical variations in bed hydrodynamics Changes in jet penetration can improve the liquid distribution in the fluidized bed: Less agglomerate formation More free moisture 4

Objectives Experimentally measure the Jet penetration of an industrial size spray nozzle. Compare it to values predicted from literature model. 5

Equipment Pie Shape 6

Equipment Industrial Size TEB Fluidization bed conditions: Injected Water: 18.28 liters. Mass of fluidized sand: 7800 kg. Conditions Minimum Maximum Nozzles Atomization Gas (N 2 ) Blow Tank (H 2 O) Liquid Flow (H 2 O) 3.45 MPa 4.83 MPa 1.75 MPa 2.07 MPa 178 LPM 236 LPM Base et al. (1999), Patent Number: 6,003,789 GLR 1.6 % 3.0 % 7

Equipment Industrial Size TEB Nozzles Open Air Blast 8

Jet Penetration Measurement Challenges Video cameras: Probes destroyed by bubbles/jet Thermocouples: Bent by jet and response times are too slow. Triboprobes above jet: Thick rods: resisted jet/bubbles But: detected changes in moisture more than voidage 9

Issues: Jet Penetration Measurement Challenges Probes bent by jet or bubbles (e.g. camera probes in photograph) Can we use this in our favor? 2 methods: 1. Bendable tubes in jet path 2. Vibration of thick, unbendable rods in jet path 10

Jet Penetration Bendable tubes deformation Bed fluidization velocity (0.08 m/s) Avoid bubbles bending the rods Nozzle flowrates 178 LPM, GLR = 2.0 % Predicted by Ariyapadi s correlation = 1.99 m 11

Jet Penetration Bendable tubes deformation 12

Jet Penetration Vibrating Rods 13

Vibrating Rods Movement in X and Y Coordinates From Video Analysis Y Coordinate X Coordinate 14

Vibrating Rods Mean Sum of Errors 15

Vibrating Rods Results 16

Conclusion At low liquid flowrates, measured jet penetrations agree with predictions from Ariyapadi s correlation. At higher liquid flowrates, measured jet penetrations are 10% lower than predictions from Ariyapadi s correlation. 17

Acknowledgements 18

Thank You! 19

Jet Penetration Ariyapadi s Correlation g = Gravity (m/s 2 ) ρ p = Density of the particles (kg/m 3 ) ρ g = Density of the gas (kg/m 3 ) ρ L = Density of the liquid (kg/m 3 ) GL = Superficial liquid mas velocity (kg/m 2 s) GLR = Gas to liquid mass ratio S = Mean slip velocity ratio ε' = Mean void fraction at slip conditions d = Nozzle tip diameter (m) C g = Nozzle geometry parameter Ariyapadi s model with empirical factor C g for a scale-down nozzle. (2004) 20

Jet Penetration Ariyapadi s Correlation Although locally, there is no slip between the gas and liquid phases, there is an apparent slip factor S in the nozzle throat because: There is a radial velocity profile There is a radial distribution of the gas holdup Nozzle orifice U mix2 ε mix2 U mix1 ε mix1 21

Jet Penetration Ariyapadi s Correlation 22