SINTERED GLASSWARE Porosity Grades and their General Use

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PRODUCT CATALOGUE Associated Scientific Mfg. Industries 10,Bhairab Mukherjee Lane, Shyambazar (Opp. R.G.Kar Medical College and Hospital Emergency Building) Kolkata 700 004 West Bengal, India Phone No. - +91 33 2554 8602, 2543 1010 Mobile - +91 9830606770, 9007618488 E-mail - associatedscientificmfgind@yahoo.co.in Contact Person Mr. Arun Kumar Bandyopadhyay

SINTERED GLASSWARE Porosity Grades and their General Use Porosity Grade Pore size General Use G-0 160-250 micron Coarse filtration, Gas dispersion and Support for other filter material. G-1 100-160 micron Coarse precipitate, filtration, Gas Dispersion, coarse grain material filtration G-2 40-100 micron Medium and crystalline precipitate Filtration, medium filtration and washing G-3 16-40 micron Fine Gas filtration and dispersion mercury filtration, fine grain material filtration, collection of fine precipitates, analytical work with medium precipitates. G-4 10-16 micron Valves for mercury collection of very fine Precipitates. Analytical work with fine precipitates. G-5 1-16 micron Valves for mercury collection of very fine Precipitates. Analytical work with fine precipitates.

CRUCIBLE: - Ghooch type with sintered disc of porosity G-0 to G-5. Cat. No. Capacity (ML) 001/01 15 001/02 30 001/03 50 BUCHNER FUNNEL: - With sintered disc of porosity G-0 to G-5, plain. Cat. No. Capacity (ML) Disc Dia (MM) 002/01 35 30 002/02 80 40 002/03 100 50 002/04 200 65 002/05 500 90 002/06 1000 120 002/07 2000 125 002/08 3000 150 With sintered disc of porosity G-0 to G-5, cone at stem. Cat. No. Capacity (ML) Disc Dia Cone at stem (MM) 002/09 35 30 14/23 or 19/26 002/10 80 40 14/23 or 19/26 or 29/32 002/11 100 50 002/12 200 65 19/26 or 24/29 or 29/32 002/13 500 90 19/26 or 24/29 or 29/32 002/14 1000 120 19/26 or 24/29 or 29/32

With sintered disc of porosity G-0 to G-5, cone, vaccum connection. Cat. No. Capacity (ML) Disc Dia (MM) Vaccum Connection 002/15 35 30 14/23 or 19/26 002/16 80 40 14/23 or 19/26 002/17 200 65 19/26 or 24/29 002/18 500 90 19/26 or 24/29 or 29/32 002/19 1000 120 19/26 or 24/29 or 29/32 SINTERED GLASS FILTER TUBE: - With sintered disc sealed in center, porosity G-0 to G-5. Cat. No. Capacity (MM) 003/01 10 003/02 20 003/03 30 003/ 04 40 003/05 60 003/06 90

CONICAL FILTER: - (HIRCH Type) With sintered disc, porosity G-0 to G-5. Cat. No. Size Dia. (MM) Capacity (ML) 004/01 20 25 004/02 30 60 004/03 30 175 SINTERED GLASS GAS DISTRIBUTION TUBE: - (Filter stick) Porosity G-0 to G-5. Cat. No. 005/01 10 005/02 20 005/03 30 Disc Dia (MM)

TUBE SEALED WITH REDUCED ENDS: - With sintered disc (pipeline filter), porosity G-0 to G-5 Cat. No. Disc Dia (MM) 006/01 30 006/02 40 006/03 50 006/04 65 006/05 90 CHROMATOGRAPHY COLUMN (SINTERED GLASS): - Plain, porosity G-0 to G-4. Cat. No. Bore (MM) Effective Length (MM) 007/01 10 200 007/02 12 400 007/03 15 300 007/04 20 300 007/05 30 300 007/06 40 550 007/07 50 550

CHROMATOGRAPHY COLUMN (SINTERED GLASS): - With stopcock, porosity G-0 to G-5. Cat. No. Bore (MM) Effective Length (MM) 008/01 10 200 008/02 12 400 008/03 15 300 008/04 20 300 008/05 30 300 008/06 40 550 008/07 50 550 CHROMATOGRAPHY COLUMN (SINTERED GLASS): - With I/C joints, porosity G-0 to G-5. Cat. No. Bore (MM) Effective Length (MM) 009/01 10 200 009/02 12 400 009/03 15 300 009/04 20 300 009/05 30 300 009/06 40 550 009/07 50 550

FILTERING APPARATUS WITT S: - Complete with filtering flask Gooch crucible with sintered disc of porosity G-0 to G-5, glass adaptor and rubber cone. Cat. No. Flask capacity (ML) Crucible capacity (ML) 010/01 250 30 010/02 500 30 010/03 1000 30 FILTERING APPARATUS WITT S: - Complete with flanged jar, flanged lid, funnel and 250 ml beaker. FILTER APPARATUS: - Complete with filter flask, with socket and Buchner funnel with sintered disc of porosity G-0 to G-5, having cone. Cat. No. Flask capacity (ML) Crucible capacity (ML) Joint 012/01 250 80 24/29 012/02 500 200 24/29 012/03 1000 500 29/32 012/04 2000 1000 29/32

MEMBRANE FILTER HOLDER (MILIPORE TYPE ASSEMBLY): - With membrane support, funnel, flask and clamp. STD joints fitting. Cat No. Membrane Dia Flask (ML) 013/01 25mm, B-29 socket 15 013/02 25mm, B-29 socket 30 013/03 25mm, B-29 socket 50 013/04 25mm, B-29 socket along with 50 250ml filtering flask 013/05 47mm,B-40socket 300 013/06 47mm, B-40 socket along with 1000ml filtering flask 300 MEMBRANE FILTER HOLDER (MILIPORE TYPE ASSEMBLY): - With membrane support, funnel, flask and clamp. Cat. No. Membrane Dia Flask (ML) 014/01 25mm, rubber cork 15 014/02 25mm, rubber cork 30 014/03 25mm, rubber cork 50 014/04 25mm, rubber cork along with 50 250ml filtering flask 014/05 47mm rubber cork 300 014/06 47mm rubber cork along with 1000ml filtering flask 300

SINTERED DISC: - Porosity G-0 to G-5. Cat. No. Dia (MM) 015/01 10 015/02 15 015/03 20 015/04 25 015/05 30 015/06 40 015/07 50 015/08 60 015/09 65 015/10 70 015/11 75 015/12 80 015/13 90 015/14 100 015/15 120 015/16 150 SPERICAL JOINTS BALL & CUP: - Cat. No. Ball & Cup Joints Size Shank Length 016/01 Capillary S-13 S-13 100 016/02 S-13 S-13 100 016/03 S-19 S-19 100 016/04 S-29 S-29 100 016/05 S-35 S-35 100 016/06 S-41 S-41 100

VISCOMETER: - U-tube, Reverse Flow, BS/IP/RF Cat. No. Size Minimum viscosity 017/01 A 2 2 017/02 B 3 6 017/03 C 4 20 017/04 D 5 60 017/05 E 6 200 017/06 F 7 600 017/07 G 8 2000 017/08 H 9 6000 017/09 I 10 20000 017/10 J 11 60000 U-tube, B S/U Cat. No. Size Viscosity Range 018/01 A 1-5 018/02 B 2-15 018/03 C 6-45 018/04 D 20-120 018/05 E 60-500 018/06 F 200-1000 018/07 G 600-4000 018/08 H 200-15000 Cannon-Fenske, for Transparent Liquids, BS/IP/CF

Cat. No. Size Viscosity Range 019/01 25 4-1.6 019/02 50 0.8-3.2 019/03 100 3-12 019/04 150 7-28 019/05 200 20-40 019/06 300 50-200 019/07 350 100-400 019/08 400 240-960 019/09 450 500-2000 019/10 500 1600-6400 019/11 600 4000-16000 Cannon-Fenske, for opaque liquids, ASTM-D445 Cat. No. Size Viscosity Range 020/01 100 3-12 020/02 150 7-12 020/03 200 20-28 020/04 300 50-200 020/05 350 100-400 020/06 400 240-960 020/07 450 500-2000 020/08 500 1600-6400 020/09 600 4000-16000 Suspended level BS/IP/SL Cat. No. Size Viscosity 021/01 A 1 2 021/02 B 1A 6 021/03 C 2 20 021/04 D 2A 60 021/05 E 3 200 021/06 F 3A 600 021/07 G 4 2000 021/08 H 4A 6000 021/09 I 5 20000

Suspended level shortened, BS/IP/SL Cat. No. Size Minimum Viscosity 022/01 A 3 2 022/02 B 4 6 022/03 C 5 20 022/04 D 6 60 022/05 E 7 200 022/06 F 8 600 022/07 G 9 2000

PORESIZES OF SINTERED GLASS FILTERS

Safety Instructions for Borosilicate Glassware Cleaning Before the first use of glass-filters, they should be cleaned with diluted, warm hydrochloric acid, followed by several rinse with distilled water to remove dust loose particles. Glass filters should be cleaned immediately after their use. The surface can be wiped with a soft squeegee or brush. Surface rinsing with a wash bottle or back flushing under the water tap is often sufficient. Pressure and Vacuum Even small scratches or internal abrasions of the glass surface can greatly reduce the vacuum or pressure resistance. Filter pores may clog during filtration and cause a pressure drop. In any case 1kp/cm 2 may not be exceeded. Never subject glassware to sudden pressure changes. Temperature Resistance The maximum allowable service temperature is approx. 500 degrees centigrade. To avoid permanent stress, the heating and cooling rate should not exceed 5 0 C/min. wet glass-filters should slowly be heated up to 80 degrees centigrade and dried for one hour, before temperature is increased. Permanent stress can reduce the mechanical and thermal resistance. Never subject glassware to sudden temperature changes. Chemical Resistance High concentrations of hydrofluoric acid or hot alkali solutions attack the glass with increasing temperature and can cause deterioration in the filter and a destruction of the pore size. Safety Advice When working with glassware always wares protective glasses and protective gloves to avoid injuries. Use a safety screen or similar protection when working with glassware subject to pressure or vacuum. Be prepared, that reagents may leak from a broken vessel. Please heed this guideline in combination with the respective statespecific regulations for the use of glassware in the laboratory.