Schedule of ccreditation United Kingdom ccreditation Service 2 Pine Trees, Chertsey Lane, Staines-upon-Thames, TW18 3HR, UK ccredited to Metals and Minerals Division 2 Perry Road Witham Essex CM8 3TU Contact: Mrs C Hargreaves Tel: +44 (0)1376 536800 Fax: +44 (0)1376 520819 E-Mail: client.services@inspectorate.com Website: www.inspectorate.com Laboratory locations: s covered by the organisation and their relevant activities details ctivity code ddress 2 Perry Road Witham Essex CM8 3TU Local contac Mrs C Hargreaves Tel: +44 (0)1376 536800 Fax: +44 (0)1376 520819 Email:witham.hq@inspectorate.co.uk Website: www.inspectorate.com Metals & Minerals Division various tests Support Functions: Quality Management including document control, auditing and quality control ddress Inspectorate Prep Container Humber International Terminal ssociated British Ports West Haven Way Immingham DN40 2YD Local contact Mrs C Hargreaves Tel: +44 (0)1376 536800 Fax: +44 (0)1376 520819 Email:witham.hq@inspectorate.co.uk Website: www.inspectorate.com Metals & Minerals Division sampling and sample preparation B ssessment Manager: DC1 Page 1 of 14
Schedule of ccreditation United Kingdom ccreditation Service ccredited to DETIL OF CCREDITTION CTLYST MTERILS Documented In house methods Pt, Pd, Rh, Ir, Ru, u, g nalysis through the appropriate application of s following the Flexible Scope procedures Section 17 and SI236 Using the following techniques: Gravimetric or ICP or S Finish XRF Palladium, Platinum Fire ssay, ICP by F42 and F43 lumina Based Catalysts Total and cid Soluble Silver Volumetric titration utocatalysts Platinum, Palladium, Rhodium ICP-OES Platinum, Palladium and Rhodium XRF Spectrometry Carbon Based Catalysts Platinum, Palladium ICP-OES, Gravimetry Industrial Based Catalysts Palladium Fire ssay, Gravimetry, ICP- OES Silver Volumetric Titration Palladium, Gold Gravimetry, ICP-OES Petroleum Catalysts cid Insolubles Gravimetry Iridium ICP-OES Platinum, Rhenium UV/VIS Spectrophotometry Platinum, Palladium Gravimetry Rhenium, Total and cid Soluble UV/VIS Spectrophotometry ssessment Manager: DC1 Page 2 of 14
Schedule of ccreditation United Kingdom ccreditation Service ccredited to CONCENTRTES, ORES ND MINERLS - BSE METL Cl and F nalysis through the appropriate application of s following the Flexible Scope procedures Section 17 and SI236 Using the following techniques: Ion Selective Electrode Determination of carbon and sulphur nalysis through the appropriate application of s following the Flexible Scope procedures Section 17 and SI236 Using the following techniques: Carbon/Sulphur nalyser (combustion with infra-red analyser) Multiple elements including but not limited to: l, Sb, s, Ba, Bi, Cd, Ca, Cr, Co, Cu, Ge, u, In, Ir, Fe, Pb, Mg, Mn, Mo, Ni, Os, Pd, P, Pt, K, Rh, Ru, Se, Si, g, Na, Sr, S, Te, Tl, Sn, Ti, V, U, Th, Y, Zn nalysis through the appropriate application of s following the Flexible Scope procedures Section 17 and SI236 Using the following techniques: cid digestion, microwave digestion or fusion peroxide followed by S or ICP Fusion or pressed pellet with XRF finish ssessment Manager: DC1 Page 3 of 14
Schedule of ccreditation United Kingdom ccreditation Service ccredited to CONCENTRTES, ORES ND MINERLS - BSE METL (cont d) (cont d) l, Sb, s, Ba, Be, Bi, B, Cd, Ce, Ca, Cr, Co, Cu, Ga, Ge, u, In, Fe, Pb, Mg, Ni, K, Se, g, Na, Sr, Te, Tl, Sn, Ti, V, Zn Fusion, acid digestion or fire assay followed by S using I1, I2, I8, I10, I17, I18, I19, I20, I31, F18,F19,F20, F21, F22, F23, F25, F26, F29, F33, F38, F41 Sb, s, B, Cr, Co, F, Ge, Fe (elemental and oxide), Mg, Mn (including oxide), Pb, S, Sn, Ti, Zn (including oxide) Fusion or acid digestion and removal of impurities by analyte precipitation or oxidation or reduction followed by volumetric titration using G2, G3, G83, G6, G14, G15, G42, G77, G70, G22, G23, G25, G26, G28, G75, G36, G37, G38, G51, G57, G62, G65, G66, G67, G68, G81, G88, G31, G32, G33 & G34 l, Sb, s, Ba, Cd, Cu, Fe, Pb, Mg, Mn, Hg, Ni, g Fusion or acid digestion followed by ICP-OES using I2, I6, I17, I18, I19, 120, I29 & I31 Ba, C, Cl, Cu, u, Mo, Ni, Si, g, S as sulphate nalyte precipitation or fire assay followed by Gravimetric quantification using G4, G8, G9, G11, G13, G16, G18, G20, G41, G42, G43, G48, G52, G53, G54, G55, G56, F18, F19, F20, F21, F22, F23, F25, F26, F29, F33, F38 & F41 Pb & Zn Fusion and XRF by I28 Chlorine Gravimetry by G11 Fluorine, Germanium, Phosphorus, Silicon UV/VIS Spectrophotometry by G21, G78, G45, G48, G49, G76, G79 & G80) ssessment Manager: DC1 Page 4 of 14
Schedule of ccreditation United Kingdom ccreditation Service ccredited to CONCENTRTES, ORES ND MINERLS - BSE METL (cont d) (cont d) Sulphur Combustion/Volumetric titration by G51 Barytes Barium, Silicon, Strontium, Calcium, Iron Gravimetry, S Bastanite, Monazite and Rare Earth Materials Bastanite, Monazite and Rare Earth Materials (cont d) cid Insolubles Gravimetry Total Rare Earths Gravimetry Cerium Volumetric titration Bauxite lumina, Ca, Fe, Mg, P, K, Na, Si, Ti XRF Spectrometry Copper Concentrates Chlorine (50-1000 ppm) XRF Spectrometry Copper concentrates containing less than 2% rsenic Copper Volumetric titration Chromium Ores Chromium and Iron Volumetric titration Phosphorus and Silica UV/VIS Spectrophotometry Silicon, Calcium, luminium, Titanium and Magnesium as oxides and Phosphorus, Chromium and Iron XRF Spectrometry Colemanite, Tincal, Ulexite Boron Volumetric titration Ilmenite and Rutile Titanium Dioxide Volumetric titration ssessment Manager: DC1 Page 5 of 14
Schedule of ccreditation United Kingdom ccreditation Service ccredited to CONCENTRTES, ORES ND MINERLS - BSE METL (cont d) (cont d) Iron Ores lumina, Ca, Cr, Mg, Mn, P, K, Si, Ti, V, Fe, Si, l, S, V, Co, Ni, Cu, s, Pb, Zn XRF Spectrometry Ca, Ce, Li, Mg, K, Na S Iron and Iron as oxide Volumetric titration Silica Gravimetry Determination of Sulphur Carbon/Sulphur nalyser Manganese Ores lumina, Ba, Ca, Fe, Mg, P, K, Si, Ti XRF Spectrometry Manganese Ores Manganese and Manganese Dioxide Volumetric titration Manganese Ores Silica Gravimetry Molybdenite Molybdenum Gravimetry Copper, Molybdenum, Rhenium XRF Spectrometry Olivine Magnesium Volumetric titration Pyrite Gold Fire ssay Gravimetry Sulphur Gravimetry Siliceous Ores Sb, s, Bi, Cd, Co, Cu, In, Fe, Pb, Mn, Ni, Se, g, Te, Tl, Zn S Silica Gravimetry Silver ores luminium as oxide, Sb, s, Pb, Zn peroxide fusion followed by ICP-OES Tantalite Tantalum and Niobium XRF Spectrometry ssessment Manager: DC1 Page 6 of 14
Schedule of ccreditation United Kingdom ccreditation Service ccredited to METLS ND LLOYS - FERROUS Multiple elements including but not limited to: l, Sb, s, Ba, Bi, Cd, Ca, Cr, Co, Cu, Ge, u, In, Ir, Fe, Pb, Mg, Mn, Mo, Ni, Os, Pd, P, Pt, K, Rh, Ru, Se, Si, g, Na, Sr, S, Te, Tl, Sn, Ti, V, U, Th, Y, Zn nalysis through the appropriate application of s following the Flexible Scope procedures Section 17 and SI236 Using the following techniques: cid digestion, microwave digestion or fusion peroxide followed by S or ICP XRF Ferrochrome and Charge Chrome Chromium Volumetric titration Ferro lloys Palladium, Platinum, Rhodium, Phosphorus ICP-OES, UV/VIS Spectrophotometry Silicon Gravimetry Ferro-Chromium and Ferro- Titanium lloys Determination of Carbon and Sulphur Carbon/Sulphur nalyser Ferro-Manganese Manganese Volumetric titration Ferro-Molybdenum Molybdenum Gravimetry, XRF Stainless steel residue Chromium, Molybdenum, Nickel and Iron XRF Spectrometry Determination of Carbon and Sulphur Carbon/Sulphur nalyser ssessment Manager: DC1 Page 7 of 14
Schedule of ccreditation United Kingdom ccreditation Service ccredited to METLS ND LLOYS - BSE METL Multiple elements including but not limited to: l, Sb, s, Ba, Bi, Cd, Ca, Cr, Co, Cu, Ge, u, In, Ir, Fe, Pb, Mg, Mn, Mo, Ni, Os, Pd, P, Pt, K, Rh, Ru, Se, Si, g, Na, Sr, S, Te, Tl, Sn, Ti, V, U, Th, Y, Zn nalysis through the appropriate application of s following the Flexible Scope procedures Section 17 and SI236 Using the following techniques: cid digestion, microwave digestion or fusion peroxide followed by S or ICP XRF l, Bi, Cr, Co, Cu, Pb, Mn, g, Sn Fusion or acid digestion and removal of impurities by analyte precipitation or oxidation or reduction followed by volumetric titration using G1, G5, G14, G42, G18, G31, G32, G33, G37, P2, G58, G59, G60 & G61 l, Sb, s, Be, Bi, B, Cd, Ca, Cr, Co, Cu, Ga, Ge, In, Fe, Pb, Mg, Mn, Hg, Mo, Ni, Se, g, Sr, Te, Tl, Sn, Ti, V, Zn cid digestion followed by S using I3, I4, I5, I7, I9 & I22 Sb, s, Bi, Cd, Cu, In, Ni, Rh cid digestion followed by ICP- OES using I9, I5, I27, I21, I32 & I22 Ba, Cd, C, Cu, Ir, Mo, Ni, Rh, Si Element precipitation followed by Gravimetric quantification using G4, G7,G9, G18, P25, G40, G41, G44, P25 & G50 u, Pd, Pt, Rh, g Fire ssay with nickel sulphide collection, Gravimetry & ICP-OES using F15 Molybdenum Oxidation, fusion & XRF using I29 ssessment Manager: DC1 Page 8 of 14
Schedule of ccreditation United Kingdom ccreditation Service ccredited to METLS ND LLOYS - BSE METL (cont d) Phosphorus UV/VIS Spectrophotometry using G45 Sulphur Combustion/Volumetric titration using G51 BSE METL MTERILS - Sweeps, Residues, Slimes, Mattes and Secondary Materials l, Sb, Bi, Cr, Co, Pb, Mg, Sn, Ti, Zn Volumetric titration l, Sb, s, Ba, Be, Bi, B, Cd, Ca, Cr, Co, Cu, Ga, Ge, In, Fe, Pb, Mg, Mn, Hg, Mo, Ni, Se, g, Sr, Te, Tl, Sn, Ti, V, Zn S Ba, Br, Cd, C, Cl, Cu, Mo, Ni, Os, Se Gravimetry Fluorine UV/VIS Spectrophotometry u, Ir, Pd, Pt, Rh, Ru, g Fire ssay/gravimetry ICP-OES Selenium ICP-OES Sulphur Combustion/Volumetric titration PRECIOUS METL BERING MTERILS Bullion: Gold, Gold/Silver, Silver, Lead, Copper/Precious metal Gold Fire ssay Gold, Silver Fire ssay, Gravimetry Palladium, Platinum Fire ssay, ICP-OES Copper Gravimetry ssessment Manager: DC1 Page 9 of 14
Schedule of ccreditation United Kingdom ccreditation Service ccredited to PRECIOUS METL BERING MTERILS (cont d) (cont d) Silver Volumetric titration Iridium, Rhodium ICP-OES Platinum bullion, precious metal concentrates and residues Platinum, Palladium, Rhodium Gravimetry, ICP-OES Carbonaceous Material Gold Fire ssay, Gravimetry Complexed Organics, Resins and Cyanides Electronic/Computer Materials Gold Gravimetry Copper and Gold Gravimetry Gold, Silver Fire ssay, Gravimetry Palladium, Platinum Fire ssay, ICP-OES Silver S Metals and lloys Copper Gravimetry Gold, Silver Fire ssay, Gravimetry Palladium, Platinum Fire ssay, ICP-OES Platinum, Rhodium, Iridium Gravimetry, ICP-OES Silver Volumetric titration Palladium, Platinum, Rhodium ICP-OES Ores and Concentrates u, Ir, Pd, Os, Pt, Rh, Ru (Osmiridium) Gravimetry, ICP-OES Silver/Film Scrap Silver: Halide and Raw Scrap Fire ssay, Gravimetry ssessment Manager: DC1 Page 10 of 14
Schedule of ccreditation United Kingdom ccreditation Service ccredited to PRECIOUS METL BERING MTERILS (cont d) (cont d) Sweeps/Residues Copper Gravimetry u, g, Pd, Pt, Rh Fire ssay, ICP-OES u, Pd, Pt, Ir, Rh, Ru Gravimetry ICP-OES Silver Fire ssay, Gravimetry CHEMICLS: INORGNIC Nickel Carbonate, Oxide, Sulphate Nickel Gravimetry Rhenium Salts Rhenium Gravimetry Sulphur sh cidity Hydrocarbons Sulphur Gravimetry Chlorine UV/VIS Spectrophotometry DUSTS ND PRTICULTES l, Sb, s, Ba, Be, Bi, B, Cd, Ca, Cr, Co, Cu, Ga, In, Fe, Pb, Mg, Mn, Mo, Ni, Se, g, Sr, Te, Th, Sn, Ti, V, Zn ICP-OES ssessment Manager: DC1 Page 11 of 14
Schedule of ccreditation United Kingdom ccreditation Service ccredited to GLSS, OXIDES Boron Volumetric titration B, Ca, Li, Mg, l, Na, Pd, Rh, Ru ICP-OES lumina, Ba, Ca, Cr, Hf, Fe, Mn, Mg, P, K, Si, Na, Sr, Ti, V, Y, Zn, Zr XRF Spectrometry High grade Rhodium Rhodium ICP-OES FLUORSPR Ca, Fe, Pb, P, Si XRF Spectrometry Fluorine UV/VIS Spectrophotometry, Volumetric titration METLS: HIGH PURITY Multiple elements including but not limited to: l, Sb, s, Ba, Bi, Cd, Ca, Cr, Co, Cu, Ge, u, In, Ir, Fe, Pb, Mg, Mn, Mo, Ni, Os, Pd, P, Pt, K, Rh, Ru, Se, Si, g, Na, Sr, S, Te, Tl, Sn, Ti, V, U, Th, Y, Zn nalysis through the appropriate application of s following the Flexible Scope procedures Section 17 and SI236 Using the following techniques: cid digestion, microwave digestion or fusion peroxide followed by S or ICP luminium, Cadmium, Lead, Tin, Zinc l, Sb, s, Ba, Be, Bi, B, Cd, Ca, Cr, Co, Cu, Ga, In, Fe, Pb, Mg, Mn, Mo, Ni, K, Se, g, Na, Sr, Te, Tl, Sn, Ti, V, Zn S Silicon and Germanium UV/VIS Spectrophotometry ssessment Manager: DC1 Page 12 of 14
Schedule of ccreditation United Kingdom ccreditation Service ccredited to SOILS l, Sb, s, Ba, Be, Bi, B, Cd, Ca, Cr, Co, Cu, Ga, In, Fe, Pb, Mg, Mn, Mo, Ni, K, Se, g, Na, Sr, Te, Th, Sn, Ti, V, Zn S Gold Fire ssay, Gravimetry u, Ir, Pd, Pt, Rh, Ru Fire ssay, ICP-OES Silver S WTER, TRDE EFFLUENT (to sewer) l, Sb, s, Ba, Be, Bi, B, Cd, Ca, Cr, Co, Ga, In, Fe, Pb, MC, Mn, Hg, Mo, Ni, Se, g, Sr, Te, Tl, Sn, Ti, V, Zn S SCN PROFILE QULITTIVE/QUNTITTI VE ll Materials in Solution Base Metals ICP-OES Non-Metallic Materials Base/Precious Metals ICP-OES Metallic Materials and Solutions LL MTERILS (LISTED IN THIS SCHEDULE EXCEPT SOLUTIONS) Base/Precious Metals ICP-OES Physical Tests Moisture content Gravimetry Loss on Ignition Gravimetry Size nalysis Mesh Screening Specific Gravity Gravimetry ssessment Manager: DC1 Page 13 of 14
Schedule of ccreditation United Kingdom ccreditation Service ccredited to SOLID MINERL FUELS Hard Coal and Coke Sampling Manual sampling using documented In-House Method C7 in accordance with ISO 18283:2006 Hard Coal and Coke Sample Preparation Sample preparation using documented In-House Method C8 in accordance with ISO 18283:2006 Hard Coal and Coke Total Moisture Content Gravimetry using documented in-house method C9 based on ISO 18283:2006 Hard Coal Moisture content Gravimetry using documented In-House Method C1 based on ISO 11722:1999 Hard Coke Moisture content Gravimetry using documented In-House Method C2 based on ISO 687:2010 Hard Coal and Coke sh Content Gravimetry using documented In-House Method C3 based on ISO 1171:2010 Hard Coal and Coke Volatile Material Gravimetry using documented In-House Method C4 based on ISO 562:2010 Hard Coal and Coke Total Sulphur content Combustion and IR spectrometry using documented In-House Method C5 based on ISO 19579:2006 Hard Coal and Coke Gross Calorific value Combustion and IR calorimeter using documented In-House Method C6 based on ISO 1928:2009 B B B END ssessment Manager: DC1 Page 14 of 14