Test Report No. F690101/LF-CTSAYAA

Transcription

1 Test Report No. F690101/LF-CTSAYAA Page 1 of 8 ROHM AND HAAS ELECTRONIC MATERIALS KOREA LTD. (RHEM) 6 3gongdan 1-ro, Seobuk-gu Cheonan-si, Chungcheongnam-do Korea The following sample(s) was/were submitted and identified by/on behalf of the client as:- SGS File No. Product Name : AYAA : Solderon ST-380 Process Item No./Part No. : N/A Received Date : Test Period : to Test Results : For further details, please refer to following page(s) SGS Korea Co., Ltd. Jeff Jang / Chemical Lab Mgr t +82 (0) f +82 (0)

2 Test Report No. F690101/LF-CTSAYAA Page 2 of 8 Sample No. : AYAA Sample Description : Solderon ST-380 Process Item No./Part No. : N/A Materials : N/A Heavy Metals Cadmium (Cd) With reference to IEC :2013 (Determination of Cadmium by ICP-OES) 0. Lead (Pb) With reference to IEC :2013 (Determination of Lead by ICP-OES) Mercury (Hg) With reference to IEC :2013 (Determination of Mercury by ICP-OES) 2 Hexavalent Chromium (Cr VI)* With reference to IEC :2017, determination of Hexavalent Chromium by Colorimetric Method using UV-Vis and/or with reference to IEC :2013, determination of Chromium by ICP-OES. 8 Antimony (Sb) With reference to EPA 302(1996), US EPA 6010B(1996), ICP 10 Flame Retardants-PBBs/PBDEs Monobromobiphenyl With reference to IEC :201 Dibromobiphenyl With reference to IEC :201 Tribromobiphenyl With reference to IEC :201 Tetrabromobiphenyl With reference to IEC :201 Pentabromobiphenyl With reference to IEC :201 Hexabromobiphenyl With reference to IEC :201 Heptabromobiphenyl With reference to IEC :201 Octabromobiphenyl With reference to IEC :201 Nonabromobiphenyl With reference to IEC :201 Decabromobiphenyl With reference to IEC :201 Monobromodiphenyl ether With reference to IEC :201 t +82 (0) f +82 (0)

3 Test Report No. F690101/LF-CTSAYAA Page 3 of 8 Sample No. : AYAA Sample Description : Solderon ST-380 Process Item No./Part No. : N/A Materials : N/A Flame Retardants-PBBs/PBDEs Dibromodiphenyl ether With reference to IEC :201 Tribromodiphenyl ether With reference to IEC :201 Tetrabromodiphenyl ether With reference to IEC :201 Pentabromodiphenyl ether With reference to IEC :201 Hexabromodiphenyl ether With reference to IEC :201 Heptabromodiphenyl ether With reference to IEC :201 Octabromodiphenyl ether With reference to IEC :201 Nonabromodiphenyl ether With reference to IEC :201 Decabromodiphenyl ether With reference to IEC :201 Phthalates Di-isobutyl phthalate (DIBP) With reference to IEC ; 2017, GC/MS 0 Di-butyl phthalate (DBP) With reference to IEC ; 2017, GC/MS 0 Benzyl butyl phthalate (BBP) With reference to IEC ; 2017, GC/MS 0 Di-(2-ethylhexyl) phthalate (DEHP) With reference to IEC ; 2017, GC/MS 0 Halogen Content Bromine(Br) With reference to EN 1482:2007, IC 30 Chlorine(Cl) With reference to EN 1482:2007, IC 30 t +82 (0) f +82 (0)

4 Test Report No. F690101/LF-CTSAYAA Page 4 of 8 NOTE: (1) = Not detected.(<mdl) (2) = ppm (3) MDL = Method Detection Limit (4) - = No regulation () Negative = Undetectable / Positive = Detectable (6) ** = Qualitative analysis (No Unit) (7) * = a. The result of Hexavalent Chromium (Cr(VI)) is ND as the result of Chromium (Cr) is ND, and confirmation test of Hexavalent Chromium (Cr(VI)) is not required. b. If the Chromium (Cr) content is greater than the MDL of Hexavalent Chromium (Cr(VI)), confirmation test of Hexavalent Chromium (Cr(VI)) is required. Picture of Sample as Received: AYAA t +82 (0) f +82 (0)

5 Test Report No. F690101/LF-CTSAYAA Page of 8 Testing Flow Chart for RoHS:Cd/Pb/Hg/Cr 6+ /PBBs&PBDEs Testing Sample cutting / weighing Sample Preparation Cd/Pb/Hg/Cr PBBs/PBDEs 6+ Cr Acid Digestion with Microwave/Hotplate Sample Solvent Extraction Nonmetallic Material Metallic Material Filtration Concentration/Dilution of Extraction Solution Dissolving by ultrasonication Digesting at 10~160 Boiling water extraction Solution Residue 1) Alkali Fusion / Dry Ashing 2) Acid to dissolve Filtration GC/MS Digestion at 60 by ultrasonication ph adjustment Separating to get aqueous phase Adding 1,-diphenylcar bazide for color UV-Vis ICP-OES/AAS Adding 1,-diphenylcarbazide for color UV-Vis The samples were dissolved totally at the acid digestion step of the above flow chart for Cd,Pb,Hg Section Chief : Minkyu Park t +82 (0) f +82 (0)

6 Test Report No. F690101/LF-CTSAYAA Page 6 of 8 Flow Chart for Inorganic Elements Testing Inorganic Elements Mechanic_Sample Sample Measurement Acid Digestion with Microwave/Hotplate Filtration Residue Total Digestion ICP-AES Major Inorganic Heavy Metals Antimony(Sb), Beryllium(Be), Phosphorus(P), Arsenic(As) etc. t +82 (0) f +82 (0)

7 Test Report No. F690101/LF-CTSAYAA Page 7 of 8 Flow Chart for Halogen Test Sample screening using XRF. Liquid containing water(>80%) Yes No Weigh the samples into the combustion boat. Add absorption solution into the bomb or tube. Admit O2 gas or O2 +Ar2 gas and start the combustion. Allow during absorption of the burnt gas. Dilute the solution (EPA300) Analyze absorbed solution using Ion Chromatography. Data t +82 (0) f +82 (0)

8 Test Report No. F690101/LF-CTSAYAA Page 8 of 8 Flow Chart for Phthalate Test Sample pretreatment / Separation Sample dissolved / extracted by THF Dilute Extracted solution Analysis was performed by GC/MS Data *** End of Report *** t +82 (0) f +82 (0)