T A B L E O F C O N T E N T S VOLUME ONE PART I METHODS FOR ANALYTES AND PROPERTIES
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1 T A B L E O F C O N T E N T S VOLUME ONE SECTION A DISCLAIMER ABSTRACT TABLE OF CONTENTS METHOD INDEX AND CONVERSION TABLE PREFACE ACKNOWLEDGEMENTS PART I METHODS FOR ANALYTES AND PROPERTIES CHAPTER ONE -- QUALITY CONTROL 1.0 Introduction 2.0 QA Project Plan 3.0 Field Operations 4.0 Laboratory Operations 5.0 Definitions 6.0 References CHAPTER TWO -- CHOOSING THE CORRECT PROCEDURE 2.1 Purpose 2.2 Required Information 2.3 Implementing the Guidance 2.4 Characteristics 2.5 Ground Water 2.6 References CHAPTER THREE -- METALLIC ANALYTES 3.1 Sampling Considerations 3.2 Sample Preparation Methods Method 3005A: Acid Digestion of Waters for Total Recoverable or Dissolved Metals for Analysis by Flame Atomic Absorption (FLAA) or Inductively Coupled Plasma (ICP) Spectroscopy CD-ROM CONTENTS - 1 Revision 3
2 Method 3010A: Method 3015: Method 3020A: Method 3040: Method 3050A: Method 3051: Acid Digestion of Aqueous Samples and Extracts for Total Metals for Analysis by Flame Atomic Absorption (FLAA) or Inductively Coupled Plasma (ICP) Spectroscopy Microwave Assisted Acid Digestion of Aqueous Samples and Extracts Acid Digestion of Aqueous Samples and Extracts for Total Metals for Analysis by Graphite Furnace Atomic Absorption (GFAA) Spectroscopy Dissolution Procedure for Oils, Greases, or Waxes Acid Digestion of Sediments, Sludges, and Soils Microwave Assisted Acid Digestion of Sediments, Sludges, Soils, and Oils 3.3 Methods for Determination of Metals Method 6010A: Method 6020: Method 7000A: Method 7020: Method 7040: Method 7041: Method 7060A: Method 7061A: Method 7062: Method 7080A: Method 7081: Method 7090: Method 7091: Method 7130: Method 7131A: Method 7140: Method 7190: Method 7191: Method 7195: Method 7196A: Method 7197: Method 7198: Method 7200: Method 7201: Method 7210: Method 7211: Method 7380: Method 7381: Method 7420: Method 7421: Inductively Coupled Plasma-Atomic Emission Spectroscopy Inductively Coupled Plasma - Mass Spectrometry Atomic Absorption Methods Aluminum (AA, Direct Aspiration) Antimony (AA, Direct Aspiration) Antimony (AA, Furnace Technique) Arsenic (AA, Furnace Technique) Arsenic (AA, Gaseous Hydride) Antimony and Arsenic (AA, Borohydride Reduction) Barium (AA, Direct Aspiration) Barium (AA, Furnace Technique) Beryllium (AA, Direct Aspiration) Beryllium (AA, Furnace Technique) Cadmium (AA, Direct Aspiration) Cadmium (AA, Furnace Technique) Calcium (AA, Direct Aspiration) Chromium (AA, Direct Aspiration) Chromium (AA, Furnace Technique) Chromium, Hexavalent (Coprecipitation) Chromium, Hexavalent (Colorimetric) Chromium, Hexavalent (Chelation/Extraction) Chromium, Hexavalent (Differential Pulse Polarography) Cobalt (AA, Direct Aspiration) Cobalt (AA, Furnace Technique) Copper (AA, Direct Aspiration) Copper (AA, Furnace Technique) Iron (AA, Direct Aspiration) Iron (AA, Furnace Technique) Lead (AA, Direct Aspiration) Lead (AA, Furnace Technique) CD-ROM CONTENTS - 2 Revision 3
3 Method 7430: Method 7450: Method 7460: Method 7461: Method 7470A: Method 7471A: Method 7480: Method 7481: Method 7520: Method 7550: Method 7610: Method 7740: Method 7741A: Method 7742: Method 7760A: Method 7761: Method 7770: Method 7780: Method 7840: Method 7841: Method 7870: Method 7910: Method 7911: Method 7950: Method 7951: Lithium (AA, Direct Aspiration) Magnesium (AA, Direct Aspiration) Manganese (AA, Direct Aspiration) Manganese (AA, Furnace Technique) Mercury in Liquid Waste (Manual Cold-Vapor Technique) Mercury in Solid or Semisolid Waste (Manual Cold-Vapor Technique) Molybdenum (AA, Direct Aspiration) Molybdenum (AA, Furnace Technique) Nickel (AA, Direct Aspiration) Osmium (AA, Direct Aspiration) Potassium (AA, Direct Aspiration) Selenium (AA, Furnace Technique) Selenium (AA, Gaseous Hydride) Selenium (AA, Borohydride Reduction) Silver (AA, Direct Aspiration) Silver (AA, Furnace Technique) Sodium (AA, Direct Aspiration) Strontium (AA, Direct Aspiration) Thallium (AA, Direct Aspiration) Thallium (AA, Furnace Technique) Tin (AA, Direct Aspiration) Vanadium (AA, Direct Aspiration) Vanadium (AA, Furnace Technique) Zinc (AA, Direct Aspiration) Zinc (AA, Furnace Technique) CD-ROM CONTENTS - 3 Revision 3
4 VOLUME ONE SECTION B CHAPTER FOUR -- ORGANIC ANALYTES 4.1 Sampling Considerations 4.2 Sample Preparation Methods Extractions and Preparations Method 3500A: Method 3510B: Method 3520B: Method 3540B: Method 3541: Method 3550A: Method 3580A: Method 5030A: Method 5040A: Method 5041: Organic Extraction and Sample Preparation Separatory Funnel Liquid-Liquid Extraction Continuous Liquid-Liquid Extraction Soxhlet Extraction Automated Soxhlet Extraction Ultrasonic Extraction Waste Dilution Purge-and-Trap Analysis of Sorbent Cartridges from Volatile Organic Sampling Train (VOST): Gas Chromatography/Mass Spectrometry Technique Protocol for Analysis of Sorbent Cartridges from Volatile Organic Sampling Train (VOST): Wide-bore Capillary Column Technique Cleanup Method 3600B: Method 3610A: Method 3611A: Method 3620A: Method 3630B: Method 3640A: Method 3650A: Method 3660A: Method 3665: Cleanup Alumina Column Cleanup Alumina Column Cleanup and Separation of Petroleum Wastes Florisil Column Cleanup Silica Gel Cleanup Gel-Permeation Cleanup Acid-Base Partition Cleanup Sulfur Cleanup Sulfuric Acid/Permanganate Cleanup CD-ROM CONTENTS - 4 Revision 3
5 4.3 Determination of Organic Analytes Gas Chromatographic Methods Method 8000A: Method 8010B: Method 8011: Method 8015A: Method 8020A: Method 8021A: Method 8030A: Method 8031: Method 8032: Method 8040A: Method 8060: Method 8061: Method 8070: Method 8080A: Method 8081: Method 8090: Method 8100: Method 8110: Method 8120A: Method 8121: Method 8140: Method 8141A: Method 8150B: Method 8151: Gas Chromatography Halogenated Volatile Organics by Gas Chromatography 1,2-Dibromoethane and 1,2-Dibromo-3-chloropropane by Microextraction and Gas Chromatography Nonhalogenated Volatile Organics by Gas Chromatography Aromatic Volatile Organics by Gas Chromatography Halogenated Volatiles by Gas Chromatography Using Photoionization and Electrolytic Conductivity Detectors in Series: Capillary Column Technique Acrolein and Acrylonitrile by Gas Chromatography Acrylonitrile by Gas Chromatography Acrylamide by Gas Chromatography Phenols by Gas Chromatography Phthalate Esters Phthalate Esters by Capillary Gas Chromatography with Electron Capture Detection (GC/ECD) Nitrosamines by Gas Chromatography Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Organochlorine Pesticides and PCBs as Aroclors by Gas Chromatography: Capillary Column Technique Nitroaromatics and Cyclic Ketones Polynuclear Aromatic Hydrocarbons Haloethers by Gas Chromatography Chlorinated Hydrocarbons by Gas Chromatography Chlorinated Hydrocarbons by Gas Chromatography: Capillary Column Technique Organophosphorus Pesticides Organophosphorus Compounds by Gas Chromatography: Capillary Column Technique Chlorinated Herbicides by Gas Chromatography Chlorinated Herbicides by GC Using Methylation or Pentafluorobenzylation Derivatization: Capillary Column Technique Gas Chromatographic/Mass Spectroscopic Methods Method 8240B: Volatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) Method 8250A: Semivolatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) CD-ROM CONTENTS - 5 Revision 3
6 Method 8260A: Volatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS): Capillary Column Technique Method 8270B: Semivolatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS): Capillary Column Technique Method 8280: The Analysis of Polychlorinated Dibenzo-p-Dioxins and Polychlorinated Dibenzofurans Appendix A: Signal-to-Noise Determination Methods Appendix B: Recommended Safety and Handling Procedures for PCDDs/PCDFs Method 8290: Polychlorinated Dibenzodioxins (PCDDs) and Polychlorinated Dibenzofurans (PCDFs) by High-Resolution Gas Chromatography/High-Resolution Mass Spectrometry (HRGC/HRMS) Attachment A: Procedures for the Collection, Handling, Analysis, and Reporting of Wipe Tests Performed within the Laboratory High Performance Liquid Chromatographic Methods Method 8310: Polynuclear Aromatic Hydrocarbons Method 8315: Determination of Carbonyl Compounds by High Performance Liquid Chromatography (HPLC) Appendix A: Recrystallization of 2,4-Dinitrophenylhydrazine (DNPH) Method 8316: Acrylamide, Acrylonitrile and Acrolein by High Performance Liquid Chromatography (HPLC) Method 8318: N-Methylcarbamates by High Performance Liquid Chromatography (HPLC) Method 8321: Solvent Extractable Non-Volatile Compounds by High Performance Liquid Chromatography/Thermospray/Mass Spectrometry (HPLC/TSP/MS) or Ultraviolet (UV) Detection Method 8330: Nitroaromatics and Nitramines by High Performance Liquid Chromatography (HPLC) Method 8331: Tetrazene by Reverse Phase High Performance Liquid Chromatography (HPLC) Fourier Transform Infrared Methods Method 8410: Gas Chromatography/Fourier Transform Infrared (GC/FT-IR) Spectrometry for Semivolatile Organics: Capillary Column CD-ROM CONTENTS - 6 Revision 3
7 4.4 Miscellaneous Screening Methods Method 3810: Method 3820: Method 4010: Method 8275: Headspace Hexadecane Extraction and Screening of Purgeable Organics Screening for Pentachlorophenol by Immunoassay Thermal Chromatography/Mass Spectrometry (TC/MS) for Screening Semivolatile Organic Compounds CD-ROM CONTENTS - 7 Revision 3
8 CHAPTER FIVE -- MISCELLANEOUS TEST METHODS VOLUME ONE SECTION C Method 5050: Method 9010A: Method 9012: Method 9013: Method 9020B: Method 9021: Method 9022: Method 9030A: Method 9031: Method 9035: Method 9036: Method 9038: Method 9056: Method 9060: Method 9065: Method 9066: Method 9067: Method 9070: Method 9071A: Method 9075: Method 9076: Method 9077: Method A: Method B: Method C: Bomb Preparation Method for Solid Waste Total and Amenable Cyanide (Colorimetric, Manual) Total and Amenable Cyanide (Colorimetric, Automated UV) Cyanide Extraction Procedure for Solids and Oils Total Organic Halides (TOX) Purgeable Organic Halides (POX) Total Organic Halides (TOX) by Neutron Activation Analysis Acid-Soluble and Acid-Insoluble Sulfides Extractable Sulfides Sulfate (Colorimetric, Automated, Chloranilate) Sulfate (Colorimetric, Automated, Methylthymol Blue, AA II) Sulfate (Turbidimetric) Determination of Inorganic Anions by Ion Chromatography Total Organic Carbon Phenolics (Spectrophotometric, Manual 4-AAP with Distillation) Phenolics (Colorimetric, Automated 4-AAP with Distillation) Phenolics (Spectrophotometric, MBTH with Distillation) Total Recoverable Oil & Grease (Gravimetric, Separatory Funnel Extraction) Oil and Grease Extraction Method for Sludge and Sediment Samples Test Method for Total Chlorine in New and Used Petroleum Products by X-Ray Fluorescence Spectrometry (XRF) Test Method for Total Chlorine in New and Used Petroleum Products by Oxidative Combustion and Microcoulometry Test Methods for Total Chlorine in New and Used Petroleum Products (Field Test Kit Methods) Fixed End Point Test Kit Method Reverse Titration Quantitative End Point Test Kit Method Direct Titration Quantitative End Point Test Kit Method CD-ROM CONTENTS - 8 Revision 3
9 Method 9131: Method 9132: Method 9200: Method 9250: Method 9251: Method 9252A: Method 9253: Method 9320: Total Coliform: Multiple Tube Fermentation Technique Total Coliform: Membrane Filter Technique Nitrate Chloride (Colorimetric, Automated Ferricyanide AAI) Chloride (Colorimetric, Automated Ferricyanide AAII) Chloride (Titrimetric, Mercuric Nitrate) Chloride (Titrimetric, Silver Nitrate) Radium-228 CHAPTER SIX -- PROPERTIES Method 1312: Method 1320: Method 1330A: Method 9040B: Method 9041A: Method 9045C: Method 9050: Method 9080: Method 9081: Method 9090A: Method 9095: Method 9096: Appendix A: Method 9100: Method 9310: Method 9315: Synthetic Precipitation Leaching Procedure Multiple Extraction Procedure Extraction Procedure for Oily Wastes ph Electrometric Measurement ph Paper Method Soil and Waste ph Specific Conductance Cation-Exchange Capacity of Soils (Ammonium Acetate) Cation-Exchange Capacity of Soils (Sodium Acetate) Compatibility Test for Wastes and Membrane Liners Paint Filter Liquids Test Liquid Release Test (LRT) Procedure Liquid Release Test Pre-Test Saturated Hydraulic Conductivity, Saturated Leachate Conductivity, and Intrinsic Permeability Gross Alpha and Gross Beta Alpha-Emitting Radium Isotopes PART II CHARACTERISTICS CHAPTER SEVEN -- INTRODUCTION AND REGULATORY DEFINITIONS 7.1 Ignitability 7.2 Corrosivity 7.3 Reactivity Test Method to Determine Hydrogen Cyanide Released from Wastes Test Method to Determine Hydrogen Sulfide Released from Wastes 7.4 Toxicity Characteristic Leaching Procedure CD-ROM CONTENTS - 9 Revision 3
10 CHAPTER EIGHT -- METHODS FOR DETERMINING CHARACTERISTICS 8.1 Ignitability Method 1010: Method 1020A: Pensky-Martens Closed-Cup Method for Determining Ignitability Setaflash Closed-Cup Method for Determining Ignitability 8.2 Corrosivity Method 1110: Corrosivity Toward Steel 8.3 Reactivity 8.4 Toxicity Method 1310A: Method 1311: Extraction Procedure (EP) Toxicity Test Method and Structural Integrity Test Toxicity Characteristic Leaching Procedure CD-ROM CONTENTS - 10 Revision 3
11 VOLUME TWO PART III SAMPLING CHAPTER NINE -- SAMPLING PLAN 9.1 Design and Development 9.2 Implementation CHAPTER TEN -- SAMPLING METHODS Method 0010: Appendix A: Appendix B: Method 0020: Method 0030: Modified Method 5 Sampling Train Preparation of XAD-2 Sorbent Resin Total Chromatographable Organic Material Analysis Source Assessment Sampling System (SASS) Volatile Organic Sampling Train PART IV MONITORING CHAPTER ELEVEN -- GROUND WATER MONITORING 11.1 Background and Objectives 11.2 Relationship to the Regulations and to Other Documents 11.3 Revisions and Additions 11.4 Acceptable Designs and Practices 11.5 Unacceptable Designs and Practices CHAPTER TWELVE -- LAND TREATMENT MONITORING 12.1 Background 12.2 Treatment Zone 12.3 Regulatory Definition 12.4 Monitoring and Sampling Strategy 12.5 Analysis 12.6 References and Bibliography CD-ROM CONTENTS - 11 Revision 3
12 CHAPTER THIRTEEN - INCINERATION 13.1 Introduction 13.2 Regulatory Definition 13.3 Waste Characterization Strategy 13.4 Stack-Gas Effluent Characterization Strategy 13.5 Additional Effluent Characterization Strategy 13.6 Selection of Specific Sampling and Analysis Methods 13.7 References CD-ROM CONTENTS - 12 Revision 3
13 APPENDIX -- COMPANY REFERENCES NOTE: A suffix of "A" in the method number indicates revision one (the method has been revised once). A suffix of "B" in the method number indicates revision two (the method has been revised twice). A suffix of "C" in the method number indicates revision three (the method has been revised three times). In order to properly document the method used for analysis, the entire method number including the suffix letter designation (e.g., A, B, or C) must be identified by the analyst. A method reference found within the RCRA regulations and the text of SW-846 methods and chapters refers to the latest promulgated revision of the method, even though the method number does not include the appropriate letter suffix. CD-ROM CONTENTS - 13 Revision 3
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