PROFICIENCY TESTING PROGRAMS PESTICIDES RESIDUES

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1 PROFICIENCY TESTING PROGRAMS PESTICIDES RESIDUES A19a Pesticides in fruits and citrus fruits A19b Pesticides in cereals A19c Pesticides in vegetables A19d Pesticides in fats A19e Pesticides in vegetables (bromides, nitrates) A19f Pesticides in wines A19g Pesticides in honeys A19h Pesticides in vegetables & fruits (dithiocarbamates) A19j Pesticides in Dairy Products A66 Multi-residue screening of pesticides in Food A = PTS accredited by COFRAC 1 / 11

2 19a- PESTICIDES IN FRUITS AND CITRUS FRUITS 68 participants worldwide 6 rounds per annual series Lemon Orange Apple Strawberry Peach Grape Fruits and Grape Acetamipride Bifenthrine Boscalide Carbendazime Carbofuran Cyprodinyl Dimethoate Diphenylamine Etephon Fenhexamid Fenitrothion Fludioxonil Glufosinate Kresoxym methyl Mandipropamide Mepanipyrim Metalaxyl-m Additional Molecules only on Grape Acrinathrine Etoxazole Benalaxyl Fenamidone Buprofezine Fenbuconazole Chlorpyriphos ethyl Flusilazole Chlorpyriphos methyl Fosetyl aluminium / Phosphorous acid (ethyl phosphite) Cyazofamide Hexytiazox Cyflufenamide Iprodione Cyproconazole Iprovalicarb Dimetomorphe Oxadixyl Citrus fruits Bifenthrine Buprofezine Carbendazime Chlorpyriphos ethyl Cyflufenamide Dimethoate Hexytiazox Imazalil Iprodione Malathion Omethoate Metrafenone Myclobutanil Omethoate Parathion methyl Phosalone Phosmet Pyraclostrobine Pyrimethanil Tebufenozide Thiaclopride Penconazole Permethrine Procymidone Proquinazide Spiroxamine Tebuconazole Tebufenpyrad Triadimenol Vinclozoline Orthophenylphenol Phosalone Phosmet Procymidone Thiabendazole 2 / 11

3 19B- PESTICIDES IN CEREALS 57 participants worldwide Common wheat Corn Feed Flour 2,4-D Ampa Bifenthrine Boscalide Chlormequat Chlorpyriphos ethyl Chlorpyriphos methyl Cypermethrine Diflufenican Fenitrothion Glyphosate Imidacloprid Malathion Mepiquat Metalaxyl-m Pendimetaline Permethrine Profenophos Propyconazole Pyrimiphos methyl Tebuconazole Thiametoxam Triazophos 3 / 11

4 19C- PESTICIDES IN VEGETABLES 57 participants worldwide 4 rounds per annual series Carrot Cabbage Green beans Lettuce Acetamipride Boscalide Carbofuran Chlorates Chlorprophame Chlorpyriphos ethyl Cyprodinyl Etephon Fludioxonil Flutolanil Fosetyl aluminium / acide phosphoreux (ethyl phosphite) Glufosinate Hydrazine maleique Imidacloprid Iprodione Linuron Metalaxyl-m Metoxuron Oxadixyl Phosmet Procymidone Propyzamide Pyrimethanil Tebufenozide Vinclozoline 4 / 11

5 19D- PESTICIDES IN FATS 41 participants worldwide 4 rounds per annual series Cheese Refined green olives Refined olive oil Soyabean Acetamipride Boscalide Carbofuran Chlorates Chlorprophame Chlorpyriphos ethyl Cyprodinyl Etephon Fludioxonil Flutolanil Fosetyl aluminium / acide phosphoreux (ethyl phosphite) Glufosinate Hydrazine maleique Imidacloprid Iprodione Linuron Metalaxyl-m Metoxuron Oxadixyl Phosmet Procymidone Propyzamide Pyrimethanil Tebufenozide Vinclozoline 5 / 11

6 19E- PESTICIDES IN VEGETABLES: NITRATES ET BROMIDES 55 participants worldwide 3 rounds per annual series. Lettuce Spinach Nitrates Bromides 6 / 11

7 19F- PESTICIDES IN WINES 53 participants worldwide 4 rounds per annual series Lettuce Spinach Azoxystrobin Benalaxyl Boscalide Carbendazim Chlorpyriphos-ethyl Chlorpyriphos-methyl Cyazofamide Cyproconazol Cyprodinil Dimethomorph Fenamidone Fenbuconazol Fenhexamide Fenitrothion Fludioxonil Flusilazol Fosetyl aluminium Iprodione Iprovalicarb Kresoxim-methyl Mandipropamid Mepanipyrime Metalaxil-M Metrafenone Myclobutanil Penconazol Procymidone Pyraclostrobin Pyrimethanil Spiroxamine Tebuconazol Tebufenozide Tebufenpyrade Vinclozolin 7 / 11

8 19G- PESTICIDES IN HONEYS 31 participants worldwide 4 rounds per annual series Honey Repellents against bees and varroacides: Acrinathrine Brompropylate Chlorfenvinphos Coumaphos Cymiazole DEET (diethyl toluamide) Deltamethrin Flumethrine Malathion Piperonil butoxide Tetradifon Tau fluvalinate Pesticides: Bifenthrine Boscalide Carbendazim Chlorpyrifos-ethyl Cypermethrin Lambda cyhalothrine Permethrin Thiaclopride 8 / 11

9 19H- PESTICIDES IN VEGETABLES & FRUITS (DITHIOCARBAMATES) Proficiency testing scheme created in participants worldwide 4 rounds per annual series Apple Endive Lettuce Dithiocarbamates form could be modified during annual series after decisions from the Committee, technical group or Chairperson. 9 / 11

10 19j- PESTICIDES IN DAIRY PRODUCTS Proficiency testing scheme created in 2016 PTS accredited by COFRAC 2 rounds per annual series Cheese Milk in powder form 2,4-D Bifenthrine Chlorpyriphos Ethyl Chlorpyriphos Methyl Cypermethrine DDT Endosulfan alpha Endosulfan bêta Endosulfan sulfate Endosulfans (sum) Fenitrothion Hexachlorobenzene Malathion Metalaxyl-M Parathion Methyl Pyrimiphos Methyl Pyroproxifen 10 / 11

11 66 - Multi-residue screening of pesticides Proficiency test created in 2013 Between 15 and 28 participants in the world 1 to 4 rounds per year For more details on the samples, please refer to the schedule. 66a - Fruits 66b - Cereals 66c Vegetables 66i Essential oils Spiking range: to mg/kg Between10 and 25 moleculesto identifyand quantify in blind among the followings: 2,4-D Acetamipride Acrinathrine AMPA Atrazine Bifenthrine Benalaxyl Bendiocarb Boscalide Bromopropylate Buprofezine Carbaryl Carbendazime Carbofuran Chlorates Chlorfenvinphos Chlorprophame Chlorpyriphos Ethyl Chlorpyriphos Methyl Coumaphos Cyazofamide Cyflufenamide Cymiazole Cypermethrine Cyproconazole Cyprodinyl DDT Diazinon Dicofol Diethyl toluamide (DEET) Difenoconazole Diflufenican Dimethoate Dimetomorphe Diphenylamine Endosulfan alpha Endosulfan bêta Endosulfan sulfate Endosulfans (somme) Etephon Ethion Etoxazole Fenamidone Fenbuconazole Fenhexamid Fenitrothion Fenproprathrine Fludioxonil Flumethrine Flusilazole Flutolanil Flutriafol HCH-alpha HCH-beta HCH-delta Hexachlorobenzene Hexytiazox Imidacloprid Imazalil Iprodione Iprovalicarb Kresoxym methyl Linuron Malathion Mandipropamide Mepanipyrim Metalaxyl-M Methidathion Metolachlor Metoxuron Metrafenone Myclobutanil Omethoate Orthophenylphenol Oxadixyl Oxidiazon Parathion Methyl Penconazole Pendimetaline Permethrine Phosalone Phosmet Prochloraz Procymidone Profenophos Propargite Propyconazole Propyzamide Proquinazide Pyraclostrobine Pyrimethanil Pyrimiphos Methyl Pyroproxifen Quintozene Spiroxamine Tau-fluvanilate Tebuconazole Tebufenozide Tebufenpyrad Tetraconazole Tetradifon Thiabendazole Thiaclopride Thiametoxam Triadimenol Triazophos Trifloxystrobine Trifluraline Vinclozoline NA => Non accredited matrix Note : BIPEA reserves the right to cancel the round in case of less than 12 participants. 11 / 11