Agilent Gas Phase Solutions
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1 Agilent Gas Phase Solutions Shannon Coleman Applications Engineer HPI Solutions Overview Page 1
2 GC SP1 Analyzers Page 2 Solutions Overview Agilent restricted January 2011
3 GC SP1 Analyzers > 100 Analyzers Impurities in Bulk Gases Transformer Oil Gas Analyzers SIMDIS Analyzers ASTM Methods GPA Methods UOP Methods EN Methods Based on Agilent Application Notes Refinery Gas Analyzers Natural Gas Analyzers Sulfur Analyzers Biodiesel Analyzers CO/CO2 Analyzers Gasoline Analyzers Green House Gases Analyzers Nitrogen Analyzers Page 3 Solutions Overview Agilent restricted January 2011
4 GC SP1 Analyzers Standard GC HW, ordered according to QBD (SP ) Factory Pre setup + 5 valves 7 columns plumbing, valve timing setup and leak checking Application Specific Consumables 7 columns all pre conditioned, and one spare set of packed columns, appropriate inert tubing if required, application specific check out standard, applicationreport macro, union connector asappropriate, appropriate, plus Application Specific Documents Customer CD: methods, manuals, test result Page 4 CE Specialist Delivers setup on site No pain, no struggle Duplicate factory checkout + Optional customer consulting services Prepare customers for 1 st sample run Solutions Overview Agilent restricted January 2011
5 Fast RGA - 3 Parallel Channels (SP ) Col 5 3rd TCD Channel C PCM Col Sample 1 2 Vent In Col 4 Col 3 C TCD Vent B Col 1 PCM A Inlet A 4 Col B TCD FID Channel Sample out In A FID Col 7 Solutions Overview Page 5
6 Fast RGA - 3 Parallel Channels (SP ) A t-2-pentene 2-methyl-2-butenee 1-pentene c-2-pentene ne ane propane pa C6+ metha ethylene cyclopropane eth propylene i-butane n-butane propadiene acetylene t-2-butene 1-butene i-butylene c--2-butene i-pentane n-pentane 1,3-butadiene propyne sec. FID Channel min 25 µv O2 CO CO2 CH4 N Back TCD Channel Carrier gas: He min 3 rd TCD Channel Carrier gas: N2 Solutions Overview Page 6
7 Extended RGA 2-Channel System for C1 C12 by FID and Permanent Gases by TCD Page 7 HPI Solution overview Agilent Restricted Neophyte training Shanghai,Sep, 2007
8 Extended RGA 2-Channel System for C1 C12 by FID and Permanent Gases by TCD FID: C1 C6 TCD: H2 C3 FID: C6 C12 Page 8 HPI Solution overview Agilent Restricted Neophyte training Shanghai,Sep, 2007
9 Hydrocarbon and Permanent Gas Analysis for LPG and Gas Samples Page 9 HPI Solution overview Agilent Restricted Neophyte training Shanghai,Sep, 2007
10 Natural Gas Analyzer (NGA) (SP ) Solutions Overview Page 10
11 Typical NGA Chromatogram (SP ) 25 uv TCD1 A, (A:\NAT00017.D) 1800 Propane 1600 Methane Ethane 1000 Nitrogen Iso-Butane N-Butane C6+ Iso-Pentane N-Pentane CO2 Oxygen min Solutions Overview Page 11
12 NGA Analysis in under 6 minutes (SP ) pa C6+ methane ethane propane i-bu utane n-butane neopen ntane i-pentan ne n-pent tane FID Channel min 25 µv CO2 N2 methane methane CH4 Back TCD Channel Carrier gas: He µv TCD3 C Aux Signal (RGAJUN27\NGAC7C D) He H2 3 rd TCD Channel Carrier gas: N min min Page 12 Solutions Overview
13 SP : Flexibility for Hydrocarbon Analysis p A methane ethane propane i-butane n-butane neopentane i-pentane n-pentane Back flush C6+, Valve switch time 0.6 minutes C min p A Back flush Back flush C7+, Valve switch time 0.75 minutes 30 nc C min p A nc C6 No back flush, see individual C6,C7,C8 peaks nc7 nc min Solutions Overview Page 13
14 GC Special Hardware Only SP1 Options Page 14 Solutions Overview Agilent restricted January 2011
15 Overview - GC Platforms & Positioning 7820 GC Entry Level LTM /7890 GC Fast heating/ cooling Price/Performance 490 Micro GC Fast Gas Analysis Compact Size 7890 GC Highest flexibility Industry leader Technologies 6850 GC Small footprint Page 15 Gas Chromatograph Agilent Restricted
16 GC Inlets/Detectors and more [ EN: 7890 specifications (description, specs, ] Introduced or refreshed in FY Page 16
17 Special Hardware Only GC Factory Options SP1s Factory installed non standard options like special columns, valves, special tubing, etc. as requested by the customer. No factory or field application checkout Solutions Overview Agilent restricted Page 17 January 2011
18 SP1 Dedicated Analyzers and Custom Hardware Only Solutions Let us help you configure your system Decide on hardware configuration Agilent pre-designed analyzer Agilent custom analyzer Agilent hardware only design Channel Partner Solution (Custom hardware, pre-tested analyzer solutions, online and process GC). Page 18
19 Sample Information: Sample Description Form: Page 19 HPI Solution overview Agilent Restricted Neophyte training Shanghai,Sep, 2007
20 Custom Solutions Page 20 HPI Solution overview Agilent Restricted Neophyte training Shanghai,Sep, 2007
21 Custom Solutions Page 21 HPI Solution overview Agilent Restricted Neophyte training Shanghai,Sep, 2007
22 Custom Solutions Page 22 HPI Solution overview Agilent Restricted Neophyte training Shanghai,Sep, 2007
23 Capillary Flow Technology Page 23 HPI Solution overview Agilent Restricted Neophyte training Shanghai,Sep, 2007
24 Types of (non-cft) Connectors Used In The GC Oven Advantages Limitations Metal Packed columns, Not inert, no ferrule Fittings reliable for capillary columns Press Fit Glass Low dead volume, inert, low cost Difficult to assemble, comes apart Page 24 Graphite Polyimide High temperature Low initial leakage Sheds active graphite particles into sample path Loosens and leaks with oven cycling, solvent tailing Capillary Flow Technology E-seminar April, 2009
25 5 Key Developments in Capillary Flow Technology Metal Ferrules Manifold Plates Easy to use, do not loosen or leak with oven cycling to 350 C Complex flow structures with low thermal mass Deactivation Makes metal surfaces as inert as column of Metal EPC Calculators Backflushing now possible, change MSD columns without venting, known column outlet pressure Accurately predict flows and pressures BEFORE installing devices Page 25 Capillary Flow Technology E-seminar April, 2009
26 Capillary Flow Technology- Design a proprietary Agilent Technology Low dead volume - Photolithographic chemical milling Diffusion bond two halves to form a single flow plate Fast thermal response - small, thin profile provides Leak tight fittings - projection welded connections for Inertness - Deactivation of all internal surfaces for Page 26 Capillary Flow Technology E-seminar April, 2009
27 Capillary Flow Technology Restrictor 1 out to vent Column 1 In Restrictor 2 or Column 2 Nut Ferrule Channel Plate Unique design provides rugged, reliable connections with minimal unswept volume and high inertness Page 27 Capillary Flow Technology E-seminar April, 2009
28 Backflush Review
29 What kind of connectors can be used for backflushing? Anything with an independent pressure or flow control. Purged Union Deans Switch Aux EPC In Column QuickSwap MSD Restrictor Purged Splitter Flow Modulator
30 Milk Extract It took additional 33 mins and column to 320oC to remove these high boilers. Run stopped at 42 min and backflushed at 280oC for 7 mins. Blank run after backflushing. Column is clean. 5 Page min Capillary Flow Technology E-seminar April, 2009
31 We Have Control Of Both The Inlet & Outlet Pressure Of The Column We can reverse the column flow during bakeout During GC Run Split Vent S/SL Inlet 25 psi Aux EPC 4 psi Capillary Flow Device Detector(s) After GC Run Split Vent S/SL Inlet 2 psi Aux EPC 60 psi Capillary Flow Device Detector(s) Page 31 Capillary Flow Technology E-seminar April, 2009
32 Backflush: Many Advantages Analysis of Complex Samples ( Dirty (Dirty Matrices ) Reduces analysis time (more samples per day) Provides more consistent GC retention times Increases lifetime of analytical column
33 Post-Column Example - Analysis Inlet EPC Aux EPC P 1 P 2 Purged Union S/Sl Inlet Det. Restrictor Split Vent Column
34 Post-Column Example Analysis Inlet EPC Aux EPC P 1 P 2 Purged Union Det. Restrictor Split Vent Column
35 Post-Column Example - Backflush Inlet EPC Aux EPC P 1 P 2 Purged Union Det. Restrictor Split Vent Column
36 Coated Pre-Column Example Inlet EPC Aux EPC P 1 P 2 Restrictor S/S Inlet Purged Union MSD Split Vent Coated Pre-Column Column
37 Coated Pre-Column Example Forward Flow Inlet EPC Aux EPC P 1 P 2 Restrictor MSD Purged Split Vent Coated Pre-Column Union Column
38 Coated Pre-Column Concurrent Backflush Inlet EPC Aux EPC P 1 P 2 Restrictor Purged Union MSD Split Vent Coated Pre-Column Column
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