Enhanced Coalbed Methane (ECBM) Field Test at South Qinshui Basin, Shanxi Province, China

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Enhanced Coalbed Methane (ECBM) Field Test at South Qinshui Basin, Shanxi Province, China Bill Gunter, Sam Wong, David Law, ARC Feng Sanli,Ye Jianping, Fan Zhiqiang, CUCBM GCEP workshop August 22-23, 2005 Beijing 1

ECBM Project in China Micro Pilot to Pilot to Commercial Demonstration 2

Micro-Pilot Test Goals To measure and evaluate data to obtain estimates of reservoir properties and sorption behavior To calibrate a simulation model for estimation of the enhancement of CBM recovery in a larger-scale pilot or full field development Enhancement of CBM recovery can not be estimated directly from micro-pilot test data 3

Demonstration Site Location Shanxi Province Hebei Province Shijiazhuang Taiyuan Qinshui County Qinshui Basin Jincheng Changzhi Anyang Henan Province Zhengzhou Potential Pilot Area 4

Attractiveness of Qinshui Basin Large areal extent Thick, laterally continuous coal seams Highest gas contents measured in China Relatively shallow depths of coal seams Reasonable access to local and distant markets (West to East Pipeline is 30-90 km from south Qinhsui at Jincheng) Relatively more explored than other basins 5

Coal Characteristics Qinshui Basin: 24,000 km 2 CBM Resource: 5.5 trillion sm 3 Primary CBM recovery performance in South Qinshui Basin (CUCBM owned 20+ wells) Peak rate: 5,000 16,000 sm 3 /d High rank semi-anthracite and Anthracite coal Vitrinite reflectance: 2.7 4% 6

China ECBM Project Canadian International Development Agency (CIDA) Canadian Climate Change Development Fund (CCCDF) (CA $ 5 million) Ministry of Commerce (MOFCOM) China United Coalbed Methane Corporation Ltd. (CUCBM) (CA $ 5 million) 3.5 - year CA $ 10 million Project (Started March 2002) 7

Major Tasks Potential pilot site selection Geological/engineering/environmental characterization and ranking of selected 3 pilot sites Design of micro-pilot field test procedures to evaluate CBM reservoir properties Carry out a single well micro-pilot field test at the best suitable site Selection of existing wells or drilling new wells Up to three micro-pilot tests will be performed if first two tests do not show commercial potential 8

Major Tasks (Continued) Micro-pilot test evaluation and numerical model calibration and fine tuning Large-scale pilot design leading to commercial production Training and technology transfer to be conducted in Canada and China 9

Site Visit 10

Primary CBM Recovery Operation CBM Production Well Gas / Water Separator 11

Target Coal Seam Well for Field Test No. 3 seam Shanxi Formation Age: Carboniferous Permian coal Depth: 478 meters Average thickness: 6 meters Reservoir temperature & pressure 25C & 500 psi To isolate seam from lower No. 15 seam, a bridge plug set in TL003 well at 573 meters 12

Well Configuration Cable to Surface Readout Downhole gauges Perforated pup Nogo seating nipple pump wellhead 244.5mm surface casing at 39.73m Perforations for #3 Seam 471.85-478.50 m NOGO seating nipple 2.4 m Perforated pup joint Blanking sub with Prism pressure tranducers at 498.47 m Top of Bridge Plug at 573 m Perforations for #15 Seam 13

Downhole Gauge Installation Installed 2 sensors 0 1500 psi range 0.025% full scale accuracy 0.0003% resolution 120 C temperature Signals transmitted via multi-conductor electromechanical wireline cable Surface Readout Live data readouts 1M data points storage capacity Gauge Carrier Surface Readouts 14

On-line Gas Chromatograph Capable of measuring produced gas composition on-line Separates and quantitates: CO 2, CH 4, O 2, N 2, C 2 -C 4, H 2 S Analysis every 5 minutes initially & decreased to 1/ hr as pilot continues Baseline Composition: CH 4-96.3%, CO 2 0.5%, N 2 3.67%, C 2 0.01% Wang Guoqiang 15

TLOO3 Wellsite & Wellhead Instrument Trailer Well head with Downhole gauge packoff 16

CO 2 Injection Strategy Goal is to inject 200 tonnes into reservoir over a 12 day period. Each truck can transport 18 tonnes of CO 2 Injection rate to be maintained below reservoir fracture pressure (1100 psi) Estimate average injection rate of 30L/min over 8-10 hr period Zhongyuan Oilfield CO 2 Truck Fleet 17

Injecting Liquid CO 2 18

25.0 Adsorption Isotherms Qinshui Basin CO 2 20.0 Sorbed Content (cc/g) 15.0 10.0 Langmuir Selectivity = 1.2 CH 4 5.0 0.0 0 5000 10000 15000 20000 Pressure (kpa) 19

Bottom-hole Pressure During Final Production Test CO2 Injection Pressure (KPa) Post CO2 Production Start Pressure Buildup 3-Apr 23-Apr 13-May 2-Jun 22-Jun 12-Jul 1-Aug 21-Aug Cumulative Time (days) 20

Injectivity versus Cumulative CO 2 21

Gas Composition During Final Production Test 80 Gas Composition, volume percentage 70 60 50 40 30 20 10 CO2 CH4 0 22-Jun 27-Jun 2-Jul 7-Jul 12-Jul 17-Jul 22-Jul 27-Jul 1-Aug 6-Aug Date 22

Results The average pressure of seam #3 is 1,241 kpa at a depth of 472 m Absolute permeability of the coal seam prior to CO 2 injection was 12 md, which was based on an effective permeability of gas of 2 md and a gas saturation of 40.8% 192 metric tonnes of CO 2 was injected Injectivity decreased during injection but permeability rebounded after an extended production period of 1 month 23

Summary The micro-pilot test as conducted in the South Qinshui TL-003 well has been completed successfully and has met all the technical objectives of the micropilot test. The history matching of the dataset from the micro-pilot and the simulation prediction for the multi-well pilot indicated a significant production enhancement compared to primary production, and that substantial CO 2 storage in the coal seam is feasible in a multi-well project. 24

Region of Investigation: 5-Spot Field Pilot Test Numerical Grid System FZ-008 Injector TL-003 780 m Rectangular Grid: 35 35 3 (Seam #3, Water zone, Seam #15) Grid Block Size: 20 m 20 m (except boundary grid blocks) FZ-002 FZ-003 780 m 25

Design of 5-Spot Field Pilot Test Numerical Simulation Scenario Continue after history matching run (November 19, 2003) Start CO 2 injection at new injector at a constant rate of 22,653 m 3 /d (0.8 MMscf/d) Inject CO 2 at coal seam #3 only Continuous production at all four Wells FZ-002, FZ-003, FZ-008 and TL- 003 at 1,560, 2,400, 1,400 and 1,450 kpa, respectively) 26

ARC Permeability Theory Fracture Porosity used in Reservoir Simulation Porosity Ratio (Phi/Phi atm ) 1.2 1.0 0.8 0.6 0.4 100% N 2 (1295.5 kpa, 0.9732) 100% CH 4 Initial Conditions: 97.54% CH 4, 2.54% N 2, 0.04% CO 2 100% CO 2 P i 0 2,000 4,000 6,000 8,000 10,000 Pressure (kpa) φ atm = 0.00822 φ i = 0.008 27

ARC Permeability Theory Fracture Permeability used in Reservoir Simulation 10 Permeability Ratio (k/k atm ) 1 100% N (1295.5 kpa, 0.9217) 2 100% CH 4 Initial Conditions: 97.54% CH 4, 2.54% N 2, 0.04% CO 2 0.1 P i 100% CO 2 0 2,000 4,000 6,000 8,000 10,000 Pressure (kpa) k atm = 13.67 md k i = 12.6 md 28

5-Spot Field Pilot Test CO 2 Injection Time 0 = March 16, 1998 Below estimated coalbed fracture pressure Start CO 2 Injection (5.6783 years) 29

5-Spot Field Pilot Test Methane Production Rate Methane Production Rate (m3/day) 8000 7000 6000 5000 4000 3000 2000 1000 Time 0 = March 16, 1998 After 6 months CO 2 Injection FZ-002 FZ-003 FZ-008 TL-003 0 5 6 7 8 9 10 11 Start CO 2 Injection Time (yr) Thick Curves: CO 2 -ECBM Thin Curves: Primary CBM 30

5-Spot Field Pilot Test CO 2 Distribution in Coal Seam #3 FZ-008 TL-003 CO 2 Mol Fr. in Fracture FZ-002 FZ-003 6 months 1 year 2 years 3 years 4 years 5 years 31

5-Spot Field Pilot Test CO 2 Inventory Time 0 = March 16, 1998 CO 2 Stored After 6 months CO 2 Injection Start CO 2 Injection (5.6783 years) 32

5-Spot Field Pilot Test Performance Prediction Well FZ-002 FZ-003 FZ-008 TL-003 CO 2 Breakthrough Time* (year after CO 2 injection) 2.6822 5.1233 3.8274 3.1205 Average CH 4 Production Rate 5,275 3,600 4,657 1,394 before CO 2 breakthrough (m 3 /day) 1,883 240 718 405 Peak CH 4 Production Rate before CO 2 breakthrough (m 3 /day) 6,319 2,036 4,901 627 5,355 1,305 1,789 520 Enhancement Factor** 2.80 15.00 6.49 3.44 * Time after CO 2 injection when 10% CO 2 occurred in production gas stream ** Ratio of average CH 4 production rate: (CO 2 -ECBM) / (Primary CBM) CO 2 -ECBM Primary CBM 33

5-Spot Field Pilot Test Cumulative CBM Production 3.5E+07 Cumulative Methane Production (m3) 3.0E+07 2.5E+07 2.0E+07 1.5E+07 1.0E+07 5.0E+06 Primary CBM ECBM Incremental Production 0.0E+00 3 4 5 6 7 8 9 10 11 Time (yr) 34

5-Spot Field Pilot Test Recommendation 20-acre 5-spot field pilot: Four corner producers are existing CBM Wells FZ- 002, FZ-003, FZ-008 and TL-003 Drill one new injector located approximately at the center of the pattern Inject CO 2 continuously at new injector at a constant rate of 22,653 m 3 /d (0.8 MMscf/d) for 6 months Enhancement of CH 4 production should be observed at all producers even though no CO 2 breakthrough should be observed at all producers 35