ANALYTICAL REPORT. Attn: Gunars Zikmanis

Transcription

1 ANALYTICAL REPORT TestAmerica Laboratories, Inc. Shuffel Street NW North Canton, OH Tel: ()- TestAmerica Job ID: -- Client Project/Site: TNEER- For: Ohio EPA-NEDO East Aurora Road Twinsburg, Ohio Attn: Gunars Zikmanis Authorized for release by: // :: PM Denise Pohl Project Manager II This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory.

2 Client: Ohio EPA-NEDO Project/Site: TNEER- Table of Contents TestAmerica Job ID: -- Cover Page Table of Contents Definitions/Glossary Case Narrative Method Summary Sample Summary Detection Summary Client Sample Results Surrogate Summary QC Sample Results QC Association Summary Lab Chronicle Certification Summary Chain of Custody Page of //

3 Client: Ohio EPA-NEDO Project/Site: TNEER- Qualifiers GC/MS VOA Qualifier J B Qualifier Description Indicates the analyte was analyzed for but not detected. Definitions/Glossary Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. Compound was found in the blank and sample. TestAmerica Job ID: -- MS, MSD: The analyte present in the original sample is times greater than the matrix spike concentration; therefore, control limits are not F GC/MS Semi VOA Qualifier X applicable. RPD of the MS and MSD exceeds the control limits Qualifier Description Indicates the analyte was analyzed for but not detected. Surrogate is outside control limits * LCS or LCSD exceeds the control limits F J F GC Semi VOA Qualifier MS or MSD exceeds the control limits Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. RPD of the MS and MSD exceeds the control limits Qualifier Description Indicates the analyte was analyzed for but not detected. MS, MSD: The analyte present in the original sample is times greater than the matrix spike concentration; therefore, control limits are not Metals Qualifier B F J applicable. Qualifier Description Compound was found in the blank and sample. MS or MSD exceeds the control limits Indicates the analyte was analyzed for but not detected. Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. General Chemistry Qualifier Qualifier Description F MS or MSD exceeds the control limits Indicates the analyte was analyzed for but not detected. Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference) DL, RA, RE, IN Indicates a Dilution, Reanalysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration EDL Estimated Detection Limit EPA nited States Environmental Protection Agency MDA imum detectable activity MDC imum detectable concentration MDL Method Detection Limit ML imum Level (Dioxin) ND Not detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry) Page of //

4 Client: Ohio EPA-NEDO Project/Site: TNEER- Glossary (Continued) Abbreviation RPD TEF TEQ Definitions/Glossary These commonly used abbreviations may or may not be present in this report. Relative Percent Difference, a measure of the relative difference between two points Toxicity Equivalent Factor (Dioxin) Toxicity Equivalent Quotient (Dioxin) TestAmerica Job ID: -- Page of //

5 Case Narrative Client: Ohio EPA-NEDO TestAmerica Job ID: -- Project/Site: TNEER- Job ID: -- Laboratory: Narrative CASE NARRATIVE Client: Ohio EPA-NEDO Project: TNEER- Report Number: -- With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required. attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmerica s operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below. The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory. Calculations are performed before rounding to avoid round-off errors in calculated results. All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below. All solid sample results are reported on an "as received" basis unless otherwise indicated by the presence of a % solids value in the method header. Requested chromatograms for organics can be found in front of the Chain of Custody section in the report. Internal chain of custody documentation of the // transfer of sample extracts to GC Semivolatiles and MS Semivolatiles was not recorded when the container transfer was made. The electronic record was updated on the following business day. This laboratory report is confidential and is intended for the sole use of TestAmerica and its client. RECEIPT The samples were received on //; the samples arrived in good condition, properly preserved and on ice. The temperature of the cooler at receipt was. C. Labels for the water layers of samples on samples WFR- and SJO- were initially applied to the incorrect containers. Labels were switched to match the client ID with the laboratory sample ID prior to finalizing the analytical report. WFR- (water phase) is reported as sample and SJO- (water phase) is reported as sample. In a // conference call with representatives of Ohio EPA, TestAmerica was asked to add analyses for VOCs and SVOCs on the water phase samples. VOLATILE ORGANIC COMPONDS (GC-MS) - Waste Samples - TANK G (OIL PHASE) (--), - CREEK (OIL PHASE) (--) and SJO- (OIL PHASE) (--) were analyzed for volatile organic compounds (GC-MS) in accordance with EPA SW- Method B. The samples were analyzed on //. Page of //

6 Case Narrative Client: Ohio EPA-NEDO TestAmerica Job ID: -- Project/Site: TNEER- Job ID: -- (Continued) Laboratory: (Continued) All samples were received in containers not stipulated in method B and received with headspace in the sample container. Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with batch.,,-trichlorobenzene was detected in method blank MB -/ at the reporting limit. If the associated sample reported a result above the MDL and/or RL, the result has been B flagged. Methylcyclohexane was detected in method blank MB -/ at a level that was above the method detection limit but below the reporting limit. The value should be considered an estimate, and has been flagged J. If the associated sample reported a result above the MDL and/or RL, the result has been B flagged. Refer to the QC report for details.,,,-tetrachloroethane exceeded the rpd limit for the MSD of sample SJO- (OIL PHASE)MSD (--) in batch -. The presence of the '' qualifier in the data indicates analytes where the concentration in the unspiked sample exceeded four times the spiking amount. No difficulties were encountered during the VOCs analyses. All quality control parameters were within the acceptance limits. VOLATILE ORGANIC COMPONDS (GC-MS) - Water Samples - TANK G (WATER PHASE) (--), - CREEK (WATER PHASE) (--), WFR- (WATER PHASE) (--) and SJO- (WATER PHASE) (--) were analyzed for volatile organic compounds (GC-MS) in accordance with EPA SW- Method B. The samples were analyzed on //. All samples were received in containers not stipulated in method B and received with headspace in the sample container. Samples were received at a ph >. The following sample(s) was diluted due to the abundance of non-target analytes: - CREEK (WATER PHASE) (--). Elevated reporting limits (RLs) are provided. Samples - TANK G (WATER PHASE) (--)[X], - CREEK (WATER PHASE) (--)[X], WFR- (WATER PHASE) (--)[X] and SJO- (WATER PHASE) (--)[X] required dilution prior to analysis. The reporting limits have been adjusted accordingly. No other difficulties were encountered during the VOCs analyses. All other quality control parameters were within the acceptance limits. SEMIVOLATILE ORGANIC COMPONDS (GC-MS) - Waste Samples - TANK G (OIL PHASE) (--), - CREEK (OIL PHASE) (--) and SJO- (OIL PHASE) (--) were analyzed for semivolatile organic compounds (GC-MS) in accordance with EPA SW- Method C. The samples were prepared on // and analyzed on //. SJO- (OIL PHASE) (--) was received in a container not stipulated in method C. Surrogates are added during the extraction process prior to dilution. When the sample is diluted, surrogate recoveries are diluted out and no corrective action is required. Samples - TANK G (OIL PHASE) (--)[X], (-- MS), (-- MSD), - CREEK (OIL PHASE) (--)[X] and SJO- (OIL PHASE) (--)[X] required dilution prior to analysis. The reporting limits have been adjusted accordingly.,,-tribromophenol (Surr) and Nitrobenzene-d (Surr) failed the surrogate recovery criteria low for - TANK G (OIL PHASE) (--). -Fluorobiphenyl (Surr) failed the surrogate recovery criteria high.,,-tribromophenol (Surr), -Fluorophenol (Surr) and Nitrobenzene-d (Surr) failed the surrogate recovery criteria low for - CREEK (OIL PHASE) (--). -Fluorobiphenyl (Surr) and Terphenyl-d (Surr) failed the surrogate recovery Page of //

7 Case Narrative Client: Ohio EPA-NEDO TestAmerica Job ID: -- Project/Site: TNEER- Job ID: -- (Continued) Laboratory: (Continued) criteria high.,,-tribromophenol (Surr) and Nitrobenzene-d (Surr) failed the surrogate recovery criteria low for SJO- (OIL PHASE) (--). -Fluorobiphenyl (Surr) failed the surrogate recovery criteria high.,,-tribromophenol (Surr) and Nitrobenzene-d (Surr) failed the surrogate recovery criteria low for - TANK G (OIL PHASE)MS (--MS).,,-Tribromophenol (Surr) and Nitrobenzene-d (Surr) failed the surrogate recovery criteria low for - TANK G (OIL PHASE)MSD (--MSD). The laboratory control sample (LCS) for batch exceeded control limits for the following analytes: Atrazine. This analyte was biased high in the LCS and was not detected in the associated samples; therefore, the data has been reported. For the MSD of sample - TANK G (OIL PHASE) MSD (--) in batch -, Several analytes failed the recovery criteria low. Several analytes failed the recovery criteria high. Also, -Methylnaphthalene, Acenaphthene and Hexachlorobutadiene exceeded the rpd limit. No other difficulties were encountered during the SVOCs analyses. All other quality control parameters were within the acceptance limits. SEMIVOLATILE ORGANIC COMPONDS (GC-MS) - Water Samples - TANK G (WATER PHASE) (--), - CREEK (WATER PHASE) (--), WFR- (WATER PHASE) (--) and SJO- (WATER PHASE) (--) were analyzed for semivolatile organic compounds (GC-MS) in accordance with EPA SW- Method C. The samples were prepared on // and analyzed on //. - CREEK (WATER PHASE) (--), WFR- (WATER PHASE) (--) and SJO- (WATER PHASE) (--) were received in containers not stipulated in method C. For multiphasic samples, the aqueous phase was separated from the oil phase by a combination of separatory funnel and centrifuge. Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with batch. Surrogates are added during the extraction process prior to dilution. When the sample is diluted, surrogate recoveries are diluted out and no corrective action is required. Samples - TANK G (WATER PHASE) (--)[X], - CREEK (WATER PHASE) (--)[X], WFR- (WATER PHASE) (--)[X] and SJO- (WATER PHASE) (--)[X] required dilution prior to analysis. The reporting limits have been adjusted accordingly.,,-tribromophenol (Surr) and Nitrobenzene-d (Surr) failed the surrogate recovery criteria low for - TANK G (WATER PHASE) (--). Refer to the QC report for details. No other difficulties were encountered during the SVOCs analyses. All other quality control parameters were within the acceptance limits. DIESEL RANGE ORGANICS (DRO) - Waste Samples - TANK G (OIL PHASE) (--), - CREEK (OIL PHASE) (--) and SJO- (OIL PHASE) (--) were analyzed for diesel range organics (DRO) in accordance with EPA SW- Method B - DRO. The samples were prepared on // and analyzed on //. SJO- (OIL PHASE) (--) was received in a container not stipulated in method B. Diesel Range Organics [C - C] failed the recovery criteria low for the MS of sample - TANK G (OIL PHASE)MS (--) in batch -. Diesel Range Organics [C - C] failed the recovery criteria high for the MSD of sample - TANK G (OIL PHASE)MSD Page of //

8 Case Narrative Client: Ohio EPA-NEDO TestAmerica Job ID: -- Project/Site: TNEER- Job ID: -- (Continued) Laboratory: (Continued) (--) in batch -. Samples - TANK G (OIL PHASE) (--)[X], - CREEK (OIL PHASE) (--)[X] and SJO- (OIL PHASE) (--)[X] required dilution prior to analysis. The reporting limits have been adjusted accordingly. No other difficulties were encountered during the DRO analyses. All other quality control parameters were within the acceptance limits. TOTAL METALS IN WASTE (ICP) - Waste Samples - TANK G (OIL PHASE) (--), - CREEK (OIL PHASE) (--), WFR- (OIL PHASE) (--) and SJO- (OIL PHASE) (--) were analyzed for total metals in waste (ICP) in accordance with EPA SW- Method B. The samples were prepared on // and analyzed on //. Calcium, Magnesium and Tin were detected in method blank MB -/-A at levels that were above the method detection limit but below the reporting limit. The values should be considered estimates, and have been flagged J. If the associated sample reported a result above the MDL and/or RL, the result has been B flagged. Refer to the QC report for details. Sample SJO- (OIL PHASE) (--)[X] required dilution for Barium prior to analysis. The reporting limits have been adjusted accordingly. No other difficulties were encountered during the metals analyses. All other quality control parameters were within the acceptance limits. TOTAL RECOVERABLE METALS (ICP) - Water Samples WFR- (WATER PHASE) (--) and SJO- (WATER PHASE) (--) were analyzed for total recoverable metals (ICP) in accordance with EPA SW- Method B. The samples were prepared on // and analyzed on //. Two separate phases were logged for samples WFR- (WATER PHASE) (--) and SJO- (WATER PHASE) (--). The water phase for each sample was obtained by pipetting the water layer off of the bottom of the container. The water layer was preserved to a ph < with Nitric Acid. Barium, Calcium and Magnesium were detected in method blank MB -/-A at levels that were above the method detection limit but below the reporting limit. The values should be considered estimates, and have been flagged J. If the associated sample reported a result above the MDL and/or RL, the result has been B flagged. Refer to the QC report for details. Samples WFR- (WATER PHASE) (--) and SJO- (WATER PHASE) (--) required multiple dilutions in order to report the list of elements: X, X, X, and X. The reporting limits have been adjusted accordingly. No other difficulties were encountered during the metals analyses. All other quality control parameters were within the acceptance limits. TOTAL MERCRY - Waste Samples - TANK G (OIL PHASE) (--), - CREEK (OIL PHASE) (--), WFR- (OIL PHASE) (--) and SJO- (OIL PHASE) (--) were analyzed for total mercury in accordance with EPA SW- Method A. The samples were prepared and analyzed on //. Mercury was detected in method blank MB -/-A at a level that was above the method detection limit but below the reporting limit. The value should be considered an estimate, and has been flagged J. If the associated sample reported a result above the MDL and/or RL, the result has been B flagged. Refer to the QC report for details. Mercury failed the recovery criteria high for the MSD of sample -- in batch -. No other difficulties were encountered during the mercury analyses. All other quality control parameters were within the acceptance limits. TOTAL MERCRY - Water Samples WFR- (WATER PHASE) (--) and SJO- (WATER PHASE) (--) were analyzed for total mercury in accordance with EPA SW- Methods A. The samples were prepared and analyzed on //. Page of //

9 Case Narrative Client: Ohio EPA-NEDO TestAmerica Job ID: -- Project/Site: TNEER- Job ID: -- (Continued) Laboratory: (Continued) Two separate phases were logged for samples WFR- (WATER PHASE) (--) and SJO- (WATER PHASE) (--). The water phase for each sample was obtained by pipetting the water layer off of the bottom of the container. The water layer was preserved to a ph < with Nitric Acid. Mercury failed the recovery criteria low for the MS of sample -- in batch -. Mercury failed the recovery criteria low for the MSD of sample -- in batch -. No other difficulties were encountered during the mercury analyses. All other quality control parameters were within the acceptance limits. ANIONS - Water Samples - TANK G (WATER PHASE) (--), - CREEK (WATER PHASE) (--), WFR- (WATER PHASE) (--) and SJO- (WATER PHASE) (--) were analyzed for anions in accordance with EPA SW- Method A. The samples were analyzed on // and //. Chloride failed the recovery criteria high for the MS of sample -- in batch -. Samples - TANK G (WATER PHASE) (--)[X], - CREEK (WATER PHASE) (--)[X], WFR- (WATER PHASE) (--)[X] and SJO- (WATER PHASE) (--)[X] required dilution prior to analysis. The reporting limits have been adjusted accordingly. No other difficulties were encountered during the anions analyses. All other quality control parameters were within the acceptance limits. Page of //

10 Client: Ohio EPA-NEDO Project/Site: TNEER- Method Summary TestAmerica Job ID: -- Method Method Description Protocol Laboratory B Volatile Organic Compounds (GC/MS) SW TAL NC C Semivolatile Organic Compounds (GC/MS) SW TAL NC B Diesel Range Organics (DRO) (GC) SW TAL NC B Metals (ICP) SW TAL NC A Mercury (CVAA) SW TAL NC A Mercury (CVAA) SW TAL NC A Anions, Ion Chromatography SW TAL NC Protocol References: SW = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November And Its pdates. Laboratory References: TAL NC =, Shuffel Street NW, North Canton, OH, TEL ()- Page of //

11 Client: Ohio EPA-NEDO Project/Site: TNEER- Sample Summary TestAmerica Job ID: -- Lab Sample ID Client Sample ID Matrix Collected Received -- - TANK G (OIL PHASE) Waste // : // : -- - TANK G (WATER PHASE) Water // : // : -- - CREEK (OIL PHASE) Waste // : // : -- - CREEK (WATER PHASE) Water // : // : -- WFR- (OIL PHASE) Waste // : // : -- SJO- (OIL PHASE) Waste // : // : -- WFR- (WATER PHASE) Water // : // : -- SJO- (WATER PHASE) Water // : // : Page of //

12 Client: Ohio EPA-NEDO Project/Site: TNEER- Detection Summary TestAmerica Job ID: -- Client Sample ID: - TANK G (OIL PHASE) Lab Sample ID: -- Analyte Result Qualifier RL MDL nit Dil Fac D Method Prep Type Benzene J ug/kg B Ethylbenzene J. ug/kg B Methylene Chloride J ug/kg B Tetrachloroethene J ug/kg B Toluene ug/kg B Xylenes, Total ug/kg B Cyclohexane J ug/kg B Isopropylbenzene J. ug/kg B Methyl acetate ug/kg B Methylcyclohexane ug/kg B C-C mg/kg B Arsenic. J.. mg/kg B Barium. mg/kg B Calcium B mg/kg B Chromium. J.. mg/kg B Lead... mg/kg B Magnesium J B. mg/kg B Potassium J. mg/kg B Strontium.. mg/kg B Tin. J B.. mg/kg B Client Sample ID: - TANK G (WATER PHASE) Lab Sample ID: -- Analyte Result Qualifier RL MDL nit Dil Fac D Method Prep Type Acetone. ug/l B Benzene... ug/l B -Butanone (MEK) J. ug/l B -Hexanone. J. ug/l B Methylcyclohexane. J B.. ug/l B Toluene... ug/l B Xylenes, Total. J.. ug/l B Chloride mg/l A Client Sample ID: - CREEK (OIL PHASE) Lab Sample ID: -- Analyte Result Qualifier RL MDL nit Dil Fac D Method Prep Type Acetone J ug/kg B Benzene J ug/kg B Ethylbenzene J. ug/kg B Tetrachloroethene J ug/kg B Toluene ug/kg B Xylenes, Total ug/kg B Cyclohexane J ug/kg B Isopropylbenzene J. ug/kg B Methyl acetate ug/kg B Methylcyclohexane ug/kg B C-C mg/kg B Arsenic. J.. mg/kg B Barium. mg/kg B Calcium B mg/kg B This Detection Summary does not include radiochemical test results. Page of //

13 Client: Ohio EPA-NEDO Project/Site: TNEER- Detection Summary TestAmerica Job ID: -- Client Sample ID: - CREEK (OIL PHASE) (Continued) Lab Sample ID: -- Analyte Result Qualifier RL MDL nit Dil Fac D Method Prep Type Chromium. J.. mg/kg B Lead... mg/kg B Magnesium J B. mg/kg B Potassium J. mg/kg B Strontium.. mg/kg B Tin. J B.. mg/kg B Mercury. J B.. mg/kg A Client Sample ID: - CREEK (WATER PHASE) Lab Sample ID: -- Analyte Result Qualifier RL MDL nit Dil Fac D Method Prep Type Acetone. ug/l B Benzene. J.. ug/l B -Butanone (MEK) J. ug/l B -Hexanone. J. ug/l B Toluene... ug/l B Xylenes, Total. J.. ug/l B Chloride. mg/l A Client Sample ID: WFR- (OIL PHASE) Lab Sample ID: -- Analyte Result Qualifier RL MDL nit Dil Fac D Method Prep Type Arsenic. J.. mg/kg B Barium. mg/kg B Calcium B mg/kg B Chromium. J.. mg/kg B Lead... mg/kg B Magnesium J B. mg/kg B Potassium J. mg/kg B Sodium J mg/kg B Strontium.. mg/kg B Tin. J B.. mg/kg B Mercury. J B.. mg/kg A Client Sample ID: SJO- (OIL PHASE) Lab Sample ID: -- Analyte Result Qualifier RL MDL nit Dil Fac D Method Prep Type Benzene ug/kg B Ethylbenzene. ug/kg B Tetrachloroethene ug/kg B Toluene ug/kg B Xylenes, Total ug/kg B Cyclohexane ug/kg B Isopropylbenzene J. ug/kg B Methyl acetate ug/kg B Methylcyclohexane ug/kg B C-C mg/kg B Arsenic... mg/kg B Barium. mg/kg B Calcium B mg/kg B This Detection Summary does not include radiochemical test results. Page of //

14 Client: Ohio EPA-NEDO Project/Site: TNEER- Detection Summary TestAmerica Job ID: -- Client Sample ID: SJO- (OIL PHASE) (Continued) Lab Sample ID: -- Analyte Result Qualifier RL MDL nit Dil Fac D Method Prep Type Chromium... mg/kg B Lead.. mg/kg B Magnesium J B. mg/kg B Potassium J. mg/kg B Sodium J mg/kg B Strontium.. mg/kg B Tin. J B.. mg/kg B Client Sample ID: WFR- (WATER PHASE) Lab Sample ID: -- Analyte Result Qualifier RL MDL nit Dil Fac D Method Prep Type Acetone. ug/l B Benzene... ug/l B -Butanone (MEK) J. ug/l B -Hexanone. J. ug/l B Methylcyclohexane. J B.. ug/l B Methylene Chloride.. ug/l B Toluene... ug/l B Xylenes, Total. J.. ug/l B Arsenic J ug/l B Total Recoverable Barium B. ug/l B Total Recoverable Calcium B ug/l B Total Recoverable Chromium ug/l B Total Recoverable Lead. ug/l B Total Recoverable Magnesium B ug/l B Total Recoverable Potassium ug/l B Total Recoverable Sodium ug/l B Total Recoverable Strontium ug/l B Total Recoverable Mercury... ug/l A Chloride mg/l A Client Sample ID: SJO- (WATER PHASE) Lab Sample ID: -- Analyte Result Qualifier RL MDL nit Dil Fac D Method Prep Type Acetone. ug/l B Benzene.. ug/l B -Butanone (MEK) J. ug/l B Cyclohexane. J.. ug/l B -Hexanone. J. ug/l B Toluene.. ug/l B Xylenes, Total. J.. ug/l B Arsenic J ug/l B Total Recoverable This Detection Summary does not include radiochemical test results. Page of //

15 Client: Ohio EPA-NEDO Project/Site: TNEER- Detection Summary TestAmerica Job ID: -- Client Sample ID: SJO- (WATER PHASE) (Continued) Lab Sample ID: -- Analyte Result Qualifier RL MDL nit Dil Fac D Method Prep Type Barium B. ug/l B Total Recoverable Calcium B ug/l B Total Recoverable Chromium ug/l B Total Recoverable Lead. ug/l B Total Recoverable Magnesium B ug/l B Total Recoverable Potassium ug/l B Total Recoverable Sodium ug/l B Total Recoverable Strontium ug/l B Total Recoverable Mercury... ug/l A Chloride mg/l A This Detection Summary does not include radiochemical test results. Page of //

16 Client: Ohio EPA-NEDO Project/Site: TNEER- Client Sample Results TestAmerica Job ID: -- Client Sample ID: - TANK G (OIL PHASE) Date Collected: // : Date Received: // : Lab Sample ID: -- Matrix: Waste Method: B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL nit D Prepared Analyzed Dil Fac Acetone ug/kg // : // : Benzene J ug/kg // : // : Dichlorobromomethane ug/kg // : // : Bromoform ug/kg // : // : Bromomethane ug/kg // : // : -Butanone (MEK) ug/kg // : // : Carbon disulfide ug/kg // : // : Carbon tetrachloride. ug/kg // : // : Chlorobenzene. ug/kg // : // : Chloroethane ug/kg // : // : Chloroform ug/kg // : // : Chloromethane ug/kg // : // :,-Dichloroethane ug/kg // : // :,-Dichloroethane ug/kg // : // :,-Dichloroethene ug/kg // : // :,-Dichloropropane ug/kg // : // : cis-,-dichloropropene ug/kg // : // : trans-,-dichloropropene ug/kg // : // : Ethylbenzene J. ug/kg // : // : -Hexanone ug/kg // : // : Methylene Chloride J ug/kg // : // : -Methyl--pentanone (MIBK) ug/kg // : // : Styrene. ug/kg // : // :,,,-Tetrachloroethane ug/kg // : // : Tetrachloroethene J ug/kg // : // : Toluene ug/kg // : // : Trichloroethene ug/kg // : // : Vinyl chloride ug/kg // : // : Xylenes, Total ug/kg // : // :,,-Trichloroethane ug/kg // : // :,,-Trichloroethane ug/kg // : // : Cyclohexane J ug/kg // : // :,-Dibromo--Chloropropane ug/kg // : // : Ethylene Dibromide ug/kg // : // : Dichlorodifluoromethane ug/kg // : // : cis-,-dichloroethene. ug/kg // : // : trans-,-dichloroethene ug/kg // : // : Isopropylbenzene J. ug/kg // : // : Methyl acetate ug/kg // : // : Methyl tert-butyl ether. ug/kg // : // :,,-Trichloro-,,-trifluoroethane ug/kg // : // :,,-Trichlorobenzene. ug/kg // : // :,-Dichlorobenzene ug/kg // : // :,-Dichlorobenzene. ug/kg // : // :,-Dichlorobenzene ug/kg // : // : Trichlorofluoromethane ug/kg // : // : Chlorodibromomethane ug/kg // : // : Methylcyclohexane ug/kg // : // : Page of //

17 Client: Ohio EPA-NEDO Project/Site: TNEER- Client Sample Results TestAmerica Job ID: -- Client Sample ID: - TANK G (OIL PHASE) Date Collected: // : Date Received: // : Lab Sample ID: -- Matrix: Waste Surrogate %Recovery Qualifier Limits Prepared Analyzed,-Dichloroethane-d (Surr) - // : // : -Bromofluorobenzene (Surr) - // : // : Toluene-d (Surr) - // : // : Dibromofluoromethane (Surr) - // : // : Method: C - Semivolatile Organic Compounds (GC/MS) Analyte Result Qualifier RL,'-Biphenyl ug/kg // : // : bis (-chloroisopropyl) ether,,-trichlorophenol,,-trichlorophenol,-dichlorophenol,-dimethylphenol,-dinitrophenol,-dinitrotoluene,-dinitrotoluene -Chloronaphthalene -Chlorophenol -Methylnaphthalene -Methylphenol -Nitroaniline -Nitrophenol,'-Dichlorobenzidine -Nitroaniline,-Dinitro--methylphenol -Bromophenyl phenyl ether -Chloro--methylphenol -Chloroaniline -Chlorophenyl phenyl ether -Nitroaniline -Nitrophenol Acenaphthene Acenaphthylene Acetophenone Anthracene Atrazine * Benzaldehyde Benzo[a]anthracene Benzo[a]pyrene Benzo[b]fluoranthene Benzo[g,h,i]perylene Benzo[k]fluoranthene Bis(-chloroethoxy)methane Bis(-chloroethyl)ether Bis(-ethylhexyl) phthalate Butyl benzyl phthalate Caprolactam Carbazole Chrysene Dibenz(a,h)anthracene MDL nit D Prepared Analyzed Dil Fac Dil Fac ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : Page of //

18 Client: Ohio EPA-NEDO Project/Site: TNEER- Client Sample Results TestAmerica Job ID: -- Client Sample ID: - TANK G (OIL PHASE) Date Collected: // : Date Received: // : Method: C - Semivolatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Lab Sample ID: -- Matrix: Waste Prepared Analyzed Dibenzofuran ug/kg // : // : Diethyl phthalate Dimethyl phthalate Di-n-butyl phthalate Di-n-octyl phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno[,,-cd]pyrene Isophorone Naphthalene Nitrobenzene N-Nitrosodi-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Phenanthrene Pyrene & Methylphenol nit D Dil Fac ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : Surrogate %Recovery Qualifier Limits Prepared Analyzed -Fluorobiphenyl (Surr) X - // : // : -Fluorophenol (Surr) - // : // :,,-Tribromophenol (Surr) X - // : // : Nitrobenzene-d (Surr) X - // : // : Phenol-d (Surr) - // : // : Terphenyl-d (Surr) - // : // : Dil Fac Method: B - Diesel Range Organics (DRO) (GC) Analyte Result Qualifier RL MDL nit D Prepared Analyzed Dil Fac C-C mg/kg // : // : C-C mg/kg // : // : Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac n-nonane - // : // : Method: B - Metals (ICP) Analyte Result Qualifier RL MDL nit D Prepared Analyzed Dil Fac Arsenic. J.. mg/kg // : // : Barium. mg/kg // : // : Cadmium... mg/kg // : // : Calcium B mg/kg // : // : Chromium. J.. mg/kg // : // : Lead... mg/kg // : // : Magnesium J B. mg/kg // : // : Potassium J. mg/kg // : // : Selenium... mg/kg // : // : Page of //

19 Client: Ohio EPA-NEDO Project/Site: TNEER- Client Sample Results TestAmerica Job ID: -- Client Sample ID: - TANK G (OIL PHASE) Date Collected: // : Date Received: // : Method: B - Metals (ICP) (Continued) Analyte Result Qualifier RL MDL Lab Sample ID: -- Matrix: Waste Prepared Analyzed Silver... mg/kg // : // : Sodium Strontium Tin Method: A - Mercury (CVAA) Analyte Result. J B Qualifier nit D Dil Fac mg/kg // : // :.. mg/kg // : // :.. mg/kg // : // : RL Mercury... mg/kg // : // : MDL nit D Prepared Analyzed Dil Fac Page of //

20 Client: Ohio EPA-NEDO Project/Site: TNEER- Client Sample Results TestAmerica Job ID: -- Client Sample ID: - TANK G (WATER PHASE) Date Collected: // : Date Received: // : Lab Sample ID: -- Matrix: Water Method: B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL nit D Prepared Analyzed Dil Fac Acetone. ug/l // : Benzene... ug/l // : Bromoform... ug/l // : Bromomethane... ug/l // : -Butanone (MEK) J. ug/l // : Carbon disulfide... ug/l // : Carbon tetrachloride... ug/l // : Chlorobenzene... ug/l // : Chlorodibromomethane... ug/l // : Chloroethane... ug/l // : Chloroform... ug/l // : Chloromethane... ug/l // : cis-,-dichloroethene... ug/l // : cis-,-dichloropropene... ug/l // : Cyclohexane... ug/l // :,-Dibromo--Chloropropane... ug/l // :,-Dichlorobenzene... ug/l // :,-Dichlorobenzene... ug/l // :,-Dichlorobenzene... ug/l // : Dichlorobromomethane... ug/l // : Dichlorodifluoromethane... ug/l // :,-Dichloroethane... ug/l // :,-Dichloroethane... ug/l // :,-Dichloroethene... ug/l // :,-Dichloropropane... ug/l // : Ethylbenzene... ug/l // : Ethylene Dibromide... ug/l // : -Hexanone. J. ug/l // : Isopropylbenzene... ug/l // : Methyl acetate. ug/l // : Methylcyclohexane. J B.. ug/l // : Methylene Chloride... ug/l // : -Methyl--pentanone (MIBK). ug/l // : Methyl tert-butyl ether. ug/l // : Styrene... ug/l // :,,,-Tetrachloroethane... ug/l // : Tetrachloroethene... ug/l // : Toluene... ug/l // : trans-,-dichloroethene... ug/l // : trans-,-dichloropropene... ug/l // :,,-Trichlorobenzene... ug/l // :,,-Trichloroethane... ug/l // :,,-Trichloroethane... ug/l // : Trichloroethene... ug/l // : Trichlorofluoromethane... ug/l // :,,-Trichloro-,,-trifluoroethane... ug/l // : Vinyl chloride... ug/l // : Xylenes, Total. J.. ug/l // : Page of //

21 Client: Ohio EPA-NEDO Project/Site: TNEER- Client Sample Results TestAmerica Job ID: -- Client Sample ID: - TANK G (WATER PHASE) Date Collected: // : Date Received: // : Lab Sample ID: -- Matrix: Water Surrogate %Recovery Qualifier Limits Prepared Analyzed -Bromofluorobenzene (Surr) - // : Dibromofluoromethane (Surr) - // :,-Dichloroethane-d (Surr) - // : Toluene-d (Surr) - // : Method: C - Semivolatile Organic Compounds (GC/MS) Analyte Result Qualifier RL Acenaphthene ug/l // : // : Acenaphthylene Acetophenone Anthracene Atrazine Benzaldehyde Benzo[a]anthracene Benzo[a]pyrene Benzo[b]fluoranthene Benzo[g,h,i]perylene Benzo[k]fluoranthene,'-Biphenyl Bis(-chloroethoxy)methane Bis(-chloroethyl)ether bis (-chloroisopropyl) ether Bis(-ethylhexyl) phthalate -Bromophenyl phenyl ether Butyl benzyl phthalate Caprolactam Carbazole -Chloroaniline -Chloro--methylphenol -Chloronaphthalene -Chlorophenol -Chlorophenyl phenyl ether Chrysene Dibenz(a,h)anthracene Dibenzofuran,'-Dichlorobenzidine,-Dichlorophenol Diethyl phthalate,-dimethylphenol Dimethyl phthalate Di-n-butyl phthalate,-dinitro--methylphenol,-dinitrophenol,-dinitrotoluene,-dinitrotoluene Di-n-octyl phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene MDL nit D Prepared Analyzed Dil Fac Dil Fac ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : Page of //

22 Client: Ohio EPA-NEDO Project/Site: TNEER- Client Sample Results TestAmerica Job ID: -- Client Sample ID: - TANK G (WATER PHASE) Date Collected: // : Date Received: // : Method: C - Semivolatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Lab Sample ID: -- Matrix: Water Prepared Analyzed Hexachlorocyclopentadiene ug/l // : // : Hexachloroethane Indeno[,,-cd]pyrene Isophorone -Methylnaphthalene -Methylphenol & Methylphenol Naphthalene -Nitroaniline -Nitroaniline -Nitroaniline Nitrobenzene -Nitrophenol -Nitrophenol N-Nitrosodi-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene,,-Trichlorophenol,,-Trichlorophenol nit D Dil Fac ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : Surrogate %Recovery Qualifier Limits Prepared Analyzed -Fluorobiphenyl (Surr) - // : // : -Fluorophenol (Surr) - // : // : Nitrobenzene-d (Surr) X - // : // : Phenol-d (Surr) - // : // : Terphenyl-d (Surr) - // : // :,,-Tribromophenol (Surr) X - // : // : Dil Fac General Chemistry Analyte Result Qualifier RL MDL nit D Prepared Analyzed Dil Fac Chloride mg/l // : Page of //

23 Client: Ohio EPA-NEDO Project/Site: TNEER- Client Sample Results TestAmerica Job ID: -- Client Sample ID: - CREEK (OIL PHASE) Date Collected: // : Date Received: // : Lab Sample ID: -- Matrix: Waste Method: B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL nit D Prepared Analyzed Dil Fac Acetone J ug/kg // : // : Benzene J ug/kg // : // : Dichlorobromomethane ug/kg // : // : Bromoform ug/kg // : // : Bromomethane ug/kg // : // : -Butanone (MEK) ug/kg // : // : Carbon disulfide ug/kg // : // : Carbon tetrachloride. ug/kg // : // : Chlorobenzene. ug/kg // : // : Chloroethane ug/kg // : // : Chloroform ug/kg // : // : Chloromethane ug/kg // : // :,-Dichloroethane ug/kg // : // :,-Dichloroethane ug/kg // : // :,-Dichloroethene ug/kg // : // :,-Dichloropropane ug/kg // : // : cis-,-dichloropropene. ug/kg // : // : trans-,-dichloropropene ug/kg // : // : Ethylbenzene J. ug/kg // : // : -Hexanone ug/kg // : // : Methylene Chloride ug/kg // : // : -Methyl--pentanone (MIBK) ug/kg // : // : Styrene. ug/kg // : // :,,,-Tetrachloroethane ug/kg // : // : Tetrachloroethene J ug/kg // : // : Toluene ug/kg // : // : Trichloroethene ug/kg // : // : Vinyl chloride ug/kg // : // : Xylenes, Total ug/kg // : // :,,-Trichloroethane ug/kg // : // :,,-Trichloroethane ug/kg // : // : Cyclohexane J ug/kg // : // :,-Dibromo--Chloropropane ug/kg // : // : Ethylene Dibromide ug/kg // : // : Dichlorodifluoromethane ug/kg // : // : cis-,-dichloroethene. ug/kg // : // : trans-,-dichloroethene ug/kg // : // : Isopropylbenzene J. ug/kg // : // : Methyl acetate ug/kg // : // : Methyl tert-butyl ether. ug/kg // : // :,,-Trichloro-,,-trifluoroethane ug/kg // : // :,,-Trichlorobenzene. ug/kg // : // :,-Dichlorobenzene ug/kg // : // :,-Dichlorobenzene. ug/kg // : // :,-Dichlorobenzene ug/kg // : // : Trichlorofluoromethane ug/kg // : // : Chlorodibromomethane ug/kg // : // : Methylcyclohexane ug/kg // : // : Page of //

24 Client: Ohio EPA-NEDO Project/Site: TNEER- Client Sample Results TestAmerica Job ID: -- Client Sample ID: - CREEK (OIL PHASE) Date Collected: // : Date Received: // : Lab Sample ID: -- Matrix: Waste Surrogate %Recovery Qualifier Limits Prepared Analyzed,-Dichloroethane-d (Surr) - // : // : -Bromofluorobenzene (Surr) - // : // : Toluene-d (Surr) - // : // : Dibromofluoromethane (Surr) - // : // : Method: C - Semivolatile Organic Compounds (GC/MS) Analyte Result Qualifier RL,'-Biphenyl ug/kg // : // : bis (-chloroisopropyl) ether,,-trichlorophenol,,-trichlorophenol,-dichlorophenol,-dimethylphenol,-dinitrophenol,-dinitrotoluene,-dinitrotoluene -Chloronaphthalene -Chlorophenol -Methylnaphthalene -Methylphenol -Nitroaniline -Nitrophenol,'-Dichlorobenzidine -Nitroaniline,-Dinitro--methylphenol -Bromophenyl phenyl ether -Chloro--methylphenol -Chloroaniline -Chlorophenyl phenyl ether -Nitroaniline -Nitrophenol Acenaphthene Acenaphthylene Acetophenone Anthracene Atrazine * Benzaldehyde Benzo[a]anthracene Benzo[a]pyrene Benzo[b]fluoranthene Benzo[g,h,i]perylene Benzo[k]fluoranthene Bis(-chloroethoxy)methane Bis(-chloroethyl)ether Bis(-ethylhexyl) phthalate Butyl benzyl phthalate Caprolactam Carbazole Chrysene Dibenz(a,h)anthracene MDL nit D Prepared Analyzed Dil Fac Dil Fac ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : Page of //

25 Client: Ohio EPA-NEDO Project/Site: TNEER- Client Sample Results TestAmerica Job ID: -- Client Sample ID: - CREEK (OIL PHASE) Date Collected: // : Date Received: // : Method: C - Semivolatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Lab Sample ID: -- Matrix: Waste Prepared Analyzed Dibenzofuran ug/kg // : // : Diethyl phthalate Dimethyl phthalate Di-n-butyl phthalate Di-n-octyl phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno[,,-cd]pyrene Isophorone Naphthalene Nitrobenzene N-Nitrosodi-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenol Phenanthrene Pyrene & Methylphenol nit D Dil Fac ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : ug/kg // : // : Surrogate %Recovery Qualifier Limits Prepared Analyzed -Fluorobiphenyl (Surr) X - // : // : -Fluorophenol (Surr) X - // : // :,,-Tribromophenol (Surr) X - // : // : Nitrobenzene-d (Surr) X - // : // : Phenol-d (Surr) - // : // : Terphenyl-d (Surr) X - // : // : Dil Fac Method: B - Diesel Range Organics (DRO) (GC) Analyte Result Qualifier RL MDL nit D Prepared Analyzed Dil Fac C-C mg/kg // : // : C-C mg/kg // : // : Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac n-nonane - // : // : Method: B - Metals (ICP) Analyte Result Qualifier RL MDL nit D Prepared Analyzed Dil Fac Arsenic. J.. mg/kg // : // : Barium. mg/kg // : // : Cadmium... mg/kg // : // : Calcium B mg/kg // : // : Chromium. J.. mg/kg // : // : Lead... mg/kg // : // : Magnesium J B. mg/kg // : // : Potassium J. mg/kg // : // : Selenium... mg/kg // : // : Page of //

26 Client: Ohio EPA-NEDO Project/Site: TNEER- Client Sample Results TestAmerica Job ID: -- Client Sample ID: - CREEK (OIL PHASE) Date Collected: // : Date Received: // : Method: B - Metals (ICP) (Continued) Analyte Result Qualifier RL MDL Lab Sample ID: -- Matrix: Waste Prepared Analyzed Silver... mg/kg // : // : Sodium Strontium Tin Method: A - Mercury (CVAA) Analyte Result. J B Qualifier nit D Dil Fac mg/kg // : // :.. mg/kg // : // :.. mg/kg // : // : RL Mercury. J B.. mg/kg // : // : MDL nit D Prepared Analyzed Dil Fac Page of //

27 Client: Ohio EPA-NEDO Project/Site: TNEER- Client Sample Results TestAmerica Job ID: -- Client Sample ID: - CREEK (WATER PHASE) Date Collected: // : Date Received: // : Lab Sample ID: -- Matrix: Water Method: B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL nit D Prepared Analyzed Dil Fac Acetone. ug/l // : Benzene. J.. ug/l // : Bromoform... ug/l // : Bromomethane... ug/l // : -Butanone (MEK) J. ug/l // : Carbon disulfide... ug/l // : Carbon tetrachloride... ug/l // : Chlorobenzene... ug/l // : Chlorodibromomethane... ug/l // : Chloroethane... ug/l // : Chloroform... ug/l // : Chloromethane... ug/l // : cis-,-dichloroethene... ug/l // : cis-,-dichloropropene... ug/l // : Cyclohexane... ug/l // :,-Dibromo--Chloropropane... ug/l // :,-Dichlorobenzene... ug/l // :,-Dichlorobenzene... ug/l // :,-Dichlorobenzene... ug/l // : Dichlorobromomethane... ug/l // : Dichlorodifluoromethane... ug/l // :,-Dichloroethane... ug/l // :,-Dichloroethane... ug/l // :,-Dichloroethene... ug/l // :,-Dichloropropane... ug/l // : Ethylbenzene... ug/l // : Ethylene Dibromide... ug/l // : -Hexanone. J. ug/l // : Isopropylbenzene... ug/l // : Methyl acetate. ug/l // : Methylcyclohexane... ug/l // : Methylene Chloride... ug/l // : -Methyl--pentanone (MIBK). ug/l // : Methyl tert-butyl ether. ug/l // : Styrene... ug/l // :,,,-Tetrachloroethane... ug/l // : Tetrachloroethene... ug/l // : Toluene... ug/l // : trans-,-dichloroethene... ug/l // : trans-,-dichloropropene... ug/l // :,,-Trichlorobenzene... ug/l // :,,-Trichloroethane... ug/l // :,,-Trichloroethane... ug/l // : Trichloroethene... ug/l // : Trichlorofluoromethane... ug/l // :,,-Trichloro-,,-trifluoroethane... ug/l // : Vinyl chloride... ug/l // : Xylenes, Total. J.. ug/l // : Page of //

28 Client: Ohio EPA-NEDO Project/Site: TNEER- Client Sample Results TestAmerica Job ID: -- Client Sample ID: - CREEK (WATER PHASE) Date Collected: // : Date Received: // : Lab Sample ID: -- Matrix: Water Surrogate %Recovery Qualifier Limits Prepared Analyzed -Bromofluorobenzene (Surr) - // : Dibromofluoromethane (Surr) - // :,-Dichloroethane-d (Surr) - // : Toluene-d (Surr) - // : Method: C - Semivolatile Organic Compounds (GC/MS) Analyte Result Qualifier RL Acenaphthene. ug/l // : // : Acenaphthylene Acetophenone Anthracene Atrazine Benzaldehyde Benzo[a]anthracene Benzo[a]pyrene Benzo[b]fluoranthene Benzo[g,h,i]perylene Benzo[k]fluoranthene,'-Biphenyl Bis(-chloroethoxy)methane Bis(-chloroethyl)ether bis (-chloroisopropyl) ether Bis(-ethylhexyl) phthalate -Bromophenyl phenyl ether Butyl benzyl phthalate Caprolactam Carbazole -Chloroaniline -Chloro--methylphenol -Chloronaphthalene -Chlorophenol -Chlorophenyl phenyl ether Chrysene Dibenz(a,h)anthracene Dibenzofuran,'-Dichlorobenzidine,-Dichlorophenol Diethyl phthalate,-dimethylphenol Dimethyl phthalate Di-n-butyl phthalate,-dinitro--methylphenol,-dinitrophenol,-dinitrotoluene,-dinitrotoluene Di-n-octyl phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene MDL nit D Prepared Analyzed Dil Fac Dil Fac. ug/l // : // : ug/l // : // :. ug/l // : // : ug/l // : // : ug/l // : // :. ug/l // : // :. ug/l // : // :. ug/l // : // :. ug/l // : // :. ug/l // : // : ug/l // : // : ug/l // : // :. ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // :. ug/l // : // : ug/l // : // : ug/l // : // :. ug/l // : // :. ug/l // : // :. ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // :. ug/l // : // :. ug/l // : // :. ug/l // : // : ug/l // : // : Page of //

29 Client: Ohio EPA-NEDO Project/Site: TNEER- Client Sample Results TestAmerica Job ID: -- Client Sample ID: - CREEK (WATER PHASE) Date Collected: // : Date Received: // : Method: C - Semivolatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Lab Sample ID: -- Matrix: Water Prepared Analyzed Hexachlorocyclopentadiene ug/l // : // : Hexachloroethane Indeno[,,-cd]pyrene Isophorone -Methylnaphthalene -Methylphenol & Methylphenol Naphthalene -Nitroaniline -Nitroaniline -Nitroaniline Nitrobenzene -Nitrophenol -Nitrophenol N-Nitrosodi-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene,,-Trichlorophenol,,-Trichlorophenol nit D Dil Fac ug/l // : // :. ug/l // : // : ug/l // : // :. ug/l // : // : ug/l // : // : ug/l // : // :. ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // :. ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // : ug/l // : // :. ug/l // : // : ug/l // : // :. ug/l // : // : ug/l // : // : ug/l // : // : Surrogate %Recovery Qualifier Limits Prepared Analyzed -Fluorobiphenyl (Surr) - // : // : -Fluorophenol (Surr) - // : // : Nitrobenzene-d (Surr) - // : // : Phenol-d (Surr) - // : // : Terphenyl-d (Surr) - // : // :,,-Tribromophenol (Surr) - // : // : Dil Fac General Chemistry Analyte Result Qualifier RL MDL nit D Prepared Analyzed Dil Fac Chloride. mg/l // : Page of //

30 Client: Ohio EPA-NEDO Project/Site: TNEER- Client Sample Results TestAmerica Job ID: -- Client Sample ID: WFR- (OIL PHASE) Date Collected: // : Date Received: // : Lab Sample ID: -- Matrix: Waste Method: B - Metals (ICP) Analyte Result Qualifier RL MDL nit D Prepared Analyzed Dil Fac Arsenic. J.. mg/kg // : // : Barium. mg/kg // : // : Cadmium... mg/kg // : // : Calcium B mg/kg // : // : Chromium. J.. mg/kg // : // : Lead... mg/kg // : // : Magnesium J B. mg/kg // : // : Potassium J. mg/kg // : // : Selenium... mg/kg // : // : Silver... mg/kg // : // : Sodium J mg/kg // : // : Strontium.. mg/kg // : // : Tin. J B.. mg/kg // : // : Method: A - Mercury (CVAA) Analyte Result Qualifier RL MDL nit D Prepared Analyzed Dil Fac Mercury. J B.. mg/kg // : // : Page of //

31 Client: Ohio EPA-NEDO Project/Site: TNEER- Client Sample Results TestAmerica Job ID: -- Client Sample ID: SJO- (OIL PHASE) Date Collected: // : Date Received: // : Lab Sample ID: -- Matrix: Waste Method: B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL nit D Prepared Analyzed Dil Fac Acetone ug/kg // : // : Benzene ug/kg // : // : Dichlorobromomethane ug/kg // : // : Bromoform ug/kg // : // : Bromomethane ug/kg // : // : -Butanone (MEK) ug/kg // : // : Carbon disulfide ug/kg // : // : Carbon tetrachloride. ug/kg // : // : Chlorobenzene. ug/kg // : // : Chloroethane ug/kg // : // : Chloroform ug/kg // : // : Chloromethane ug/kg // : // :,-Dichloroethane ug/kg // : // :,-Dichloroethane ug/kg // : // :,-Dichloroethene ug/kg // : // :,-Dichloropropane ug/kg // : // : cis-,-dichloropropene. ug/kg // : // : trans-,-dichloropropene ug/kg // : // : Ethylbenzene. ug/kg // : // : -Hexanone ug/kg // : // : Methylene Chloride ug/kg // : // : -Methyl--pentanone (MIBK) ug/kg // : // : Styrene. ug/kg // : // :,,,-Tetrachloroethane ug/kg // : // : Tetrachloroethene ug/kg // : // : Toluene ug/kg // : // : Trichloroethene ug/kg // : // : Vinyl chloride ug/kg // : // : Xylenes, Total ug/kg // : // :,,-Trichloroethane ug/kg // : // :,,-Trichloroethane ug/kg // : // : Cyclohexane ug/kg // : // :,-Dibromo--Chloropropane ug/kg // : // : Ethylene Dibromide ug/kg // : // : Dichlorodifluoromethane ug/kg // : // : cis-,-dichloroethene. ug/kg // : // : trans-,-dichloroethene ug/kg // : // : Isopropylbenzene J. ug/kg // : // : Methyl acetate ug/kg // : // : Methyl tert-butyl ether. ug/kg // : // :,,-Trichloro-,,-trifluoroethane ug/kg // : // :,,-Trichlorobenzene. ug/kg // : // :,-Dichlorobenzene ug/kg // : // :,-Dichlorobenzene. ug/kg // : // :,-Dichlorobenzene ug/kg // : // : Trichlorofluoromethane ug/kg // : // : Chlorodibromomethane ug/kg // : // : Methylcyclohexane ug/kg // : // : Page of //