University of Nevada Reno

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University of Nevada Reno Presented by: Elie Y. Hajj, Ph.D. Manitoba PTH 8 RAP Field Sections Update on Laboratory Test Results Recycled Asphalt Pavement Expert Task Group Oklahoma City, Oklahoma October 26, 2010

Manitoba RAP Sections (PTH8) Provincial Highway 8 between Gimli & Hnausa, Manitoba, Canada. Total Project length: 17 miles Comparative pavement site: 6 miles Construction date: Sept. 2009 RAP: ½ NMAS Heaviest Traffic lane About 3 km About 3 km About 3 km 1-3 km 2 HMA/50% RAP 4 th lift HMA/50% RAP 4 th lift with grade change HMA/15% RAP 4 th lift HMA/No RAP 4 th lift 2 HMA/50% RAP 3 rd lift HMA/50% RAP 3 rd lift with grade change HMA/15% RAP 3 rd lift HMA/No RAP 3 rd lift New HMA/50% RAP 2 nd lift New HMA/50% RAP 1 st lift

Manitoba RAP Sections (PTH8) Mixtures Types Mixture Binder Field Mix Lab Compacted Lab Mix Lab Compacted 0% RAP no grade change Pen 150 200 F 0% 150 L 0% 150 15% RAP no grade change Pen 150 200 F 15% 150 L 15% 150 50% RAP no grade change Pen 150 200 F 50% 150 L 50% 150 50% RAP grade change Pen 200 300 F 50% 200 L 50% 200

Manitoba RAP Sections (PTH8) Mixtures Types Mixture Mix Lift Optimum Binder Content RAP Design Binder Content by Ignition i Oven Binder %* F 0% 150 Bit B 4 5.2% 5.0% F 15% 150 Bit B 4 5.2% 5.1% 13.8% F 50% 150 Bit B 4 5.0% 4.8% 49.0% F 50% 200 Bit B 4 5.0% 4.8% 49.0% L 0% 150 Bit B 4 5.2% L 15% 150 Bit B 4 5.2% 13.6% L 50% 150 Bit B 4 5.0% 47.0% L 50% 200 Bit B 4 5.0% 47.0% * Based on RAP binder content of 4.7% (from Ignition Oven)

Manitoba RAP Sections (PTH8) Test Experiment Matrix Binders Determine PG grading for: virgin binders: Pen 150-200, Pen 200-300 recovered binders (85% Toluene + 15% Ethanol): F-0%-150, F-15%-150, F-50%-150, F-50%-200 L-0%-150, L-15%-150, L-50%-150, L-50%-200 RAP-100%

Manitoba RAP Sections (PTH8) Test Experiment Matrix Binders Evaluate the following: Blending chart process RAP mortar procedure (UWM) Predicted binder properties from Hirsh model Predicted binder properties from Huet-Sayegh modified model (2S2P1D model) Predicted binder properties from Lytton et al. model

Manitoba RAP Sections (PTH8) Test Experiment Matrix Mixtures Property F 0% 15 50 50 F 15% 1 50 F 50% 1 F 50% 20 00 L 0% 15 50 L 15% 15 50 L 50% 15 50 L 50% 20 00 Resistance to Moisture Damage TS vs. F T cycles: 0, 1 and 3 F T TSR at 1 and 3 F T X X X X X X X X X X X X X X X X E* vs. F T cycles: 0, 1 and 3 F T X X X X X X X X Resistance to Thermal Cracking TSRST: 0 and 3 F T X X X X X X X X Resistance to Fatigue Cracking X X X X X X X X

Extraction/Recovery Using Centrifuge Superpave PG Grades PG Temp perature ( C) 84.0 72.0 60.0 48.0 36.0 24.0 12.0 0.0 12.0 24.0 36.0 48.0 0 76.5 69.1 61.0 62.6 65.1 67.3 59.0 59.4 63.1 54.1 58.6 30.9 24.3 14.7 12.2 15.8 18.5 22.7 23.0 14.9 17.8 21.6 14.7 21.2 32.5 34.4 31.6 29.5 25.1 22.3 32.6 30.5 26.6 Asphalt Binder Type High PG Intermediate PG Low PG

Extraction/Recovery Using Centrifuge Superpave PG Grades Virgin Extr./ Rec. using centrifuge Mix PG Grade PEN150 200 58 28 PEN200 300 52 34 F 0% 150 58 28 F 15% 150 58 28 F 50% 150 64 16 F 50% 200 64 22 L 0% 150 58 28 L 15% 150 58 28 L 50% 150 64 22 L 50% 200 58 22 RAP binder (AASHTO M320) 76 10

Asphalt Binder Blending Chart High Critical Temperature

Asphalt Binder Blending Chart Intermediate Critical Temperature

Asphalt Binder Blending Chart Low Critical Temperature

RAP Mortar Procedure (UWM) Flow Chart of Material Preparation and Testing RAP passing Mix with sieve #50 & original binder retained on sieve #100 Mix with RTFO (R100) binder Ignition oven Calculate R100 binder content Fresh SRAP mortar RTFO SRAP mortar PAV aging PAV SRAP mortar PAV RRAP mortar DSR (High Temperature) DSR (Inter. Temperature) BBR (Low Temperature) Retained aggregates Mix with RTFO binder Mix with original binder RTFO RRAP mortar Fresh RRAP mortar DSR (High Temperature)

RAP Mortar Procedure (UWM) Typical Results PG Gr rade Temperat ture ( C) 70 60 50 40 30 20 10 0 10 20 30 40 Percent RAP Binder as Percent of Total Binder 58.7 16.7 30.9 0 10 20 30 40 50 Low Temperature High Temperature % RAP Binder Intermediate Temperature Low Temperature (Extrapolated) 70 60 50 40 30 20 10 0 10 20 30 40 PG Gr rade Temperat ture ( C)

Predictions Using Hirsh Model Use semi-empirical empirical model proposed by Christensen et al. (2003) to estimate shear dynamic modulus. Measured E*laboratory data used. Minimize Error between Hirsch model prediction and real data by varying binder stiffness. Compare estimated stiffness with measured stiffness. Determine e binder critical ca temperature. e

Summary of PG Grades Preliminary Results for Pen 150-200 % RAP Virgin Binder Mix Rec. Critical T High Critical T Intermediate Critical T Low Blend Mortar Blend Mortar Blend Mortar TSRST Hirsh Rec. Hirsh Rec. Hirsh Chart Testing Chart Testing Chart Testing 59.0 14.7 32.5 0 15 50 F 61.0 IP 15.8 IP 31.6 32.8 L 58.6 57.5 14.9 16.0 32.6 33.0 F 62.6 63.6 6 IP 18.5 18.1 IP 29.5 29.19 30.8 58.7 16.7 30.9 L 59.4 61.3 57.6 17.8 18.3 18.6 30.5 29.3 30.9 F 69.1 68.8 IP 24.3 23.4 IP 21.2 23.2 29.1 61.0 21.8 28.4 L 67.3 67.6 62.5 23.0 23.7 24.0 22.3 23.7 27.2

Summary of PG Grades (cont d) Preliminary Results for Pen 200-300 % RAP Virgin Binder Mix Rec. Critical T High Critical T Intermediate Critical T Low Blend Mortar Blend Mortar Blend Mortar TSRST Hirsh Rec. Hirsh Rec. Hirsh Chart Testing Chart Testing Chart Testing 54.1 12.2 34.4 0* 50 F 61.0 IP 15.8 IP 31.6 32.8 L 58.6 57.5 14.9 16.0 32.6 33.0 F 65.1 65.3 IP 22.9 21.6 IP 25.1 24.66 32.1 57.0 18.8 31.4 L 63.1 63.2 64.1 21.6 21.8 20.1 26.6 24.5 34.4 *0% RAP manufactured with Pen150 200

Inverse Problem for Low Temp Characterization A. C. Falchetto, M. O. Marasteanu & H. Di Benedetto Huet Model (Huet 1963)

Inverse Problem for Low Temp Characterization A. C. Falchetto, M. O. Marasteanu & H. Di Benedetto Calculated S(t) binder from measured S(t) mixture Authors showed very good predictions for the binder stiffness from the mixture stiffness.

Huet-Sayegh Modified 2S2P1D Model (Olard and Di Benedetto, 2003) Generalization of Huet-Sayegh model i : complex number, ω: 2π*frequency k, h : exponents such as 0<k<h<1, δ : dimensionless constant E 0 the static modulus when ω 0, E the glassy modulus when ω, η : Newtonian viscosity, η=(e E 0 ).β.τ ; when ω 0, then E*(iωτ) ~ E0+ iω.(e -E0).β.τ; β is dimensionless. τ : characteristic time varying with temperature

Huet-Sayegh Modified 2S2P1D Model (Olard and Di Benedetto, 2003) Relationship between the characteristic time of the mixture and the characteristic time of the corresponding binder at the reference temperature: α: Regression coefficient depending on mixture & aging

Huet-Sayegh Modified 2S2P1D Model (Olard and Di Benedetto, 2003) Relationship between mix and binder complex moduli Relationship between mix and binder complex moduli was proposed

Predictions Using Huet-Sayegh Modified Approach Forward Calculation Measure complex modulus for the various mixtures & their associated recovered asphalt binders. Fit Huet-Sayegh Modified (2S2P1D) model to measured E* data: Determine δ, h, k, β and τ 0 for binder and mix Examine the relationship between log(τmix) & log(τbinder)

Predictions Using Huet-Sayegh Modified Lab-Produced mixtures mix) Log10(τ 8.0E+00 6.0E+00 4.0E+00 2.0E+00 0.0E+00 2.0E+00 4.0E+00 6.0E+00 8.0E+00 y = 0.0981x 2 + 2.4446x + 9.4162 R² = 0.9982 1.2E+01 1.0E+01 8.0E+00 6.0E+00 4.0E+00 2.0E+00 0.0E+00 Log10(τ binder ) 0%RAP 150 50%RAP 150 100%RAP Poly. Fit Note: not the same parameters (δ, k, and h) were used for the mixes and binders

Predictions Using Huet-Sayegh Modified Promising results if relationship was found to be a unique relationship Continuing Effort: Refine the analysis for lab-produced mixtures Conduct the same analysis for field-produced mixtures Conduct the same analysis for other mixtures Evaluate the inverse calculation l

Mixtures Testing TS and TSR at multiple F-T cycles E* at multiple F-T cycles TSRST at multiple F-T cycles Fatigue testing

TS at 77 F and 0, 1 and 3 F-T Tens sile Strength at 77 F, psi 200 150 100 50 127 117 115 101 73 75 171 155 117 189 170 165 153 143 132 122 123 124 113 70 75 169 161 93 0 F 0% 150 F 15% 150 F 50% 150 F 50% 200 L 0% 150 L 15% 150 L 50% 150 L 50% 200 Mixture Type 0 F T 1 F T 3 F T

TSR at 77 F, 1 and 3 F-T 120 io at 77 F, % Strength Rati 80 40 86 63 91 90 59 68 100 74 86 86 53 53 81 66 95 55 Tensile 0 F 0% 150 F 15% 150 F 50% 150 F 50% 200 L 0% 150 L 15% 150 L 50% 150 L 50% 200 Mixture Type 1 F T 3 F T

Resistance to Moisture Damage E* Test Results at 77 F 700 677 10 Hz, ksi 600 500 487 546 534 478 487470 at 77 F and E* 400 300 200 406 397 335 314 280 250 248 225 222 215 306 276 241 335 335 295279 100 F 0% 150 F 15% 150 150 F 50% 150 F 50% 200 L 0% 150 L 15% 150 150 L 50% 150 L 50% 200 Mixture Type 0 F T 1 F T 3 F T

Resistance to Moisture Damage E* Ratio at 77 F E* Rat tio at 77 F and 10 Hz, % 100 75 50 25 67 66 77 62 72 59 98 88 97 89 90 88 77 79 69 83 0 F 0% 150 F 15% 150 F 50% 150 F 50% 200 L 0% 150 L 15% 150 L 50% 150 L 50% 200 Mixture Type 1 F T 3 F T

Resistance to Thermal Cracking TSRST Test Results Fracture Temperature 0 F-T

References T. J. Hirsch, Modulus of elasticity of concrete affected by elastic moduli of cement paste matrix and aggregate. Journal of the American Concrete 5 Institute, Vol. 59(3), 1962, pp 427-4522. D. Christensen, T. Pellinen, R. F. Bonaquist, Hirsch model for estimating the modulus of asphalt concrete. Journal of Association of Asphalt 8 Paving Technologists, Vol. 72, 2003, pp 97-121. A. Zofka, M. O. Marasteanu, X. Li, T. Clyne,J. McGraw, Simple method to obtain asphalt binders low temperature properties from asphalt mixtures properties. Journal of the Association of Asphalt Paving Technologists, Vol. 74, 2005, pp255-282. F. Olard, H. Di Benedetto, General 2S2P1D model and relation between the linear viscoelastic behaviors of bituminous binders and mixes. RMPD, Vol. 4/2 Special Issue, 1 2003, pp185-224. H. Di Benedetto, F. Olard, C. Sauzéat, B. Delaporte, Linear viscoelastic behaviour of bituminous materials: from binders to mixes, RMPD, Vol. 5 Special Issue, 2004, pp163-202.

References B. Delaporte, H. Di Benedetto, P. Chaverot, G. Gauthier, Linear viscoelastic properties of bituminous materials: from binders to mastics. J. of the AAPT, Vol. 76, 2007, pp 455-494. A. C. Falchetto, M. O. Marasteanu, H. Di Benedetto, Analogical Based Approach to Forward and Inverse Problems for Asphalt Materials Characterization at Low Temperatures. Submitted for possible publication in the AAPT Journal, 2011. M. O. Marasteanu, Relating Low Temperature Mixture and Binder Properties Using Phenomenological and Analogical Models. Asphalt Binder ETG meeting, Madison, Wisconsin, September 2010....