Project introduction. Oswin Kerkhof, VSL. +31 (0)

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Metrology for LNG Project introduction Oswin Kerkhof, VSL okerkhof@vsl.nl, +31 (0)15 2691509

Metrology for LNG The project - background and motivation LNG strongly growing business worldwide LNG market changes: more commercial, increased liquidity, short vs long term, More focus on transparency and accuracy New application areas/new metering challenges: off-shore LNG, small & mid-scale LNG Sound metrological framework not yet fully in place 1% uncertainty = 440 M per year in 2010 1% uncertainty = 900 M per year in 2015

Metrology for LNG Overall objective To contribute to a significant reduction of uncertainty (by at least a factor two) in the determination of transferred energy in LNG custody transfer processes. Contribute t to: Improving existing methods Validating new methods Creation of new calibration systems with improved uncertainty International technical and legal standards and guidelines

LNG custody transfer Measurement of energy Volume x Density x Gross Calorific Value Source: GIGGNL Custody transfer handbook, 3 rd edition

Project aims and objectives Volume Mass Density Gross Calorific Value Developing traceability for LNG (mass and volume) flow meters (WP1) Testing and evaluating LNG quantity metering systems (WP2) Improving LNG composition measurement systems (WP3) Reducing uncertainties in LNG density calculations (WP4) Improving LNG composition measurement systems (WP3) Reducing uncertainties in calorific value calculations (WP4) WP5 Measurement Guidelines Written Standards Legal Metrology Energy

Workpackage descriptions WP1 Developing traceability for LNG flow meters 1. Developing of a primary LNG mass flow standard (25 m 3 /h, target uncertainty 0,05% 05% ) 2. Developing Small/Mid-scale flow standard /1 st stage up-scaling standard (200 m 3 /h, target uncertainty 0,07%) 3. Comparing water, LIN and LNG calibrations 4. Defining economic calibration concept 5. Feasibility study Cryogenic Laser Doppler Velocity system

Workpackage descriptions WP2 Testing and evaluating LNG quantity metering systems 1. Evaluating uncertainty of shiptank based measurement systems 2. Field testing: ti comparing static ti (tank level l and weighing) and dynamic (flow metering) quantity metering systems 3. Studying (simulation and experiments) effect of cryogenic media on flow metering systems 4. Studying (simulation and experiments) of installation effects on LNG flow meters.

Workpackage descriptions WP3 Testing and evaluating LNG composition measurement systems 1. Collecting information on sampling methods and uncertainties 2. Collecting data on sample retention ti during LNG loading and unloading 3. Evaluating the performance of the most suitable sampling technologies based on the provided data 4. Providing recommendations to ISO TC28/SC5 5. Comparing alternative composition method: Raman spectroscopy

Workpackage descriptions WP 4 Improving LNG density and calorific value calculations 1. Development of a primary LNG densitometer 2. Produce experimental reference data with LNG densitometer for at least four LNG-like mixtures 3. Develop and produce experimental reference data with LNG pycnometer system 4. Validating and comparing equations of state used for density calculation 5. Calculation l of LNG calorific value at different reference conditions 6. Assessing the impact of temperature, t composition and density gradients in tanks on total measurement uncertainty range where data with at least ten times higher uncertainty are available

Workpackage descriptions WP5 Contributing to measurement guidelines, written standards and legal metrology 1. Providing input to ISO and CEN standardization (ISO TC28/SC5, ISO10976, ISO8943-2007, ISO TC67/WG10, ISO TC193, ISO 6976, CEN TC282, EN 12838-2000) 2. Providing information/guidelines to EURAMET-TC-flow 3. Providing input to legal metrology (MID / OIML) 4. Providing input to GIIGNL (custody transfer handbook) and LNG industry

Metrology for LNG Project duration: May 2010 May 2013 Funding: 3 Million Euro, 46% EU/EMRP, 54% Metrology organisations Co-funding from GERG project on LNG density Additional investment budget from NMI s Additional in-kind contribution from industry Project partners: VSL (coordinator), SP, TUV NEL, FORCE, JUSTERVESENET, CMI, CESAME, INRiM, PTB ENAGAS, ELENGY, E.ON RUHRGAS

Metrology for LNG advisory group Members Krohne altometer (chair) Krohne Ltd Cameron Caldon Elster Instromet Emerson Process Management Flow Gasunie transport services National Grid Grain LNG Rasgas Shell Global Solutions International Kongsberg Maritime Petronas Enagas Elengy E.On Ruhrgas Honeywell Enraf Tokyo Gas Gate Terminal Valtronics Endress + Hauser GdFSuez

Project website WWW.LNGMETROLOGY.INFO Detailed project information Objectives, tasks, activities Progress reports, project results Project news Photo gallery Discussion forum Publications and articles Project presentations and articles Other LNG measurement articles Relevant standards and guidelines