26 course participants (16 nationalities representing institutes from 16 countries) 1 local attendant
|
|
|
- Brendan Baker
- 5 years ago
- Views:
Transcription
1 26 course participants (16 nationalities representing institutes from 16 countries) 1 local attendant 10 external lecturers and 10 tutors/lecturers from EMBL-Hamburg
2 EMBL Outstation at DESY, Hamburg years later Macromolecular crystallography EMBL synchrotron facilities 2 MX beamlines (P13, P14) at the upgraded Petra-3 Small-angle ring 1 scattering BioSAXS beamline (P12) Sample preparation and characterization facility (SPC) Absorption spectroscopy
3 Biological EMBL-HH Group leader: D. Svergun Staff : C.Jeffries, C.Blanchet, D.Franke, A.Kikhney, H.Mertens, C.Kerr, C.Borges Postdocs: A.Tuukkanen, M.Graewert, A.Spilotros, A.Panjkovich, M.Schroer, A.Gruzinov Predocs: N.Hajizadeh, K.Malanastas Major tasks: Development of data analysis methods Running and developing SAXS beamlines User support and collaborative projects Interactions, education and training
4 Small-angle scattering in structural biology Incident beam Wave vector k, k=2π/λ Radiation sources: X-ray tube (λ = nm) Synchrotron (λ = nm) Thermal neutrons (λ = nm) Complementary techniques MS Crystallography Bioinformatics AUC Sample Solvent FRET 2θ EM NMR Biochemistry EPR Detector Scattered beam, k 1 lg I, relative Additional information In preparation for an EMBO Course (courtesy of F.Gabel, IBS, Grenoble) Resolution, nm: s, nm -1 Homology models Orientations Scattering curve I(s) Atomic models Interfaces Data analysis Shape determination The new SAS book is not yet available for everyone (courtesy of M.Graewert, EMBL-HH) Distances Rigid body modelling Missing fragments Oligomeric mixtures Hierarchical systems Flexible systems
5 All new is well forgotten old On finishing my university studies, in 1936, I obtained a post as assistant, which gave me the opportunity to work towards my thesis My boss, who looked after my dissertation, was a crystallographer who kept an eye on my work rather distantly, but he did pass on a very good idea on me: to study, in addition to Bragg diffractions, diffuse scattering. <He> asked me to make a camera with monochromatic primary radiation and with minimum parasitic radiation That is why I studied especially small-angle scattering. I observed that the scattering is strong when the sample contains fine grains (10 to 100 nm). I produced next the means of determining the grain size from the scattering curve. It was the beginning of X-rays small-angle scattering Guinier, A. (1939). "La diffraction des rayons X aux tres petits angles; application a l'etude de phenomenes ultramicroscopiques." Ann. Phys. (Paris) 12:
6 When biologists go for SAS Care for a shape? This is just a trivial case: You will learn that SAXSMAN ( A.Kikhney) yields much, much more
7 High brilliance EMBL SAXS beamline P12 About ph/sec in 200*120 mm 2 Energy between 4 and 20 kev (3.0 to 0.6 Å) Divergence below 0.05*0.05 mrad 2 Multilayer monochromator mode: over ph/sec SASFLOW pipeline for on-line data processing and analysis Full automation, remote and mail-in access Robotic EMBL/ESRF sample changer Automated FPLC/HPLC in parallel with biophysical sample characterisation
8 ATSAS (All That SAS) roadmap Raw data Polydisperse systems Volume fractions of components Unfolded or flexible proteins Data reduction and processing Databases of computed and experimental patterns and models World most comprehensive program suite for small-angle scattering data analysis from biomacromolecular solutions Consists of more then 25 programs developed at EMBL-HH since 1991 Data regularization and overall structural parameters Available for download since 1999, accessible on-line since 2006 Presently, ATSAS has over 12,000 users from over 50 countries; on-line usage: 750 users/~30000 jobs per year Rigid body modelling Ab initio analysis Bead modelling Multiphase bead modelling Dummy residues modelling Add missing fragments to high resolution models High resolution models Computation of solution scattering from atomic models (X-rays and neutrons) Manual and local refinement Multisubunit complexes modelling Multidomain proteins modelling against multiple data sets Models superposition, averaging and clustering
9 Schedule of the Course Day 1 : Basics of small-angle scattering (Mon 17 Oct) Day 2 : From sample to data (Tue 18 Oct) Day 3 : From data to shape (Wed 19 Oct) Day 4 : Rigid body (hybrid) modelling (Thu 20 Oct) Day 5 : Mixtures and interacting systems (Fri 21 Oct) Day 6 : SAXS and complemenrary methods I (Sat 22 Oct) Day 7 : SAXS and complemenrary methods II (Sun 23 Oct) Day 8 : General discussion (Mon 03 Nov)
10 Lectures and Practicals Theory Lectures (48e Seminar Room, 2 nd floor) Software Demonstrations/Tutorials (48e Seminar Room, PC, LCD projector) Structural Biology Seminars (48e Seminar Room, 2 nd floor) Practicals: (P12 beamline and user room, 48e, ground floor). Data Analysis and SAXS Quest (48e Seminar Room, 2 nd floor)
11 SAXS Play Station V (anti-sleeping pills) SAXS Quest
12 Practical measurements at P12 Own samples Those who brought their own samples, shall measure them, analyse the data, and report the results at the end of the Course. No own samples Those who brought no samples, shall measure the alien proteins provided by us, analyse the data, and report the results at the end of the Course. Measurements on Tuesday SAXS/WAXS setup, smaller proteins Measurements on Thursday SAXS setup, larger proteins Measurements on Friday SAXS setup, reserved time
13 Whom to ask General questions: Dmitri Svergun (internal 125, mobile *127), Alexey Kikhney (170, mobile *150) Organizational questions: Margret Fischer (internal 110, mobile ) Sarah Marshall (111) Computer hardware: Felipo Goncalves (133) Computer software: Daniel Franke (244), Maxim Petoukhov (177), Peter Konarev (129), Haydyn Mertens (179) SAXS practicals: Clement Blanchet (192), Alessandro Spilotros (241), Melissa Graewert (115), Cy Jeffries (115), P12 (312) Emergency phone: SAXS group phone ( )
14 Miscellaneous Course photo: Saturday October 22, first coffee break Course dinner: Sunday October 23, as of 20:00 Pairing for the Quest: The list is given in the Course materials Quest winners will get very SAXSy prizes Quest run starts tomorrow Own laptops: network EMBLHH-guest (password available in the seminar room) Your presentations: 26 participants (with or without PPT, as you wish) 8 minutes per participant (SHARP: 6 min talk + 2 min questions)
A Brief Introduction to Structural Biology and Protein Crystallography
A Brief Introduction to Structural Biology and Protein Crystallography structural biology of H2O http://courses.cm.utexas.edu/jrobertus/ch339k/overheads-1/water-structure.jpg Protein polymers fold up into
Direct Correlation Between Ligand-Induced α- Synuclein Oligomers and Amyloid-like Fibril Growth. Supplementary Information
Direct Correlation Between Ligand-Induced α- Synuclein Oligomers and Amyloid-like Fibril Growth Supplementary Information Martin Nors Perdersen 1, Vito Foderà 1, Istvan Horvath 2, Andreas van Maarschalkerweerd
Small-angle X-ray scattering (SAXS) with synchrotron radiation
Small-angle X-ray scattering (SAXS) with synchrotron radiation Martin Müller Institut für Experimentelle und Angewandte Physik der Christian-Albrechts-Universität zu Kiel Introduction to small-angle scattering
Florent Bernaudat scientific coordinator
Florent Bernaudat scientific coordinator The Partners International Institutions: Institut Laue Langevin European Synchrotron Radiation Facility European Molecular Biology Laboratory National Institution:
Characterization by solution small angle X-ray scattering of the oligomeric state of structural genomics protein targets
SUNY College of Environmental Science and Forestry Digital Commons @ ESF Honors Theses 5-2013 Characterization by solution small angle X-ray scattering of the oligomeric state of structural genomics protein
X-Ray Diffraction by Macromolecules
N. Kasai M. Kakudo X-Ray Diffraction by Macromolecules With 351 Figures and 56 Tables Kodansha ~Springer ... Contents Preface v Part I Fundamental 1. Essential Properties of X-Rays................. 3 1.1
The Partners 05/03/2015. Florent Bernaudat scientific coordinator. International Institutions: Institut Laue Langevin
Florent Bernaudat scientific coordinator The Partners International Institutions: Institut Laue Langevin European Synchrotron Radiation Facility European Molecular Biology Laboratory National Institution:
Proposal by EMBL-Hamburg. for an Integrated Life Science Centre at PETRA-III
Proposal by EMBL-Hamburg Hamburg, August 2004 Contributors (EMBL-Hamburg): Stefan Fiedler (instrumentation) Arie Geerlof (sample preparation) Matthew Groves (MX) Christoph Hermes (instrumentation) Malgorzata
Stress Mitigation of X-ray Beamline Monochromators using a Topography Test Unit
128 Stress Mitigation of X-ray Beamline Monochromators using a Topography Test Unit J. Maj 1, G. Waldschmidt 1 and A. Macrander 1, I. Koshelev 2, R. Huang 2, L. Maj 3, A. Maj 4 1 Argonne National Laboratory,
Atomic Densities. Linear Density. Planar Density. Linear Density. Outline: Planar Density
Atomic Densities Outline: Atomic Densities - Linear Density - Planar Density Single- vs poly- crystalline materials X-ray Diffraction Example Polymorphism and Allotropy Linear Density Number of atoms per
Instrument Configuration for Powder Diffraction
Instrument Configuration for Powder Diffraction Advanced X-ray Workshop S.N. Bose National Centre for Basic Sciences, 14-15/12/2011 Innovation with Integrity Overview What is the application? What are
Structure of crystallographically challenged hydrogen storage materials using the atomic pair distribution function analysis
Structure of crystallographically challenged hydrogen storage materials using the atomic pair distribution function analysis H. Kim, 1 K. Sakaki, 1 K. Asano, 1 M. Yamauchi, 2 A. Machida, 3 T. Watanuki,
European Molecular Biology Laboratory (EMBL) Hamburg by Matthias Wilmanns, Head of Outstation
European Molecular Biology Laboratory (EMBL) Hamburg by Matthias Wilmanns, Head of Outstation During the year 2000, the EMBL Hamburg Outstation has continued to provide the scientific community with its
X-ray diffraction. Talián Csaba Gábor University of Pécs, Medical School Department of Biophysics
X-ray diffraction Talián Csaba Gábor University of Pécs, Medical School Department of Biophysics 2012.10.11. Outline of the lecture X-ray radiation Interference, diffraction Crystal structure X-ray diffraction
Earth & Planetary Science Applications of X-Ray Diffraction: Advances Available for Research with our New Systems
Earth & Planetary Science Applications of X-Ray Diffraction: Advances Available for Research with our New Systems James R. Connolly Dept. of Earth & Planetary Sciences University of New Mexico 401/501
Fundamentals of Crystalline State p. 1 Introduction p. 1 Crystalline state p. 2 Crystal lattice and crystal structure p. 4 Shape of the unit cell p.
Preface p. xvii Fundamentals of Crystalline State p. 1 Introduction p. 1 Crystalline state p. 2 Crystal lattice and crystal structure p. 4 Shape of the unit cell p. 6 Content of the unit cell p. 7 Asymmetric
PRESS - KIT CRYO-EM PLATFORM. Inauguration of the cryo-electron microscopy platform. Friday 10 November ESRF - Grenoble (France)
PRESS - KIT CRYO-EM PLATFORM Inauguration of the cryo-electron microscopy platform Friday 10 November 2017 ESRF - Grenoble (France) Characteristics of the ESRF cryo-em A brand new cryo-electron microscope
Chapter 3 Basic Crystallography and Electron Diffraction from Crystals. Lecture 9. Chapter 3 CHEM Fall, L. Ma
Chapter 3 Basic Crystallography and Electron Diffraction from Crystals Lecture 9 Outline The geometry of electron diffraction Crystallography Kinetic Theory of Electron diffraction Diffraction from crystals
Lecture C4b Microscopic to Macroscopic, Part 4: X-Ray Diffraction and Crystal Packing
Lecture C4b Microscopic to Macroscopic, Part 4: X-Ray Diffraction and Crystal Packing X-ray Diffraction Max von Laue won the 1914 Nobel Prize for his discovery of the diffraction of x-rays by crystals.
Defect depth profiling of CdZnTe using high-energy diffraction measurements
Defect depth profiling of CdZnTe using high-energy diffraction measurements M.S. Goorsky, a H. Yoon, a M. Ohler, b K. Liss b a Department of Materials Science and Engineering University of California,
Travaux Pratiques de Matériaux de Construction
Travaux Pratiques de Matériaux de Construction Section Matériaux 6 ème semestre 2009 Etude de Matériaux Cimentaire Par Diffraction des Rayons X Responsable: Silke Ruffing E-Mail: silke.ruffing@epfl.ch
Structural Biology. Single crystal X-ray diffraction and SAXS. Systems designed for structural biology
Structural Biology Single crystal X-ray diffraction and SAXS Systems designed for structural biology Rigaku Oxford Diffraction THE POWER OF SYNERGY Combining the single crystal groups from Rigaku and Oxford
Fundamentals of Crystalline State and Crystal Lattice p. 1 Crystalline State p. 2 Crystal Lattice and Unit Cell p. 4 Shape of the Unit Cell p.
Fundamentals of Crystalline State and Crystal Lattice p. 1 Crystalline State p. 2 Crystal Lattice and Unit Cell p. 4 Shape of the Unit Cell p. 7 Crystallographic Planes, Directions, and Indices p. 8 Crystallographic
Lesson 1 Good Diffraction Data
Lesson 1 Good Diffraction Data Nicola Döbelin RMS Foundation, Bettlach, Switzerland Digital Diffractometers Transmission Geometry Debye-Scherrer Geometry Reflective Geometry Bragg-Brentano Geometry Glass
Atomic Densities. Linear Density Number of atoms per length whose centers lie on the direction vector for a specific crystallographic direction.
Atomic Densities Linear Density Number of atoms per length whose centers lie on the direction vector for a specific crystallographic direction. Planar Density Number of atoms per unit area that are centered
X-RAY DIFFRACTION IN SEMICONDUCTOR INDUSTRY AND RESEARCH
X-RAY DIFFRACTION IN SEMICONDUCTOR INDUSTRY AND RESEARCH M. Leszczyński High Pressure Research Center UNIPRESS, Sokolowska 29/37, 01 142 Warsaw, Poland, e-mail: mike@unipress.waw.pl ABSTRACT The paper
Fundamentals of X-ray diffraction and scattering
Fundamentals of X-ray diffraction and scattering Don Savage dsavage@wisc.edu 1231 Engineering Research Building (608) 263-0831 X-ray diffraction and X-ray scattering Involves the elastic scattering of
eresearch Tools for the Australian Synchrotron User Community
eresearch Tools for the Australian Synchrotron User Community Uli Felzmann Australian Synchrotron ICALEPCS 2013 San Francisco AUSTRALIAN SYNCHROTRON Located at 800 Blackburn Road, Clayton, Victoria (Melbourne)
LECTURE 7. Dr. Teresa D. Golden University of North Texas Department of Chemistry
LECTURE 7 Dr. Teresa D. Golden University of North Texas Department of Chemistry Diffraction Methods Powder Method For powders, the crystal is reduced to a very fine powder or microscopic grains. The sample,
Atomic resolution data collection with the PILATUS3 R 1M detector on a metaljet X-ray source. Application Note 29-May-18
Atomic resolution data collection with the PILATUS3 R 1M detector on a metaljet X-ray source Claudio Klein, GmbH, Norderstedt 1 1. Introduction Home X-ray sources have limited capabilities compared to
Lecture C4a Microscopic to Macroscopic, Part 4: X-Ray Diffraction and Crystal Packing
Lecture C4a Microscopic to Macroscopic, Part 4: X-Ray Diffraction and Crystal Packing X-ray Diffraction Max von Laue won the 1914 Nobel Prize for his discovery of the diffraction of x-rays by crystals.
World-class beamlines for Australian science
World-class beamlines for Australian science 2 First tranche beamlines 3 In just 11 years of operation, the Australian Synchrotron has emerged as one of Australia s most important pieces of landmark scientific
Pasteur course. 2 nd INTEGRATIVE STRUCTURAL BIOLOGY
Pasteur course 2 nd INTEGRATIVE STRUCTURAL BIOLOGY PROGRAM 2016-2017 Pasteur course 2 nd INTEGRATIVE STRUCTURAL BIOLOGY 2016-2017 (17 22 July, 2017) Course Organizers Claudine Mayer Michael Nilges Nicolas
Protein Crystallography: Tutorial on Crystal Structure Determination
ICTP School on Synchrotron Radiation and Application Trieste 10.05.04 Protein Crystallography: Tutorial on Crystal Structure Determination Alberto Cassetta CNR - Istituto di Cristallografia Trieste Summary
[CRYSTALLIZATION AND DIFFRACTION] Fall Weeks Course. Crystallization and Diffraction GOALS
![[CRYSTALLIZATION AND DIFFRACTION] Fall Weeks Course. Crystallization and Diffraction GOALS](/thumbs/83/87620905.jpg "[CRYSTALLIZATION AND DIFFRACTION] Fall Weeks Course. Crystallization and Diffraction GOALS")
Crystallization and Diffraction Practical course in Protein Crystallization and X-Ray Diffraction Session: Lecture: 60 min; Lab: 90 min; Q&A: 30 min; 3 weeks 2 sessions/week GOALS The practical course
The object of this experiment is to test the de Broglie relationship for matter waves,
Experiment #58 Electron Diffraction References Most first year texts discuss optical diffraction from gratings, Bragg s law for x-rays and electrons and the de Broglie relation. There are many appropriate
Nanoconfinement Crystallization of Frustrated Alkyl Groups: Crossover of Mesophase to Crystalline Structure
Nanoconfinement Crystallization of Frustrated Alkyl Groups: Crossover of Mesophase to Crystalline Structure Haifeng Shi,,,* Haixia Wang, John H. Xin, Xingxiang Zhang, and Dujin Wang, * State Key Laboratory
Computational Structural Biology Research Unit
Computational Structural Biology Research Unit 1. Team members Florence Tama (Unit Leader) Atsushi Tokuhisa (Research Scientist) Sachiko Kikumoto (Assistant) 2. Research Activities Biological molecular
X-ray diffraction
2.2.3.- X-ray diffraction 2.2.3.1.- Origins and fundamentals of the technique The first experimental evidence concerning x-ray diffraction was given by Max von Laue who in 1912 demonstrated that x-rays
Single crystal X-ray diffraction. Zsolt Kovács
Single crystal X-ray diffraction Zsolt Kovács based on the Hungarian version of the Laue lab description which was written by Levente Balogh, Jenő Gubicza and Lehel Zsoldos INTRODUCTION X-ray diffraction
X-Ray Analytical Methods
X-Ray Analytical Methods X-rays were discovered by W.C. Röentgen in 1895, and led to three major uses: X-ray radiography is used for creating images of light-opaque materials relies on the relationship
Steps in solving a structure. Diffraction experiment. Obtaining well-diffracting crystals. Three dimensional crystals
Protein structure from X-ray diffraction Diffraction images: ciprocal space Protein, chemical structure: IALEFGPSLKMNE Conformation, 3D-structure: CRYST1 221.200 73.600 80.900 90.00 90.00 90.00 P 21 21
MATERIALS SCIENCE & ENGINEERING. MSE 8803F Advanced X-ray Diffraction and Scattering
MATERIALS SCIENCE & ENGINEERING MSE 8803F Advanced X-ray Diffraction and Scattering (3 credit hours) Instructors: R. Snyder, and H. Garmestani Lecture: 3:05 pm - 3:55 pm MWF Instr Center 109 Laboratory:
Materials Lab 1(MT344) X-ray Diffractometer Operation and Data Analysis. Instructor: Dr. Xueyan Wu ( 吴雪艳 )
Materials Lab 1(MT344) X-ray Diffractometer Operation and Data Analysis Instructor: Dr. Xueyan Wu ( 吴雪艳 ) Goals To give students a practical introduction into the use of X-ray diffractometer and data collection.
9/29/2014 8:52 PM. Chapter 3. The structure of crystalline solids. Dr. Mohammad Abuhaiba, PE
1 Chapter 3 The structure of crystalline solids 2 Home Work Assignments HW 1 2, 7, 12, 17, 22, 29, 34, 39, 44, 48, 53, 58, 63 Due Sunday 12/10/2014 Quiz # 1 will be held on Monday 13/10/2014 at 11:00 am
Methodological Aspects of the Highenergy Synchrotron X-ray Diffraction Technique for Internal Stress Evaluation
Journal of Neutron Research, Vol. 9, pp. 495 501 Reprints available directly from the publisher Photocopying permitted by license only q 2001 OPA (Overseas Publishers Association) N.V. Published by license
Possibilities and limitations of X-ray diffraction using high-energy X-rays on a laboratory system
Z. Kristallogr. Suppl. 30 (2009) 163-169 / DOI 10.1524/zksu.2009.0023 163 by Oldenbourg Wissenschaftsverlag, München Possibilities and limitations of X-ray diffraction using high-energy X-rays on a laboratory
BM29 BM29: BIOSAXS BEAMLINE STATUS AND NEWS. Petra Pernot ESRF 5 th February 2018 BAG Meeting. Page 1
BM29: BIOSAXS BEAMLINE STATUS AND NEWS BM29 Petra Pernot ESRF 5 th February 2018 BAG Meeting Page 1 BIOSAXS LCS Mark Tully: ESRF scientist - started March 2017 Martha Brennich: EMBL scientist - formerly
Benchtop XRD diffractometer. MiniFlex. Analysis of materials by X-ray diffraction
Benchtop XRD diffractometer MiniFlex Analysis of materials by X-ray diffraction More power More flexibility More results The new MiniFlex is available in two models. The MiniFlex 600 is the most powerful
MiniFlex. Analysis of materials by X-ray diffraction. Benchtop XRD diffractometer
MiniFlex Analysis of materials by X-ray diffraction Benchtop XRD diffractometer More power More flexibility More results The new MiniFlex is available in two models. The MiniFlex 600 is the most powerful
FOCUSING POLYCAPILLARY OPTICS FOR DIFFRACTION
Copyright (c)jcpds-international Centre for Diffraction Data 2002, Advances in X-ray Analysis, Volume 45. 325 FOCUSING POLYCAPILLARY OPTICS FOR DIFFRACTION H. Huang a, C. A. MacDonald a, W. M. Gibson a,b,
In Situ X-ray Fluorescence Measurements During Atomic Layer Deposition: Nucleation and
In Situ X-ray Fluorescence Measurements During Atomic Layer Deposition: Nucleation and Growth of TiO 2 on Planar Substrates and in Nanoporous Films 1 and In-Situ Synchrotron X-Ray Scattering Study of Thin
Supplementary Information
Time-resolved X-ray Tracking of Expansion and Compression Dynamics in Supersaturating Ion-Networks Y. Matsushita 1, H. Sekiguchi 2, K. Ichiyanagi 3, N. Ohta 2 K. Ikezaki 1, Y. Goto 4, Y. C. Sasaki 1,2
Identification of Crystal Structure and Lattice Parameter. for Metal Powders Using X-ray Diffraction. Eman Mousa Alhajji
Identification of Crystal Structure and Lattice Parameter for Metal Powders Using X-ray Diffraction Eman Mousa Alhajji North Carolina State University Department of Materials Science and Engineering MSE
Key crystallographic concepts: Theory of diffraction. (Crystallography y without tears, Part 1)
Protein Crystallography (3) Key crystallographic concepts: Theory of diffraction. (Crystallography y without tears, Part 1) Cele Abad-Zapatero University of Illinois at Chicago Center for Pharmaceutical
This lecture is part of the Basic XRD Course.
This lecture is part of the Basic XRD Course. Basic XRD Course 1 A perfect polycrystalline sample should contain a large number of crystallites. Ideally, we should always be able to find a set of crystallites
OPTIMIZING XRD DATA. By: Matthew Rayner
OPTIMIZING XRD DATA By: Matthew Rayner 1 XRD Applications PANalytical classifies XRD applications in 4 groups 1. Powders 2. Nanomaterials 3. Solid objects 4. Thin films Many day-to-day samples cross these
What if your diffractometer aligned itself?
Ultima IV Perhaps the greatest challenge facing X-ray diffractometer users today is how to minimize time and effort spent on reconfiguring of the system for different applications. Wade Adams, Ph.D., Director,
Microdroplet Sample Mounting Techniques in Small Angle X-Ray. Scattering. Andrew P. Huang
Microdroplet Sample Mounting Techniques in Small Angle X-Ray Scattering Andrew P. Huang Office of Science, Science Undergraduate Laboratory Internship (SULI) Washington University in St. Louis Stanford
The multi-scale architecture of cellulose in plant cell wall systems investigated by small angle scattering techniques
The multi-scale architecture of cellulose in plant cell wall systems investigated by small angle scattering techniques Marta Martinez-Sanz mmartinez@iata.csic.es The Plant Cell Wall The plant cell wall
TEM and Electron Diffraction Keith Leonard, PhD (1999) U. Cincinnati
TEM and Electron Diffraction Keith Leonard, PhD (1999) U. Cincinnati Electron Microscopes: Electron microscopes, such as the scanning electron microscope (SEM) and transmission electron microscope (TEM)
HIGH-RESOLUTION PARALLEL-BEAM POWDER DIFFRACTION MEASUREMENT OF SUB-SURFACE DAMAGE IN ALUMINA-SILICON CARBIDE NANOCOMPOSITE
169 HIGH-RESOLUTION PARALLEL-BEAM POWDER DIFFRACTION MEASUREMENT OF SUB-SURFACE DAMAGE IN ALUMINA-SILICON CARBIDE NANOCOMPOSITE B K Tanner, H Z Wu + and S G Roberts * Department of Physics, University
ATTACHMENTES FOR APD 2000 PRO POWDER X-RAY DIFFRACTOMETER. Monochromators
Monochromators Secondary graphite monochromator Johansson Ka 1 monochromator Parabolic monochromator Secondary flat and curved graphite monochromators suitable for Ag, Cr, Fe, Cu, Co and Mo radiations
Aeris. Research edition
Aeris Research edition It s like making a cup of coffee except it s even easier Watch our video on www.xrdiseasy.com Surprisingly intuitive Meet the Research edition of Aeris PANalytical s easy-to-operate
Introduction to Powder Diffraction/Practical Data Collection
Durham University Chemistry Department Introduction to Powder Diffraction/Practical Data Collection Dr Ivana Evans Durham, January 2007 Durham Outline Information in a powder pattern What is diffraction
LECTURE 8. Dr. Teresa D. Golden University of North Texas Department of Chemistry
LECTURE 8 Dr. Teresa D. Golden University of North Texas Department of Chemistry Practical applications for lattice parameter measurements: -determine composition (stoichiometry) of the sample -determine
Basics of XRD part IV
Basics of XRD part IV Dr. Peter G. Weidler Institute of Functional Interfaces IFG 1 10/31/17 KIT The Research University in the Helmholtz Association Name of Institute, Faculty, Department www.kit.edu
Combining microfluidics and synchrotron SAXS to investigate biomoleculesin solution
Structural Biophysics group, Niels Bohr Institute Combining microfluidics and synchrotron SAXS to investigate biomoleculesin solution Lise Arleth Structural Biophysics Group, Niels Bohr Institute University
Grazing Incidence X-Ray Diffraction of Longitudinal and Perpendicular Magnetic Recording Media for HDD
Grazing Incidence X-Ray Diffraction of Longitudinal and Perpendicular Magnetic Recording Media for HDD Michio OHSAWA, Fuji Electric Corporate Research and Development, Ltd. ohsawa-michio@fujielectric.co.jp
This experiment is included in the upgrade packages: XRC 4.0 X-ray characteristics and XRS 4.0 X-ray structural analysis.
Characteristic X-rays of copper TEP Related Topics X-ray tube, bremsstrahlung, characteristic radiation, energy levels, crystal structures, lattice constant, absorption, absorption edges, interference,
Pace University Request for Proposal Contracting Services
Pace University Request for Proposal Contracting Services Addendum #1 Dated: 4/20/07 Pace University seeks proposals to provide general contracting services related to the renovations of the theater at
11.3 The analysis of electron diffraction patterns
11.3 The analysis of electron diffraction patterns 277 diameter) Ewald reflecting sphere, the extension of the reciprocal lattice nodes and the slight buckling of the thin foil specimens all of which serve
Full report available at genomicscience.energy.gov/userfacilities/structuralbiologyworkshop/
Full report available at genomicscience.energy.gov/userfacilities/structuralbiologyworkshop/ a Applications of New DOE National User Facilities in Biology Workshop May 2011 Convened by U.S. Department
Characterization of Materials Using X-Ray Diffraction Powder Diffraction
Praktikum III, Fall Term 09 Experiment P1/P2; 23.10.2009 Characterization of Materials Using X-Ray Diffraction Powder Diffraction Authors: Michael Schwarzenberger (michschw@student.ethz.ch) Philippe Knüsel
Multiscale investigations on tracheids and ray. parenchyma cells of spruce
Multiscale investigations on tracheids and ray Kari Pirkkalainen www.helsinki.fi/yliopisto 5.10.2010 1 The people behind the work Kari Pirkkalainen Pekka Saranpää Kirsi Leppänen Prof. Ritva Serimaa Marko
Example: Compute the wavelength of a 1 [kg] block moving at 1000 [m/s].
![Example: Compute the wavelength of a 1 [kg] block moving at 1000 [m/s].](/thumbs/95/123245062.jpg "Example: Compute the wavelength of a 1 [kg] block moving at 1000 [m/s].")
Example: Calculate the energy required to excite the hydrogen electron from level n = 1 to level n = 2. Also calculate the wavelength of light that must be absorbed by a hydrogen atom in its ground state
Diffraction Basics. The qualitative basics:
The qualitative basics: Diffraction Basics Coherent scattering around atomic scattering centers occurs when x-rays interact with material In materials with a crystalline structure, x-rays scattered in
Synchrotron Science and Protein Crystallography
Your Brief You will work with your mentors to grow protein crystals and use X-ray diffraction sources to study the crystal structure of lysozyme. You will have an overall view of what it takes to study
The first measurement will be performed with a sample temperature of 35 by executing the following steps:
Work Instructions The experimental procedure of this practical is subdivided into two parts. In one part, a phase diagram of DEPE lipids is scanned through different temperatures, where a phase transition
Travaux Pratiques de Matériaux de Construction. Etude de Matériaux Cimentaires par Diffraction des Rayons X sur Poudre
Travaux Pratiques de Matériaux de Construction Section Matériaux 6 ème semestre 2015 Etude de Matériaux Cimentaires par Diffraction des Rayons X sur Poudre Study Cementitious Materials by X-ray diffraction
conference papers Anomalous small- and wide-angle X-ray scattering and X-ray absorption spectroscopy for Pt and Pt Ru nanoparticles
Journal of Applied Crystallography ISSN 0021-8898 Anomalous small- and wide-angle X-ray scattering and X-ray absorption spectroscopy for Pt and Pt Ru nanoparticles Received 14 August 2006 Accepted 11 January
Computational methods in bioinformatics: Lecture 1
Computational methods in bioinformatics: Lecture 1 Graham J.L. Kemp 2 November 2015 What is biology? Ecosystem Rain forest, desert, fresh water lake, digestive tract of an animal Community All species
Micro- and Nano-Technology... for Optics
Micro- and Nano-Technology...... for Optics 3.2 Lithography U.D. Zeitner Fraunhofer Institut für Angewandte Optik und Feinmechanik Jena Electron Beam Column electron gun beam on/of control magnetic deflection
HOLIDAY SCHEDULE
2018-2019 HOLIDAY SCHEDULE Happy Holidays! Below you ll find our holiday schedules from now through New Year s Day. Please contact Customer Service if you have any questions. EXTENDED SEASONAL CUSTOMER
BIOLOGIA STRUTTURALE
LUCI DI SINCROTRONE Presente e futuro delle grandi sorgenti di raggi X e UV italiane nel contesto europeo: BIOLOGIA STRUTTURALE Martino Bolognesi Dept. BioSciences University of Milano, Italy Biological
Thermo Scientific ARL EQUINOX X-ray Diffractometers
Thermo Scientific ARL EQUINOX 1000 X-ray Diffractometers High performance in a compact size Thermo Scientific ARL EQUINOX 1000 X-ray diffractometer (XRD) is designed to meet structural and phase analysis
FIP -BM30A: an automated beamline for protein crystallography
FIP -BM30A: an automated beamline for protein crystallography Automated (Xnemo) Cryogenic Automated Transfer System (CATS) Automated Data Processing (ADP) J.-L. Ferrer FIP-BM30A / ESRF Institut de Biologie
High Brilliance Beamline ID02
High Brilliance Beamline ID02 1. Guidelines for sample preparation 2. Sample environments 3. Shipping of samples contacts for further question: M. Sztucki, +33 (0)4 76 88 28 93, sztucki@esrf.eu T. Narayanan,
9/16/ :30 PM. Chapter 3. The structure of crystalline solids. Mohammad Suliman Abuhaiba, Ph.D., PE
Chapter 3 The structure of crystalline solids 1 Mohammad Suliman Abuhaiba, Ph.D., PE 2 Home Work Assignments HW 1 2, 7, 12, 17, 22, 29, 34, 39, 44, 48, 53, 58, 63 Due Sunday 17/9/2015 3 Why study the structure
X-ray Powder Diffraction in Catalysis
X-ray Powder Diffraction in Catalysis 0/63 Introduction Introduction: scope of this lecture This lecture is designed as a practically oriented guide to powder XRD in catalysis, not as an introduction into
Computational Structural Biology Research Unit
Computational Structural Biology Research Unit 1. Unit members Florence Tama (Unit Leader) Atsushi Tokuhisa (Research Scientist) Sachiko Kikumoto (Assistant) 2. Research Activities Biological molecular
Workunit: P Title:MT
Workunit: P000003 Title:MT Model Summary: Model information: Modelled residue range: 48 to 340 Quaternary structure information: Based on template: 3aptA (1.85 A) Template (3aptA): Unknown Sequence Identity
Basic Energy Sciences
Basic Energy Sciences Board on Physics and Astronomy Keck Center of the National Academies April 27, 2012 Harriet Kung Director, Office of Basic Energy Sciences Office of Science, U.S. Department of Energy
Physical structure of matter. Monochromatization of molybdenum X-rays X-ray Physics. What you need:
X-ray Physics Physical structure of matter Monochromatization of molybdenum X-rays What you can learn about Bremsstrahlung Characteristic radiation Energy levels Absorption Absorption edges Interference
Kinematical theory of contrast
Kinematical theory of contrast Image interpretation in the EM the known distribution of the direct and/or diffracted beam on the lower surface of the crystal The image on the screen of an EM = the enlarged
Lesson 1 X-rays & Diffraction
Lesson 1 X-rays & Diffraction Nicola Döbelin RMS Foundation, Bettlach, Switzerland February 11 14, 2013, Riga, Latvia Electromagnetic Spectrum X rays: Wavelength λ: 0.01 10 nm Energy: 100 ev 100 kev Interatomic
Organizing Committee Scientific Committee
PROGRAM Organizing Committee Amit Kohn (Tel Aviv University) Zahava Barkay (Tel Aviv University) Ben Britton (Imperial College) Scientific Committee Amit Kohn (Materials Science, Tel Aviv University) Zahava
Pasteur course. 3 rd INTEGRATIVE STRUCTURAL BIOLOGY
Pasteur course 3 rd INTEGRATIVE STRUCTURAL BIOLOGY PROGRAM 2017-2018 Pasteur course 3 rd INTEGRATIVE STRUCTURAL BIOLOGY 2017-2018 (16-20 July, 2018) Course Organizers Claudine Mayer Michael Nilges Nicolas
INVESTIGATION OF LOCAL TEXTURES IN EXTRUDED MAGNESIUM BY SYNCHROTRON RADIATION
Copyright JCPDS - International Centre for Diffraction Data 2003, Advances in X-ray Analysis, Volume 46. 151 INVESTIGATION OF LOCAL TEXTURES IN EXTRUDED MAGNESIUM BY SYNCHROTRON RADIATION Heinz-Günter
Thin Film Scattering: Epitaxial Layers
Thin Film Scattering: Epitaxial Layers 6th Annual SSRL Workshop on Synchrotron X-ray Scattering Techniques in Materials and Environmental Sciences: Theory and Application May 29-31, 2012 Thin films. Epitaxial