OREGON Environmental Laboratory Accreditation Program ORELAP Fields of Accreditation

Transcription

1

2 MATRIX Reference Code Analyte Code Description Air Eurofins Calscience, Inc. ASTM D EPA RSK-175 (GC-FID) 3755 Carbon dioxide 3780 Carbon monoxide 1767 Helium 1772 Hydrogen 4926 Methane 1843 Nitrogen 3895 Oxygen 3755 Carbon dioxide 4747 Ethane 4752 Ethene 4926 Methane 5029 n-propane Reformed Gas by Gas Chromatography Methane, Ethane, and Ethene in water by Headspace GC/FID EPA TO-13A Polycyclic Aromatic Hydrocarbons in Ambient Air by GC/MS 5500 Acenaphthene 5505 Acenaphthylene 5555 Anthracene 5575 Benzo(a)anthracene 5580 Benzo(a)pyrene 5600 Benzo(k)fluoranthene 5855 Chrysene 5895 Dibenz(a,h) anthracene 6265 Fluoranthene 6270 Fluorene 6315 Indeno(1,2,3-cd) pyrene 5005 Naphthalene 6615 Phenanthrene 6665 Pyrene EPA TO-14A Volatile Organic Compounds with SUMMA canister and GC/MS ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethylene ,2,4-Trichlorobenzene 1 of 75

3 Air EPA TO-14A ,2,4-Trimethylbenzene ,2-Dibromoethane (EDB, Ethylene dibromide) ,2-Dichlorobenzene ,2-Dichloroethane (Ethylene dichloride) ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Butadiene ,3-Dichlorobenzene ,4-Dichlorobenzene 4375 Benzene 5635 Benzyl chloride 4395 Bromodichloromethane 4400 Bromoform 4455 Carbon tetrachloride 4475 Chlorobenzene 4485 Chloroethane (Ethyl chloride) 4505 Chloroform 4645 cis-1,2-dichloroethylene 4625 Dichlorodifluoromethane (Freon-12) 4765 Ethylbenzene 4835 Hexachlorobutadiene 4950 Methyl bromide (Bromomethane) 4975 Methylene chloride (Dichloromethane) 5100 Styrene 5115 Tetrachloroethylene (Perchloroethylene) 5140 Toluene 4700 trans-1,2-dichloroethylene 4685 trans-1,3-dichloropropylene 5170 Trichloroethene (Trichloroethylene) 5175 Trichlorofluoromethane (Fluorotrichloromethane, Freon 11) 5235 Vinyl chloride 5260 Xylene (total) EPA TO VOCs collected in Canisters by GC/MS ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethylene ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene 2 of 75

4 Air EPA TO ,2-Dichlorobenzene ,2-Dichloroethane (Ethylene dichloride) EPA TO-15 GC/MS SIM ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Butadiene ,3-Dichlorobenzene ,4-Dichlorobenzene ,4-Dioxane (1,4- Diethyleneoxide) Butanone (Methyl ethyl ketone, MEK) Methyl-2-pentanone (MIBK) 4315 Acetone 4375 Benzene 5635 Benzyl chloride 4395 Bromodichloromethane 4400 Bromoform 4450 Carbon disulfide 4455 Carbon tetrachloride 4475 Chlorobenzene 4485 Chloroethane (Ethyl chloride) 4505 Chloroform 4645 cis-1,2-dichloroethylene 4680 cis-1,3-dichloropropene 4625 Dichlorodifluoromethane (Freon-12) 4765 Ethylbenzene 4835 Hexachlorobutadiene 4950 Methyl bromide (Bromomethane) 4960 Methyl chloride (Chloromethane) 5000 Methyl tert-butyl ether (MTBE) 4975 Methylene chloride (Dichloromethane) 4855 n-hexane 5100 Styrene 5115 Tetrachloroethylene (Perchloroethylene) 5140 Toluene 4700 trans-1,2-dichloroethylene 4685 trans-1,3-dichloropropylene 5170 Trichloroethene (Trichloroethylene) 5175 Trichlorofluoromethane (Fluorotrichloromethane, Freon 11) 5225 Vinyl acetate 5235 Vinyl chloride 5260 Xylene (total) ,1,1,2-Tetrachloroethane VOCs collected in Canisters by GC/MS SIM 3 of 75

5 Air ,1,1-Trichloro-2,2,2-trifluoroethane EPA TO-15 GC/MS SIM ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethylene ,1-Dichloropropene ,2,3-Trichloropropane ,2,3-Trimethylbenzene ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane (DBCP) ,2-Dibromoethane (EDB, Ethylene dibromide) ,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon-114) ,2-Dichlorobenzene ,2-Dichloroethane (Ethylene dichloride) ,2-Dichloropropane ,2-Epoxybutane ,3,5-Trimethylbenzene ,3-Butadiene ,3-Dichlorobenzene ,3-Dichloropropane ,3-Propane sultone ,4-Dichlorobenzene ,4-Dioxane (1,4- Diethyleneoxide) Butene Chloro-1,2,2-trifluoroethane (Freon 133) Hexene Pentene Propene (Propylene) ,2,4-Trimethylpentane ,2-Dichloro-1,1,1-trifluoroethane (Freon 123) ,2-Dichloropropane ,2-Dimethylbutane ,3,4-Trimethylpentane ,3-Dimethylbutane ,3-Dimethylpentane ,4-Dimethylpentane Butanone (Methyl ethyl ketone, MEK) 4 of 75

6 Air Chlorotoluene EPA TO-15 GC/MS SIM Ethyltoluene Hexanone (MBK) Hexene Methyl-2-Butene Methylbutane (Isopentane) Methylheptane Methylhexane Methylnaphthalene Methylpentane (Isohexane) Methylphenol (o-cresol) methylpropane (Isobutane) Nitropropane Ethyltoluene (1-Methyl-3- ethylbenzene) Methyl-1-Butene Methylheptane Methylhexane Methylpentane Chlorotoluene Ethyltoluene Isopropyltoluene (p-cymene) Methyl-1-Pentene Methyl-2-pentanone (MIBK) 4300 Acetaldehyde 4315 Acetone 4320 Acetonitrile 5510 Acetophenone 4323 Acetylene 4325 Acrolein (Propenal) 4330 Acrylamide 4335 Acrylic acid 4340 Acrylonitrile 4355 Allyl chloride (3-Chloropropene) 6698 alpha-pinene 4375 Benzene 5635 Benzyl chloride 5075 beta-propiolactone 5765 bis(2-chloroethyl) ether 5780 bis(2-chloroisopropyl) ether 4515 bis(chloromethyl)ether 4385 Bromobenzene 4390 Bromochloromethane 4395 Bromodichloromethane 5 of 75

7 Air 4397 Bromoethane (Ethyl Bromide) EPA TO-15 GC/MS SIM 4398 Bromoethene 4400 Bromoform 4450 Carbon disulfide 4455 Carbon tetrachloride 7215 Carbonyl sulfide 7235 Catechol 9336 Chloroacetic acid 4475 Chlorobenzene 4575 Chlorodibromomethane 4577 Chlorodifluoromethane (Freon-22) 4485 Chloroethane (Ethyl chloride) 4505 Chloroform 4525 Chloroprene (2-Chloro-1,3-butadiene) 4705 cis & trans-1,2-dichloroethene 4645 cis-1,2-dichloroethylene 4680 cis-1,3-dichloropropene 4602 cis-2-butene 4604 cis-2-hexene 4603 cis-2-pentene 7325 Cresol/Cresylic acid (mixed isomers) 4555 Cyclohexane 4562 Cyclopentane 4563 Cyclopentene 4595 Dibromomethane (Methylene bromide) 4625 Dichlorodifluoromethane (Freon-12) 4627 Dichlorofluoromethane (Freon 21) 6080 Diethyl sulfate 7480 Dimethyl carbamoyl chloride 7485 Dimethyl sulfate 6208 d-limonene 4745 Epichlorohydrin (1-Chloro-2,3- epoxypropane) 4747 Ethane 4750 Ethanol 4752 Ethene 4755 Ethyl acetate 4760 Ethyl acrylate 6250 Ethyl carbamate (Urethane) 4765 Ethylbenzene 4795 Ethylene oxide 4770 Ethyl-t-butylether (ETBE) (2-Ethoxy-2- methylpropane) 4815 Formaldehyde 6 of 75

8 Air 9408 Gasoline range organics (GRO) EPA TO-15 GC/MS SIM 4835 Hexachlorobutadiene 4840 Hexachloroethane 4870 Iodomethane (Methyl iodide) 6317 Isoheptane 6320 Isophorone 4895 Isopropyl alcohol (2-Propanol, Isopropanol) 4900 Isopropylbenzene (Cumene) 5240 m+p-xylene 4930 Methanol 4940 Methyl acetate 4950 Methyl bromide (Bromomethane) 4960 Methyl chloride (Chloromethane) 9498 Methyl isocyanate 4990 Methyl methacrylate 5000 Methyl tert-butyl ether (MTBE) 4965 Methylcyclohexane 4966 Methylcyclopentane 4975 Methylene chloride (Dichloromethane) 5245 m-xylene 5010 n, n-dimethyl formamide 5005 Naphthalene 5007 n-butane 4415 n-butyl-acetate 4435 n-butylbenzene 5875 n-decane 4825 n-heptane 4855 n-hexane 5015 Nitrobenzene 6530 n-nitrosodimethylamine 6555 n-nitrosomorpholine 6520 n-nitroso-n-methylurea 5026 n-nonane 5027 n-octane 5028 n-pentane 5029 n-propane 5055 n-propanol 5090 n-propylbenzene 6747 n-undecane 5250 o-xylene 5253 p-diethylbenzene 6625 Phenol 7995 Phosgene 7 of 75

9 Air 6935 Propanal (Propionaldehyde) EPA TO-15 GC/MS SIM 9579 Propylene oxide 5255 p-xylene 4440 sec-butylbenzene 5100 Styrene 9594 Styrene oxide 4370 T-amylmethylether (TAME) 4420 tert-butyl alcohol 4445 tert-butylbenzene 5115 Tetrachloroethylene (Perchloroethylene) 5120 Tetrahydrofuran (THF) 5140 Toluene 4700 trans-1,2-dichloroethylene 4685 trans-1,3-dichloropropylene 4607 trans-2-butene 4606 trans-2-hexene 4608 trans-2-pentene 5170 Trichloroethene (Trichloroethylene) 5175 Trichlorofluoromethane (Fluorotrichloromethane, Freon 11) 5202 Trifluoromethane (Freon 23) 5225 Vinyl acetate 5230 Vinyl bromide (Bromoethane) 5235 Vinyl chloride 5260 Xylene (total) EPA TO Determination of Volatile Organic Compounds in Ambient Air Using Active Sampling Onto Sorbent Tubes ,1,1-Trichloroethane ,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethylene ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane (DBCP) ,2-Dibromoethane (EDB, Ethylene dibromide) ,2-Dichlorobenzene ,2-Dichloroethane (Ethylene dichloride) ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Butadiene ,3-Dichlorobenzene 8 of 75

10 Air EPA TO ,4-Dichlorobenzene ,4-Dioxane (1,4- Diethyleneoxide) ,2,4-Trimethylpentane Butanone (Methyl ethyl ketone, MEK) Methyl-2-pentanone (MIBK) 4315 Acetone 4375 Benzene 4395 Bromodichloromethane 4400 Bromoform 4450 Carbon disulfide 4455 Carbon tetrachloride 4475 Chlorobenzene 4485 Chloroethane (Ethyl chloride) 4505 Chloroform 4645 cis-1,2-dichloroethylene 4680 cis-1,3-dichloropropene 4625 Dichlorodifluoromethane (Freon-12) 4765 Ethylbenzene 4835 Hexachlorobutadiene 4900 Isopropylbenzene (Cumene) 5240 m+p-xylene 4960 Methyl chloride (Chloromethane) 5000 Methyl tert-butyl ether (MTBE) 4975 Methylene chloride (Dichloromethane) 4855 n-hexane 5250 o-xylene 5100 Styrene 5115 Tetrachloroethylene (Perchloroethylene) 5140 Toluene 4700 trans-1,2-dichloroethylene 4685 trans-1,3-dichloropropylene 5170 Trichloroethene (Trichloroethylene) 5175 Trichlorofluoromethane (Fluorotrichloromethane, Freon 11) 5225 Vinyl acetate 5235 Vinyl chloride 5260 Xylene (total) EPA TO Cryogenic Trapping 9408 Gasoline range organics (GRO) 4926 Methane EPA TO-4A Pesticides and PCBs by HV PUF GC ,4'-DDD ,4'-DDE 9 of 75

11 Air EPA TO-4A ,4'-DDT 7025 Aldrin 7110 alpha-bhc (alpha- Hexachlorocyclohexane) 7240 alpha-chlordane 8880 Aroclor-1016 (PCB-1016) 8885 Aroclor-1221 (PCB-1221) 8890 Aroclor-1232 (PCB-1232) 8895 Aroclor-1242 (PCB-1242) 8900 Aroclor-1248 (PCB-1248) 8905 Aroclor-1254 (PCB-1254) 8910 Aroclor-1260 (PCB-1260) 8912 Aroclor-1262 (PCB-1262) 8913 Aroclor-1268 (PCB-1268) 7115 beta-bhc (beta- Hexachlorocyclohexane) 7250 Chlordane (tech.) 7105 delta-bhc 7470 Dieldrin 7510 Endosulfan I 7515 Endosulfan II 7520 Endosulfan sulfate 7540 Endrin 7530 Endrin aldehyde 7535 Endrin ketone 7120 gamma-bhc (Lindane, gamma- HexachlorocyclohexanE) 7245 gamma-chlordane 7685 Heptachlor 7690 Heptachlor epoxide 7810 Methoxychlor 8250 Toxaphene (Chlorinated camphene) Drinking EPA ph - Electrometric Measurement 1900 ph EPA Total Dissolved Solids, 180 C Total dissolved solids EPA Total Suspended Solids, 0.2um 1960 Residue-nonfilterable (TSS) EPA Total Solids, C Residue-total 10 of 75

12 Drinking EPA Total Volatile Solids, 550 C Residue-volatile 1970 Residue-volatile 2070 Volatile suspended solids 2070 Volatile suspended solids EPA Settleable solids 1965 Residue-settleable EPA Turbidity - Nephelometric 2055 Turbidity EPA ICP - metals 1000 Aluminum 1015 Barium 1020 Beryllium 1023 Bismuth 1025 Boron 1030 Cadmium 1035 Calcium 1040 Chromium 1050 Cobalt 1055 Copper 1760 Hardness (calc.) 1070 Iron 1080 Lithium 1085 Magnesium 1090 Manganese 1100 Molybdenum 1105 Nickel 1910 Phosphorus, total 1125 Potassium 1990 Silica as SiO Silicon 1150 Silver 1155 Sodium 1160 Strontium 2017 Sulfur 1175 Tin 1180 Titanium 1185 Vanadium 1190 Zinc EPA Metals by ICP-MS 1000 Aluminum 11 of 75

13 Drinking EPA Antimony 1010 Arsenic 1015 Barium 1020 Beryllium 1025 Boron 1030 Cadmium 1035 Calcium 1040 Chromium 1050 Cobalt 1055 Copper 1760 Hardness (calc.) 1070 Iron 1075 Lead 1080 Lithium 1085 Magnesium 1090 Manganese 1100 Molybdenum 1105 Nickel 1910 Phosphorus, total 1125 Potassium 1140 Selenium 1145 Silicon 1150 Silver 1155 Sodium 1160 Strontium 1165 Thallium 1175 Tin 1180 Titanium 1185 Vanadium 1190 Zinc EPA Dissolved Hexavalent Chromium by Ion Chromatography 1045 Chromium VI EPA Mercury by Cold Vapor Atomic Absorption 1095 Mercury EPA Methods for the Determination of Inorganic Substances in Environmental Samples 1540 Bromide 1575 Chloride 1730 Fluoride 1810 Nitrate as N 1820 Nitrate-nitrite 1840 Nitrite as N 12 of 75

14 Drinking EPA Orthophosphate as P 1910 Phosphorus, total 2000 Sulfate EPA Perchlorate in Drinking by Ion Chromatography 1895 Perchlorate EPA Determination of Perchlorate in Drinking by Liquid Chromatography Electrospray Mass Spectrometry (LC/ESI/MS) 1895 Perchlorate EPA Phosphorous - Colorimetric, Automated persulfate 1870 Orthophosphate as P 1910 Phosphorus, total EPA Phosphorous - Colorimetric, automated block Orthophosphate as P 1910 Phosphorus, total EPA Phosphorous - Colorimetric, automated block Phosphorus, total EPA EDB/DBCP/TCP micro-extraction, GC/ECD ,2-Dibromo-3-chloropropane (DBCP) ,2-Dibromoethane (EDB, Ethylene dibromide) EPA Volatile Organic Compounds GC/MS Capillary Column ,1,1,2-Tetrachloroethane ,1,1-Trichloro-2,2,2-trifluoroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ,1,2-Trichloroethane ,1-Dichloro-2-propanone ,1-Dichloroethane ,1-Dichloroethylene ,1-Dichloropropene ,2,3-Trichlorobenzene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane (DBCP) ,2-Dibromoethane (EDB, Ethylene dibromide) 13 of 75

15 Drinking EPA ,2-Dichlorobenzene ,2-Dichloroethane (Ethylene dichloride) ,2-Dichloropropane ,3,5-Trichlorobenzene ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,3-Dichloropropane ,4-Dichlorobenzene Chlorobutane Chlorohexane ,2-Dichloropropane Butanone (Methyl ethyl ketone, MEK) Chloroethyl vinyl ether Chlorotoluene Hexanone (MBK) Nitropropane Bromofluorobenzene Chlorotoluene Isopropyltoluene (p-cymene) Methyl-2-pentanone (MIBK) 4315 Acetone 4325 Acrolein (Propenal) 4340 Acrylonitrile 4355 Allyl chloride (3-Chloropropene) 4375 Benzene 4385 Bromobenzene 4390 Bromochloromethane 4395 Bromodichloromethane 4397 Bromoethane (Ethyl Bromide) 4400 Bromoform 4450 Carbon disulfide 4455 Carbon tetrachloride 4475 Chlorobenzene 4575 Chlorodibromomethane 4485 Chloroethane (Ethyl chloride) 4505 Chloroform 4705 cis & trans-1,2-dichloroethene 4645 cis-1,2-dichloroethylene 4680 cis-1,3-dichloropropene 4600 cis-1,4-dichloro-2-butene 4555 Cyclohexane 4595 Dibromomethane (Methylene bromide) 4625 Dichlorodifluoromethane (Freon-12) 14 of 75

16 Drinking EPA Di-isopropylether (DIPE) 4765 Ethylbenzene SM 2130 B-94 online SM 2320 B 21st ED SM 2340 B 21st ED 4835 Hexachlorobutadiene 4840 Hexachloroethane 4870 Iodomethane (Methyl iodide) 4900 Isopropylbenzene (Cumene) 5240 m+p-xylene 4940 Methyl acetate 4950 Methyl bromide (Bromomethane) 4960 Methyl chloride (Chloromethane) 5000 Methyl tert-butyl ether (MTBE) 4975 Methylene chloride (Dichloromethane) 5245 m-xylene 5005 Naphthalene 4435 n-butylbenzene 5015 Nitrobenzene 5090 n-propylbenzene 5250 o-xylene 5035 Pentachloroethane 5255 p-xylene 4440 sec-butylbenzene 5100 Styrene 4370 T-amylmethylether (TAME) 4420 tert-butyl alcohol 4445 tert-butylbenzene 5115 Tetrachloroethylene (Perchloroethylene) 5140 Toluene 5205 Total trihalomethanes 4700 trans-1,2-dichloroethylene 4685 trans-1,3-dichloropropylene 4605 trans-1,4-dichloro-2-butene 5170 Trichloroethene (Trichloroethylene) 5175 Trichlorofluoromethane (Fluorotrichloromethane, Freon 11) 5225 Vinyl acetate 5235 Vinyl chloride 5260 Xylene (total) 2055 Turbidity 1505 Alkalinity as CaCO Hardness Turbidity by Nephelometric Method Alkalinity by Titration Method Hardness by calculation 15 of 75

17 Drinking SM 2340 B 22nd Ed SM 2340 C-97 online SM 2510 B 22nd Ed SM 2540 B 21st ED SM 2540 C 21st ED SM 2540 D 21st ED SM 2540 E SM 4500-Cl C 20th ED SM 4500-CN E 20th ED SM 4500-CN G 20th ED SM 4500-F C- 97 online SM 4500-H+ B online SM 4500-NO2 B-2000 online SM 4500-NO3 E minus SM 4500-NO2 B (calc.)-97 online SM 4500-NO3 E-2000 online 1760 Hardness (calc.) 1750 Hardness 1755 Total hardness as CaCO Conductivity 1950 Residue-total 1955 Residue-filterable (TDS) 1960 Residue-nonfilterable (TSS) 1725 Total, fixed, and volatile residue 1575 Chloride 1635 Cyanide 1645 Total cyanide 1510 Amenable cyanide 1730 Fluoride 1900 ph 1835 Nitrite 1840 Nitrite as N 1805 Nitrate 1810 Nitrate as N 1805 Nitrate 1810 Nitrate as N 1823 Nitrate plus Nitrite as N Hardness - Hardness by Calculation Hardness by EDTA Titration Method Conductivity by Probe Total Solids Dried at C Total Dissolved Solids Dried at 180C Total Suspended Solids Dried at C Fixed & Volatile Solids Ignited at 550 C Chloride by Iodometric Method II Cyanide by Colorimetric Determination Cyanide Amenable to Chlorination after Distillation Fluoride by Ion-Selective Electrode Method ph Value by Electrometric Method Nitrite by Colorimetric Determination Nitrate by Nitrate by calculation Nitrate Nitrogen by Cadmium Reduction Method 16 of 75

18 Drinking SM 4500-NO Nitrate-nitrite E-2000 online 1840 Nitrite as N Non- Potable SM 4500-P E- 97 online SM 5310 B-96 online SM 5540 C-93 online 1870 Orthophosphate as P 1910 Phosphorus, total 1710 Dissolved organic carbon (DOC) 2040 Total organic carbon 2025 Surfactants - MBAS Phosphorus by Ascorbic Acid Method TOC by High-Temperature Combustion Method Surfactants by Anionic Surfactants as MBAS EPA Pensky-Martens Closed-Cup Method for Determining Ignitability 1780 Ignitability EPA Corrosivity Toward Steel 1615 Corrosivity EPA Conductance - 25 C 1610 Conductivity EPA Toxicity Characteristic Leaching Procedure 9822 Extraction/Preparation EPA Synthetic Precipitation Leaching Procedure 9822 Extraction/Preparation EPA ph - Electrometric Measurement 1900 ph EPA Total Dissolved Solids, 180 C Total dissolved solids EPA Total Suspended Solids, 0.2um 1960 Residue-nonfilterable (TSS) EPA Total Solids, C Residue-total EPA Total Volatile Solids, 550 C Residue-volatile 2070 Volatile suspended solids EPA Settleable solids 1965 Residue-settleable 17 of 75

19 Non- Potable EPA 1631E Mercury in by Oxidation, Purge & Trap, and Cold Vapor Atomic Fluorescence 1095 Mercury EPA Trace Elements by Chelation Preconcentration and ICP/MS EPA 1664A (HEM) EPA 1664A (SGT-HEM) 1010 Arsenic 1030 Cadmium 1055 Copper 1075 Lead 1105 Nickel 1150 Silver 1190 Zinc 1803 n-hexane Extractable Material (O&G) 1860 Oil & Grease 2050 Total Petroleum Hydrocarbons (TPH) 1803 n-hexane Extractable Material (O&G) 1860 Oil & Grease 2050 Total Petroleum Hydrocarbons (TPH) N-Hexane Extractable Material (Oil and Grease) by Extraction and Gravimetry Silica Gen Treated N-Hexane Extractable Material (Oil and Grease) EPA Turbidity - Nephelometric 2055 Turbidity EPA ICP - metals 1000 Aluminum 1005 Antimony 1010 Arsenic 1015 Barium 1020 Beryllium 1023 Bismuth 1025 Boron 1030 Cadmium 1035 Calcium 1040 Chromium 1050 Cobalt 1055 Copper 1760 Hardness (calc.) 1070 Iron 1075 Lead 1080 Lithium 1085 Magnesium 1090 Manganese 18 of 75

20 Non- EPA Molybdenum Potable 1105 Nickel 1910 Phosphorus, total 1125 Potassium 1140 Selenium 1990 Silica as SiO Silicon 1150 Silver 1155 Sodium 1160 Strontium 2017 Sulfur 1165 Thallium 1175 Tin 1180 Titanium 1185 Vanadium 1190 Zinc EPA Metals by ICP-MS 1000 Aluminum 1005 Antimony 1010 Arsenic 1015 Barium 1020 Beryllium 1025 Boron 1030 Cadmium 1035 Calcium 1040 Chromium 1050 Cobalt 1055 Copper 1760 Hardness (calc.) 1070 Iron 1075 Lead 1085 Magnesium 1090 Manganese 1100 Molybdenum 1105 Nickel 1125 Potassium 1140 Selenium 1150 Silver 1155 Sodium 1160 Strontium 1165 Thallium 1175 Tin 1180 Titanium 19 of 75

21 EPA Vanadium Non- Potable 1190 Zinc EPA Dissolved Hexavalent Chromium by Ion Chromatography 1045 Chromium VI EPA Mercury by Cold Vapor Atomic Absorption 1095 Mercury EPA Methods for the Determination of Inorganic Substances in Environmental Samples 1540 Bromide 1575 Chloride 1730 Fluoride 1810 Nitrate as N 1820 Nitrate-nitrite 1840 Nitrite as N 1870 Orthophosphate as P 1910 Phosphorus, total 2000 Sulfate EPA Ion chromatography - anions Chlorate EPA 3005A Acid Digestion of waters for Total Recoverable or Dissolved Metals 9822 Extraction/Preparation EPA 3010A Acid Digestion of Aqueous samples and Extracts for Total Metals 9822 Extraction/Preparation EPA 3020A Acid Digestion of Aqueous samples and Extracts for Total Metals for Analysis by GFAA 8031 Extraction/Preparation EPA Perchlorate in Drinking by Ion Chromatography 1895 Perchlorate EPA Determination of Perchlorate in Drinking by Liquid Chromatography Electrospray Mass Spectrometry (LC/ESI/MS) 1895 Perchlorate EPA Ammonia Nitrogen - Colorimetric, Auto Phenate 1515 Ammonia as N EPA 3500B Organic Extraction and sample preparation 9822 Extraction/Preparation 20 of 75

22 Non- Potable EPA Total Kjeldahl Nitrogen - Block Digest, Phenate 1790 Kjeldahl nitrogen EPA 3510C Separatory Funnel Liquid-liquid extraction 9822 Extraction/Preparation EPA Organic Compounds in by Microextraction 8031 Extraction/Preparation EPA 3520C Continuous Liquid-liquid extraction 9822 Extraction/Preparation EPA 3630C Silica gel cleanup 9822 Extraction/Preparation EPA Phosphorous - Colorimetric, Automated persulfate 1870 Orthophosphate as P 1910 Phosphorus, total EPA Phosphorous - Colorimetric, two reagent Orthophosphate as P 1910 Phosphorus, total EPA Phosphorous - Colorimetric, automated block Orthophosphate as P EPA Chemical Oxygen Demand - Colorimetric, Automated Chemical oxygen demand EPA Oil and Grease - Spectrophotometric, Infrared Oil & Grease EPA Petroleum Hydrocarbons - Spec. Infrared Total Petroleum Hydrocarbons (TPH) EPA Phenolics - Spectrophotometric, manual Total phenolics EPA Sample Preparation for Volatile Organics 9822 Extraction/Preparation EPA 5030B Purge and trap for aqueous samples 9822 Extraction/Preparation EPA 5030C Purge-and-Trap for Aqueous Samples 8031 Extraction/Preparation EPA Volatile Organic Compounds GC/MS Capillary Column ,1,1-Trichloroethane 21 of 75

23 EPA ,1,2,2-Tetrachloroethane Non- Potable ,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ,1,2-Trichloroethane ,1-Dichloro-2-propanone ,1-Dichloroethane ,1-Dichloroethylene ,1-Dichloropropene ,2,3-Trichlorobenzene ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane (DBCP) ,2-Dibromoethane (EDB, Ethylene dibromide) ,2-Dichlorobenzene ,2-Dichloroethane (Ethylene dichloride) ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,3-Dichloropropane ,4-Dichlorobenzene ,2-Dichloropropane Butanone (Methyl ethyl ketone, MEK) Chloroethyl vinyl ether Chlorotoluene Hexanone (MBK) Bromofluorobenzene Chlorotoluene Isopropyltoluene (p-cymene) Methyl-2-pentanone (MIBK) 4315 Acetone 4325 Acrolein (Propenal) 4340 Acrylonitrile 4355 Allyl chloride (3-Chloropropene) 4375 Benzene 4385 Bromobenzene 4390 Bromochloromethane 4395 Bromodichloromethane 4397 Bromoethane (Ethyl Bromide) 4400 Bromoform 4450 Carbon disulfide 4455 Carbon tetrachloride 4475 Chlorobenzene 4575 Chlorodibromomethane 22 of 75

24 Non- EPA Chloroethane (Ethyl chloride) Potable 4505 Chloroform 4705 cis & trans-1,2-dichloroethene 4645 cis-1,2-dichloroethylene 4680 cis-1,3-dichloropropene 4555 Cyclohexane 4595 Dibromomethane (Methylene bromide) 4625 Dichlorodifluoromethane (Freon-12) 9375 Di-isopropylether (DIPE) 4765 Ethylbenzene 4835 Hexachlorobutadiene 4870 Iodomethane (Methyl iodide) 4900 Isopropylbenzene (Cumene) 5240 m+p-xylene 4925 Methacrylonitrile 4950 Methyl bromide (Bromomethane) 4960 Methyl chloride (Chloromethane) 4990 Methyl methacrylate 5000 Methyl tert-butyl ether (MTBE) 4975 Methylene chloride (Dichloromethane) 5245 m-xylene 5005 Naphthalene 4435 n-butylbenzene 5090 n-propylbenzene 5250 o-xylene 5035 Pentachloroethane 5080 Propionitrile (Ethyl cyanide) 5255 p-xylene 4440 sec-butylbenzene 5100 Styrene 4370 T-amylmethylether (TAME) 4420 tert-butyl alcohol 4445 tert-butylbenzene 5115 Tetrachloroethylene (Perchloroethylene) 5120 Tetrahydrofuran (THF) 5140 Toluene 5205 Total trihalomethanes 4700 trans-1,2-dichloroethylene 4685 trans-1,3-dichloropropylene 4605 trans-1,4-dichloro-2-butene 5170 Trichloroethene (Trichloroethylene) 5175 Trichlorofluoromethane (Fluorotrichloromethane, Freon 11) 5225 Vinyl acetate 23 of 75

25 EPA Vinyl chloride Non- Potable 5260 Xylene (total) EPA Volatile Organic Compounds GC/MS Capillary Column 4470 Chloroacetonitrile 4725 Diethyl ether 4810 Ethyl methacrylate 4770 Ethyl-t-butylether (ETBE) (2-Ethoxy-2- methylpropane) 4925 Methacrylonitrile 5080 Propionitrile (Ethyl cyanide) 5120 Tetrahydrofuran (THF) EPA 6010B ICP - AES 1000 Aluminum 1005 Antimony 1010 Arsenic 1015 Barium 1020 Beryllium 1023 Bismuth 1025 Boron 1030 Cadmium 1035 Calcium 1040 Chromium 1050 Cobalt 1055 Copper 1057 Gallium 1760 Hardness (calc.) 1070 Iron 1075 Lead 1080 Lithium 1085 Magnesium 1090 Manganese 1100 Molybdenum 1105 Nickel 1910 Phosphorus, total 1125 Potassium 1140 Selenium 1990 Silica as SiO Silicon 1150 Silver 1155 Sodium 1160 Strontium 2017 Sulfur 24 of 75

26 Non- EPA 6010B 1165 Thallium Potable 1175 Tin 1180 Titanium 1185 Vanadium 1190 Zinc EPA Purgeable Aromatics by GC/PID Purge & Trap ,2-Dichlorobenzene ,3-Dichlorobenzene ,4-Dichlorobenzene 4375 Benzene 4765 Ethylbenzene 5240 m+p-xylene 5250 o-xylene 5140 Toluene 5260 Xylene (total) EPA Inductively Coupled Plasma-Mass Spectrometry 1005 Antimony 1010 Arsenic 1015 Barium 1020 Beryllium 1030 Cadmium 1040 Chromium 1050 Cobalt 1055 Copper 1075 Lead 1100 Molybdenum 1105 Nickel 1140 Selenium 1150 Silver 1165 Thallium 1185 Vanadium 1190 Zinc EPA Organochlorine Pesticides & PCBs by GC/ECD ,4'-DDD ,4'-DDE ,4'-DDT 7025 Aldrin 7110 alpha-bhc (alpha- Hexachlorocyclohexane) 7240 alpha-chlordane 8880 Aroclor-1016 (PCB-1016) 8885 Aroclor-1221 (PCB-1221) 25 of 75

27 Non- EPA Aroclor-1232 (PCB-1232) Potable 8895 Aroclor-1242 (PCB-1242) 8900 Aroclor-1248 (PCB-1248) 8905 Aroclor-1254 (PCB-1254) 8910 Aroclor-1260 (PCB-1260) 8912 Aroclor-1262 (PCB-1262) 8913 Aroclor-1268 (PCB-1268) 7115 beta-bhc (beta- Hexachlorocyclohexane) 7250 Chlordane (tech.) 7105 delta-bhc 7470 Dieldrin 7510 Endosulfan I 7515 Endosulfan II 7520 Endosulfan sulfate 7540 Endrin 7530 Endrin aldehyde 7535 Endrin ketone 7120 gamma-bhc (Lindane, gamma- HexachlorocyclohexanE) 7245 gamma-chlordane 7685 Heptachlor 7690 Heptachlor epoxide 6275 Hexachlorobenzene 7810 Methoxychlor 7870 Mirex 8250 Toxaphene (Chlorinated camphene) EPA Volatile Organic Compounds by purge and trap GC/MS ,1,1,2-Tetrachloroethane ,1,1-Trichloro-2-propanone ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethylene ,1-Dichloropropene ,2,3-Trichlorobenzene ,2,3-Trichloropropane ,2,3-Trimethylbenzene ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane (DBCP) 26 of 75

28 Non- Potable EPA ,2-Dibromoethane (EDB, Ethylene dibromide) ,2-Dichlorobenzene ,2-Dichloroethane (Ethylene dichloride) ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Butadiene ,3-Dichlorobenzene ,3-Dichloropropane ,4-Dichlorobenzene ,4-Dioxane (1,4- Diethyleneoxide) ,2,4-Trimethylpentane ,2-Dichloro-1,1,1-trifluoroethane (Freon 123) ,2-Dichloropropane Butanone (Methyl ethyl ketone, MEK) Chloroethyl vinyl ether Chlorotoluene Hexanone (MBK) Chlorotoluene Isopropyltoluene (p-cymene) Methyl-2-pentanone (MIBK) 4315 Acetone 4320 Acetonitrile 4325 Acrolein (Propenal) 4340 Acrylonitrile 4355 Allyl chloride (3-Chloropropene) 4375 Benzene 4385 Bromobenzene 4390 Bromochloromethane 4395 Bromodichloromethane 4397 Bromoethane (Ethyl Bromide) 4400 Bromoform 4450 Carbon disulfide 4455 Carbon tetrachloride 4475 Chlorobenzene 4575 Chlorodibromomethane 4485 Chloroethane (Ethyl chloride) 4505 Chloroform 4705 cis & trans-1,2-dichloroethene 4645 cis-1,2-dichloroethylene 4680 cis-1,3-dichloropropene 4600 cis-1,4-dichloro-2-butene 4555 Cyclohexane 27 of 75

29 Non- EPA Cyclohexanone Potable 4590 Dibromofluoromethane 4595 Dibromomethane (Methylene bromide) 4625 Dichlorodifluoromethane (Freon-12) 4725 Diethyl ether 9375 Di-isopropylether (DIPE) 4750 Ethanol 4810 Ethyl methacrylate 4765 Ethylbenzene 4770 Ethyl-t-butylether (ETBE) (2-Ethoxy-2- methylpropane) 4870 Iodomethane (Methyl iodide) 4875 Isobutyl alcohol (2-Methyl-1-propanol) 4895 Isopropyl alcohol (2-Propanol, Isopropanol) 4900 Isopropylbenzene (Cumene) 5240 m+p-xylene 4950 Methyl bromide (Bromomethane) 4960 Methyl chloride (Chloromethane) 5000 Methyl tert-butyl ether (MTBE) 4975 Methylene chloride (Dichloromethane) 5245 m-xylene 5005 Naphthalene 4435 n-butylbenzene 4855 n-hexane 5015 Nitrobenzene 5090 n-propylbenzene 5250 o-xylene 5080 Propionitrile (Ethyl cyanide) 5255 p-xylene 4440 sec-butylbenzene 5100 Styrene 4370 T-amylmethylether (TAME) 4420 tert-butyl alcohol 4445 tert-butylbenzene 5115 Tetrachloroethylene (Perchloroethylene) 5140 Toluene 5205 Total trihalomethanes 4700 trans-1,2-dichloroethylene 4685 trans-1,3-dichloropropylene 4605 trans-1,4-dichloro-2-butene 5170 Trichloroethene (Trichloroethylene) 5175 Trichlorofluoromethane (Fluorotrichloromethane, Freon 11) 28 of 75

30 Non- EPA Vinyl acetate Potable 5230 Vinyl bromide (Bromoethane) 5235 Vinyl chloride 5260 Xylene (total) EPA Base/Neutrals and Acids by GC/MS ,1'-Biphenyl (BZ-0) ,2,3,4-Tetrachlorobenzene ,2,4,5-Tetrachlorobenzene ,2,4-Trichlorobenzene ,2-Dichlorobenzene ,2-Dinitrobenzene ,2-Diphenylhydrazine ,3,5-Trinitrobenzene (1,3,5-TNB) ,3-Dichlorobenzene ,3-Dinitrobenzene (1,3-DNB) ,4-Dichlorobenzene ,4-Dinitrobenzene ,4-Dioxane (1,4- Diethyleneoxide) ,4-Naphthoquinone ,4-Phenylenediamine Chloronaphthalene Methylnaphthalene Methylphenanthrene Naphthylamine ,2-Oxybis(1-chloropropane) ,3,4,6-Tetrachlorophenol ,3,4-Trichlorophenol ,3,5,6-Tetrachlorophenol ,3,5-Trichlorophenol ,3,6-Trichlorophenol (4C) ,3-Dichloroaniline ,3-Dichlorophenol ,3-Dinitrotoluene ,4,5-Trichlorophenol ,4,6-Trichlorophenol ,4-Diaminotoluene ,4-Dichlorophenol ,4-Dimethylphenol ,4-Dinitrophenol ,4-Dinitrotoluene (2,4-DNT) ,5-Dichlorophenol ,5-Dinitrophenol ,6-Diaminotoluene 29 of 75

31 Non- EPA ,6-Dichlorophenol Potable ,6-Dinitrotoluene (2,6-DNT) Acetylaminofluorene Chloronaphthalene Chlorophenol Methyl-4,6-dinitrophenol (4,6-Dinitro-2 -methylphenol) Methylaniline (o-toluidine) Methylnaphthalene Methylphenol (o-cresol) Naphthylamine Nitroaniline Nitrophenol Terphenyl & 4 Methylphenol ,3'-Dichlorobenzidine ,3'-Dimethylbenzidine ,4,5-Trichlorophenol ,4-Dichlorophenol Chlorophenol Methylcholanthrene Methylphenol (m-cresol) Nitroaniline ,4'-DDD ,4'-DDE ,4'-DDT Aminobiphenyl Bromophenyl phenyl ether (BDE-3) Chloro-2-methylphenol Chloro-3-methylphenol Chloroaniline Chlorophenol Chlorophenyl phenylether Dimethyl aminoazobenzene Methylphenol (p-cresol) Nitroaniline Nitrophenol Chloro-3-methylphenol ,12-Dimethylbenz(a) anthracene 5500 Acenaphthene 5505 Acenaphthylene 5510 Acetophenone 4330 Acrylamide 7010 Aldicarb (Temik) 30 of 75

32 EPA Aldrin Non- Potable 7110 alpha-bhc (alpha- Hexachlorocyclohexane) 6700 alpha-terpineol 5545 Aniline 5555 Anthracene 7065 Atrazine 5562 Azobenzene 5565 Benzal chloride 5570 Benzaldehyde 5595 Benzidine 5575 Benzo(a)anthracene 5580 Benzo(a)pyrene 5590 Benzo(g,h,i)perylene 5600 Benzo(k)fluoranthene 5585 Benzo[b]fluoranthene 5587 Benzofluoranthene 5610 Benzoic acid 5630 Benzyl alcohol 7115 beta-bhc (beta- Hexachlorocyclohexane) 5760 bis(2-chloroethoxy)methane 5765 bis(2-chloroethyl) ether 5780 bis(2-chloroisopropyl) ether 6062 bis(2-ethylhexyl)adipate 5670 Butyl benzyl phthalate 5680 Carbazole 7205 Carbofuran (Furaden) 7210 Carbofuran phenol 7250 Chlordane (tech.) 7260 Chlorobenzilate 5855 Chrysene 8906 Coelution - 3-Chlorophenol + 4- Chlorophenol 5862 Cresols, Total 7105 delta-bhc 6065 Di(2-ethylhexyl) phthalate (bis(2- Ethylhexyl)phthalate, DEHP) 7405 Diallate 5895 Dibenz(a,h) anthracene 5905 Dibenzofuran 4625 Dichlorodifluoromethane (Freon-12) 7470 Dieldrin 6070 Diethyl phthalate 7475 Dimethoate 31 of 75

33 EPA Dimethyl phthalate Non- Potable 5925 Di-n-butyl phthalate 6200 Di-n-octyl phthalate 8620 Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP) 6210 Diphenyl ether (Diphenyl Oxide) 6205 Diphenylamine 8625 Disulfoton 7510 Endosulfan I 7515 Endosulfan II 7520 Endosulfan sulfate 7540 Endrin 6260 Ethyl methanesulfonate 7580 Famphur 6265 Fluoranthene 6270 Fluorene 7120 gamma-bhc (Lindane, gamma- HexachlorocyclohexanE) 7650 Garlon (Triclopyr) 7685 Heptachlor 7690 Heptachlor epoxide 6275 Hexachlorobenzene 4835 Hexachlorobutadiene 6285 Hexachlorocyclopentadiene 4840 Hexachloroethane 6290 Hexachlorophene 6295 Hexachloropropene 6312 Indene 6315 Indeno(1,2,3-cd) pyrene 7725 Isodrin 6320 Isophorone 6325 Isosafrole 7740 Kepone 6345 Methapyrilene 7810 Methoxychlor 4960 Methyl chloride (Chloromethane) 6375 Methyl methanesulfonate 7825 Methyl parathion (Parathion, methyl) 5005 Naphthalene 5875 n-decane 6230 n-docosane 6235 n-dodecane 6240 n-eicosane 6300 n-hexadecane 32 of 75

34 Non- EPA Nitrobenzene Potable 6525 n-nitrosodiethylamine 6530 n-nitrosodimethylamine 5025 n-nitroso-di-n-butylamine 6545 n-nitrosodi-n-propylamine 6535 n-nitrosodiphenylamine 6550 n-nitrosomethylethalamine 6560 n-nitrosopiperidine 6565 n-nitrosopyrrolidine 6580 n-octadecane 6745 n-tetradecane 8290 o,o,o-triethyl phosphorothioate 5553 Octachlorostyrene 7955 Parathion, ethyl 6590 Pentachlorobenzene 5035 Pentachloroethane 6600 Pentachloronitrobenzene 6605 Pentachlorophenol 6610 Phenacetin 6615 Phenanthrene 6625 Phenol 7985 Phorate 6640 Phthalic anhydride 6650 Pronamide (Kerb) 6665 Pyrene 5095 Pyridine 6685 Safrole 8200 Tetrachlorvinphos (Stirophos, Gardona) Z-isomer 8235 Thionazin (Zinophos) 8250 Toxaphene (Chlorinated camphene) 5200 Triethylamine EPA Perchlorate in, Soils and Solid Wastes Using High Performance Liquid Chromatography/Electrospray Ionization/Mass Spectrometry 1895 Perchlorate EPA 7196A Chromium Hexavalent colorimetric 1045 Chromium VI EPA Determination of Hexavalent Chromium in Drinking, Groundwater and Industrial Wastewater Effluents by Ion Chromatography 1045 Chromium VI 33 of 75

35 EPA Lead by Flame Atomic Absorption Non- Potable 1075 Lead EPA 7470A Mercury in Liquid Waste by Cold Vapor Atomic Absorption 1095 Mercury EPA 8015B Non-halogenated organics using GC/FID 9369 Diesel range organics (DRO) 4750 Ethanol 9408 Gasoline range organics (GRO) 4875 Isobutyl alcohol (2-Methyl-1-propanol) 4895 Isopropyl alcohol (2-Propanol, Isopropanol) 9488 Jet Fuel 9409 Kerosene 4930 Methanol 9410 Mineral Spirits 9499 Motor Oil 4425 n-butyl alcohol (1-Butanol, n-butanol) 5055 n-propanol 2050 Total Petroleum Hydrocarbons (TPH) 1935 Total recoverable petroleum hydrocarbons (TRPH) EPA 8021B Aromatic and Halogenated Volatiles by GC with PID and/or ECD Purge & Trap ,2-Dichlorobenzene ,3-Dichlorobenzene ,4-Dichlorobenzene 4375 Benzene 4765 Ethylbenzene 5000 Methyl tert-butyl ether (MTBE) 5140 Toluene 5260 Xylene (total) EPA 8081A Organochlorine Pesticides by GC/ECD ,4'-DDD ,4'-DDE ,4'-DDT ,4'-DDD ,4'-DDE ,4'-DDT 7025 Aldrin 7110 alpha-bhc (alpha- Hexachlorocyclohexane) 7240 alpha-chlordane 34 of 75

36 Non- Potable EPA 8081A 7115 beta-bhc (beta- Hexachlorocyclohexane) 7250 Chlordane (tech.) 7260 Chlorobenzilate 7925 cis-nonachlor 7405 Diallate 7470 Dieldrin 7510 Endosulfan I 7515 Endosulfan II 7520 Endosulfan sulfate 7540 Endrin 7530 Endrin aldehyde 7535 Endrin ketone 7120 gamma-bhc (Lindane, gamma- HexachlorocyclohexanE) 7245 gamma-chlordane 7685 Heptachlor 7690 Heptachlor epoxide 6275 Hexachlorobenzene 6285 Hexachlorocyclopentadiene 7740 Kepone 7870 Mirex 3890 Oxychlordane 8250 Toxaphene (Chlorinated camphene) 7910 trans-nonachlor EPA Polychlorinated Biphenyls (PCBs) by GC/ECD 8880 Aroclor-1016 (PCB-1016) 8885 Aroclor-1221 (PCB-1221) 8890 Aroclor-1232 (PCB-1232) 8895 Aroclor-1242 (PCB-1242) 8900 Aroclor-1248 (PCB-1248) 8905 Aroclor-1254 (PCB-1254) 8910 Aroclor-1260 (PCB-1260) 8912 Aroclor-1262 (PCB-1262) 8913 Aroclor-1268 (PCB-1268) EPA 8082A Polychlorinated Biphenyls (PCBs) by GC/ECD 8880 Aroclor-1016 (PCB-1016) 8885 Aroclor-1221 (PCB-1221) 8890 Aroclor-1232 (PCB-1232) 8895 Aroclor-1242 (PCB-1242) 8900 Aroclor-1248 (PCB-1248) 8905 Aroclor-1254 (PCB-1254) 8910 Aroclor-1260 (PCB-1260) 35 of 75

37 EPA 8082A 8912 Aroclor-1262 (PCB-1262) Non- Potable 8913 Aroclor-1268 (PCB-1268) EPA 8141A Organophosphorous Pesticides by GC/NPD 7065 Atrazine 7075 Azinphos-methyl (Guthion) 7125 Bolstar (Sulprofos) 7300 Chlorpyrifos 7315 Coumaphos 7390 Demeton 7395 Demeton-o 7385 Demeton-s 7410 Diazinon 8610 Dichlorovos (DDVP, Dichlorvos) 7475 Dimethoate 8625 Disulfoton 7550 EPN 7555 EPTC (Eptam, s-ethyl-dipropyl thio carbamate) 7565 Ethion 7570 Ethoprop 7580 Famphur 7600 Fensulfothion 7605 Fenthion 7770 Malathion 7785 Merphos 7825 Methyl parathion (Parathion, methyl) 7850 Mevinphos 7905 Naled 7955 Parathion, ethyl 7985 Phorate 8110 Ronnel 8125 Simazine 8155 Sulfotepp 8200 Tetrachlorvinphos (Stirophos, Gardona) Z-isomer 8235 Thionazin (Zinophos) 8245 Tokuthion (Prothiophos) 8275 Trichloronate EPA 8151A Chlorinated Herbicides by GC/ECD ,4,5-T ,4-D ,4-DB 8550 Dacthal (DCPA) 36 of 75

38 EPA 8151A 8555 Dalapon Non- Potable 8595 Dicamba 8605 Dichloroprop (Dichlorprop) 8620 Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP) 7775 MCPA 7780 MCPP 8650 Silvex (2,4,5-TP) EPA 8260B Volatile Organic Compounds by purge and trap GC/MS ,1,1,2-Tetrachloroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloroethane ,1-Dichloroethane ,1-Dichloroethylene ,1-Dichloropropene ,2,3-Trichlorobenzene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromoethane (EDB, Ethylene dibromide) ,2-Dichlorobenzene ,2-Dichloroethane (Ethylene dichloride) ,2-Dichloropropane ,3,5-Trimethylbenzene ,3-Dichlorobenzene ,3-Dichloropropane ,4-Dichlorobenzene ,4-Dioxane (1,4- Diethyleneoxide) ,2-Dichloropropane Butanone (Methyl ethyl ketone, MEK) Chloroethyl vinyl ether Chlorotoluene Hexanone (MBK) Chlorotoluene Methyl-2-pentanone (MIBK) 4315 Acetone 4320 Acetonitrile 4325 Acrolein (Propenal) 4340 Acrylonitrile 4355 Allyl chloride (3-Chloropropene) 4375 Benzene 37 of 75

39 Non- EPA 8260B 4385 Bromobenzene Potable 4390 Bromochloromethane 4395 Bromodichloromethane 4400 Bromoform 4450 Carbon disulfide 4455 Carbon tetrachloride 4475 Chlorobenzene 4575 Chlorodibromomethane 4485 Chloroethane (Ethyl chloride) 4505 Chloroform 4525 Chloroprene (2-Chloro-1,3-butadiene) 4645 cis-1,2-dichloroethylene 4680 cis-1,3-dichloropropene 4590 Dibromofluoromethane 4595 Dibromomethane (Methylene bromide) 4627 Dichlorofluoromethane (Freon 21) 4810 Ethyl methacrylate 4765 Ethylbenzene 4770 Ethyl-t-butylether (ETBE) (2-Ethoxy-2- methylpropane) 4835 Hexachlorobutadiene 4870 Iodomethane (Methyl iodide) 4875 Isobutyl alcohol (2-Methyl-1-propanol) 4900 Isopropylbenzene (Cumene) 4925 Methacrylonitrile 4950 Methyl bromide (Bromomethane) 4960 Methyl chloride (Chloromethane) 4990 Methyl methacrylate 5000 Methyl tert-butyl ether (MTBE) 4975 Methylene chloride (Dichloromethane) 5005 Naphthalene 4435 n-butylbenzene 5015 Nitrobenzene 5090 n-propylbenzene 5035 Pentachloroethane 5040 Pentafluorobenzene 5080 Propionitrile (Ethyl cyanide) 4440 sec-butylbenzene 5100 Styrene 4370 T-amylmethylether (TAME) 4420 tert-butyl alcohol 4445 tert-butylbenzene 5115 Tetrachloroethylene (Perchloroethylene) 5140 Toluene 38 of 75

40 Non- EPA 8260B 4700 trans-1,2-dichloroethylene Potable 4685 trans-1,3-dichloropropylene 4605 trans-1,4-dichloro-2-butene 5170 Trichloroethene (Trichloroethylene) 5175 Trichlorofluoromethane (Fluorotrichloromethane, Freon 11) 5225 Vinyl acetate 5235 Vinyl chloride 5260 Xylene (total) EPA 8260B SIM Volatile Organic Compounds by purge and trap GC/MS-SIM ,2,3-Trichloropropane ,4-Dioxane (1,4- Diethyleneoxide) EPA 8260C Volatile Organics: GC/MS (capillary column) ,1,1,2-Tetrachloroethane ,1,1-Trichloro-2,2,2-trifluoroethane ,1,1-Trichloroethane ,1,2,2-Tetrachloroethane ,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ,1,2-Trichloroethane ,1,2-Trichlorofluoroethane ,1,2-Trifluoroethane ,1-Dichloroethane ,1-Dichloroethylene ,1-Dichloropropene ,2,3-Trichlorobenzene ,2,3-Trichloropropane ,2,4-Trichlorobenzene ,2,4-Trimethylbenzene ,2-Dibromo-3-chloropropane (DBCP) ,2-Dibromoethane (EDB, Ethylene dibromide) ,2-Dichloro-1,1,2-trifluoroethane ,2-Dichlorobenzene ,2-Dichloroethane (Ethylene dichloride) ,2-Dichloropropane ,3,5-Trichlorobenzene ,3,5-Trimethylbenzene ,3-Dichloro-2-propanol ,3-Dichlorobenzene ,3-Dichloropropane ,3-Dichloropropene ,4-Dichlorobenzene 39 of 75

41 Non- EPA 8260C ,4-Difluorobenzene Potable ,4-Dioxane (1,4- Diethyleneoxide) Chlorohexane ,2-Dichloropropane Butanone (Methyl ethyl ketone, MEK) Chloroethyl vinyl ether Chlorotoluene Hexanone (MBK) Pentanone Bromofluorobenzene Chlorotoluene Isopropyltoluene (p-cymene) Methyl-2-pentanone (MIBK) 4315 Acetone 4320 Acetonitrile 4325 Acrolein (Propenal) 4340 Acrylonitrile 4355 Allyl chloride (3-Chloropropene) 4375 Benzene 5635 Benzyl chloride 4385 Bromobenzene 4390 Bromochloromethane 4395 Bromodichloromethane 4397 Bromoethane (Ethyl Bromide) 4400 Bromoform 4450 Carbon disulfide 4455 Carbon tetrachloride 4475 Chlorobenzene 4575 Chlorodibromomethane 4485 Chloroethane (Ethyl chloride) 4505 Chloroform 4525 Chloroprene (2-Chloro-1,3-butadiene) 4705 cis & trans-1,2-dichloroethene 4645 cis-1,2-dichloroethylene 4680 cis-1,3-dichloropropene 4600 cis-1,4-dichloro-2-butene 4555 Cyclohexane 4560 Cyclohexanone 4580 Dibromochloropropane 4590 Dibromofluoromethane 4595 Dibromomethane (Methylene bromide) 4625 Dichlorodifluoromethane (Freon-12) 9375 Di-isopropylether (DIPE) 40 of 75

42 EPA 8260C 4750 Ethanol Non- Potable EPA 8260C SIM 4755 Ethyl acetate 4765 Ethylbenzene 4770 Ethyl-t-butylether (ETBE) (2-Ethoxy-2- methylpropane) 9408 Gasoline range organics (GRO) 4840 Hexachloroethane 4870 Iodomethane (Methyl iodide) 4900 Isopropylbenzene (Cumene) 5240 m+p-xylene 4950 Methyl bromide (Bromomethane) 4960 Methyl chloride (Chloromethane) 5000 Methyl tert-butyl ether (MTBE) 4975 Methylene chloride (Dichloromethane) 5005 Naphthalene 4435 n-butylbenzene 4855 n-hexane 5015 Nitrobenzene 5250 o-xylene 4440 sec-butylbenzene 5100 Styrene 4420 tert-butyl alcohol 4445 tert-butylbenzene 5115 Tetrachloroethylene (Perchloroethylene) 5140 Toluene 4700 trans-1,2-dichloroethylene 4685 trans-1,3-dichloropropylene 5170 Trichloroethene (Trichloroethylene) 5225 Vinyl acetate 5230 Vinyl bromide (Bromoethane) 5235 Vinyl chloride 5260 Xylene (total) ,2,3-Trichloropropane ,4-Dioxane (1,4- Diethyleneoxide) Volatile Organic Compounds by GC/MS-SIM EPA 8270C Semivolatile Organic compounds by GC/MS ,2,4,5-Tetrachlorobenzene ,2,4-Trichlorobenzene ,2-Dichlorobenzene ,2-Dinitrobenzene ,2-Diphenylhydrazine ,3,5-Trichlorobenzene 41 of 75

43 Non- EPA 8270C ,3-Dichlorobenzene Potable ,3-Dinitrobenzene (1,3-DNB) ,4-Dichlorobenzene ,4-Dinitrobenzene ,4-Naphthoquinone ,4-Phenylenediamine Acetyl-2-thiourea Chloronaphthalene Naphthylamine ,3,4,6-Tetrachlorophenol ,4,5-Trichlorophenol ,4,6-Trichlorophenol ,4-Diaminotoluene ,4-Dichlorophenol ,4-Dimethylphenol ,4-Dinitrophenol ,4-Dinitrotoluene (2,4-DNT) ,4-Toluene diisocyanate ,6-Dichlorophenol ,6-Dinitrotoluene (2,6-DNT) Acetylaminofluorene Chloronaphthalene Chlorophenol Cyclohexyl-4,6-dinitrophenol Methyl-4,6-dinitrophenol (4,6-Dinitro-2 -methylphenol) Methylaniline (o-toluidine) Methylnaphthalene Methylphenol (o-cresol) Naphthylamine Nitroaniline Nitrophenol Picoline (2-Methylpyridine) ,3'-Dimethoxybenzidine ,3'-Dimethylbenzidine Chloroaniline Methylcholanthrene Methylphenol (m-cresol) Nitroaniline Aminobiphenyl Bromophenyl phenyl ether (BDE-3) Chloro-3-methylphenol Chloroaniline Chlorophenyl phenylether 42 of 75

44 Non- EPA 8270C Dimethyl aminoazobenzene Potable Methylphenol (p-cresol) Nitroaniline Nitrophenol Nitro-o-toluidine ,12-Dimethylbenz(a) anthracene 6125 a-a-dimethylphenethylamine 5500 Acenaphthene 5505 Acenaphthylene 5510 Acetophenone 5545 Aniline 5555 Anthracene 5560 Aramite 5595 Benzidine 5575 Benzo(a)anthracene 5580 Benzo(a)pyrene 5590 Benzo(g,h,i)perylene 5600 Benzo(k)fluoranthene 5585 Benzo[b]fluoranthene 5610 Benzoic acid 5630 Benzyl alcohol 5760 bis(2-chloroethoxy)methane 5765 bis(2-chloroethyl) ether 5780 bis(2-chloroisopropyl) ether 5670 Butyl benzyl phthalate 5680 Carbazole 5855 Chrysene 6065 Di(2-ethylhexyl) phthalate (bis(2- Ethylhexyl)phthalate, DEHP) 5900 Dibenz(a, j) acridine 5895 Dibenz(a,h) anthracene 5890 Dibenzo(a,e) pyrene 5905 Dibenzofuran 6070 Diethyl phthalate 6080 Diethyl sulfate 6075 Diethylstilbestrol 6090 Dihydrosafrole 6135 Dimethyl phthalate 5925 Di-n-butyl phthalate 6200 Di-n-octyl phthalate 6205 Diphenylamine 6250 Ethyl carbamate (Urethane) 6260 Ethyl methanesulfonate 6265 Fluoranthene 43 of 75

45 Non- EPA 8270C 6270 Fluorene Potable 6275 Hexachlorobenzene 4835 Hexachlorobutadiene EPA 8270C SIM 6285 Hexachlorocyclopentadiene 4840 Hexachloroethane 6290 Hexachlorophene 6295 Hexachloropropene 6315 Indeno(1,2,3-cd) pyrene 6320 Isophorone 6325 Isosafrole 6335 Maleic anhydride 6375 Methyl methanesulfonate 5005 Naphthalene 6450 Nicotine 5015 Nitrobenzene 6525 n-nitrosodiethylamine 6530 n-nitrosodimethylamine 5025 n-nitroso-di-n-butylamine 6545 n-nitrosodi-n-propylamine 6535 n-nitrosodiphenylamine 6550 n-nitrosomethylethalamine 6555 n-nitrosomorpholine 6560 n-nitrosopiperidine 6565 n-nitrosopyrrolidine 5620 p-benzoquinone (Quinone) 6590 Pentachlorobenzene 6600 Pentachloronitrobenzene 6605 Pentachlorophenol 6610 Phenacetin 6615 Phenanthrene 6625 Phenol 6640 Phthalic anhydride 6650 Pronamide (Kerb) 6660 Propylthiouracil 6665 Pyrene 5095 Pyridine 6680 Resorcinol 6685 Safrole 6695 Strychnine 6750 Thiophenol (Benzenethiol) ,1'-Biphenyl (BZ-0) ,2,4,5-Tetrachlorobenzene Semivolatile Organic compounds by GC/MS Selective Ion Monitoring 44 of 75

46 4735 1,4-Dioxane (1,4- Diethyleneoxide) Non- Potable EPA 8270C SIM Methylnaphthalene Chloronaphthalene Methylaniline (o-toluidine) Methylnaphthalene & 4 Methylphenol ,4'-DDD ,4'-DDE ,4'-DDT 5500 Acenaphthene 5505 Acenaphthylene 7025 Aldrin 7110 alpha-bhc (alpha- Hexachlorocyclohexane) 7240 alpha-chlordane 5555 Anthracene 5595 Benzidine 5575 Benzo(a)anthracene 5580 Benzo(a)pyrene 5605 Benzo(e)pyrene 5590 Benzo(g,h,i)perylene 9309 Benzo(j)fluoranthene 5600 Benzo(k)fluoranthene 5585 Benzo[b]fluoranthene 7115 beta-bhc (beta- Hexachlorocyclohexane) 5670 Butyl benzyl phthalate 5680 Carbazole 7250 Chlordane (tech.) 5855 Chrysene 7105 delta-bhc 6065 Di(2-ethylhexyl) phthalate (bis(2- Ethylhexyl)phthalate, DEHP) 5895 Dibenz(a,h) anthracene 5905 Dibenzofuran 5910 Dibenzothiophene 7470 Dieldrin 6070 Diethyl phthalate 9375 Di-isopropylether (DIPE) 6135 Dimethyl phthalate 5925 Di-n-butyl phthalate 6200 Di-n-octyl phthalate 7510 Endosulfan I 7515 Endosulfan II 45 of 75