Test Report. No. SHAEC Date: 24 Jul Page 1 of 13.

Transcription

1 Test Report. No. SHAEC Date: 24 Jul Page 1 of 13. HERAEUS( ZHAOYUAN) PRECIOUS METAL MATERIALS CO.,LTD.. NO.9 ANKANG SOUTH ROAD,ZHAOYUAN CITY,SHANDONG PROVINCE.. The following sample(s) was/were submitted and identified on behalf of the clients as : Gold Wire. SGS Job No. : SP SH. Model No. :. HD. Date of Sample Received :. 09 Jul Testing Period :. 09 Jul Jul Test Requested :. Test Method :. Selected test(s) as requested by client.. Please refer to next page(s).. Test Results :. Conclusion :. Please refer to next page(s).. Based on the performed tests on submitted sample(s), the results of Cadmium, Lead, Mercury, Hexavalent chromium, Polybrominated biphenyls (PBBs), Polybrominated diphenyl ethers (PBDEs) and Phthalates such as Bis(2-ethylhexyl) phthalate (DEHP), Butyl benzyl phthalate (BBP), Dibutyl phthalate (DBP) and Diisobutyl phthalate (DIBP) comply with the limits as set by RoHS Directive (EU) 2015/863 amending Annex II to Directive 2011/65/EU.. Signed for and on behalf of SGS-CSTC Standards Technical Services (Shanghai) Co., Ltd.. Helen Liu. Approved Signatory.

2 Test Report. No. SHAEC Date: 24 Jul Page 2 of 13. Test Results :. Test Part Description :. Specimen No.. SGS Sample ID. Description. SN1. SHA Golden metal wire. Remarks :. (1) 1 mg/kg = 1 ppm = %. (2) MDL = Method Detection Limit. (3) ND = Not Detected ( < MDL ). (4) "-" = Not Regulated. RoHS Directive (EU) 2015/863 amending Annex II to Directive 2011/65/EU. Test Method :. With reference to IEC :2013+AMD1:2017, IEC :2013, IEC :2015, IEC :2015 and IEC :2017, analyzed by ICP-OES, UV-Vis and GC-MS.. Test Item(s). Limit. Unit. MDL Cadmium (Cd). 100 mg/kg. 2 ND Lead (Pb) mg/kg. 2 ND Mercury (Hg) mg/kg. 2 ND Hexavalent Chromium (Cr(VI)). -. µg/cm² ND Sum of PBBs mg/kg. - ND Monobromobiphenyl. - mg/kg. 5 ND Dibromobiphenyl. - mg/kg. 5 ND Tribromobiphenyl. - mg/kg. 5 ND Tetrabromobiphenyl. - mg/kg. 5 ND Pentabromobiphenyl. - mg/kg. 5 ND Hexabromobiphenyl. - mg/kg. 5 ND Heptabromobiphenyl. - mg/kg. 5 ND Octabromobiphenyl. - mg/kg. 5 ND Nonabromobiphenyl. - mg/kg. 5 ND Decabromobiphenyl. - mg/kg. 5 ND Sum of PBDEs mg/kg. - ND Monobromodiphenyl ether. - mg/kg. 5 ND Dibromodiphenyl ether. - mg/kg. 5 ND Tribromodiphenyl ether. - mg/kg. 5 ND Tetrabromodiphenyl ether. - mg/kg. 5 ND

3 Test Report. No. SHAEC Date: 24 Jul Page 3 of 13. Test Item(s). Limit. Unit. MDL Pentabromodiphenyl ether. - mg/kg. 5 ND Hexabromodiphenyl ether. - mg/kg. 5 ND Heptabromodiphenyl ether. - mg/kg. 5 ND Octabromodiphenyl ether. - mg/kg. 5 ND Nonabromodiphenyl ether. - mg/kg. 5 ND Decabromodiphenyl ether. - mg/kg. 5 ND Di-butyl Phthalate (DBP) mg/kg. 50 ND Benzyl Butyl Phthalate (BBP) mg/kg. 50 ND Di-2-Ethyl Hexyl Phthalate (DEHP) mg/kg. 50 ND Diisobutyl Phthalates (DIBP) mg/kg. 50 ND Notes :. (1)The maximum permissible limit is quoted from RoHS Directive (EU) 2015/863. IEC series is equivalent to EN series _ID: ,25 (2) = a. The sample is positive for CrVI if the CrVI concentration is greater than 0.13 μg/cm². The sample coating is considered to contain CrVI b. The sample is negative for CrVI if CrVI is ND (concentration less than 0.10 μg/cm²). The coating is considered a non-crvi based coating c. The result between 0.10 μg/cm² and 0.13 μg/cm² is considered to be inconclusive - unavoidable coating variations may influence the determination Information on storage conditions and production date of the tested sample is unavailable and thus Cr(VI) results represent status of the sample at the time of testing.. Element(s). Test Method :. With reference to US EPA Method 3050B:1996, analysis was performed by ICP-OES.. Test Item(s). Unit. MDL Beryllium (Be). mg/kg. 5 ND Antimony (Sb). mg/kg. 10 ND Beryllium oxide (BeO). mg/kg. 15 ND Antimony trioxide (Sb₂O₃). mg/kg. 12 ND Arsenic (As). mg/kg. 10 ND Phosphorus (P). mg/kg. 20 ND Notes :. (1) Calculated concentration of BeO is based on the identified Be Calculated concentration of Sb₂O₃ is based on the identified Sb.

4 Test Report. No. SHAEC Date: 24 Jul Page 4 of 13. Halogen. Test Method :. With reference to EN 14582: 2016, analysis was performed by IC.. Test Item(s). Unit. MDL Fluorine (F). mg/kg. 50 ND Chlorine (Cl). mg/kg. 50 ND Bromine (Br). mg/kg. 50 ND Iodine (I). mg/kg. 50 ND Phthalates Content. Test Method :. With reference to EN 14372:2004, analysis was performed by GC-MS.. Test Item(s). CAS NO. Unit. MDL Diisononyl Phthalate (DINP) % ND / Di-n-octyl Phthalate (DNOP) % ND Diisodecyl Phthalate (DIDP) % ND / Di-n-pentyl Phthalates (DnPP) % ND Tetrabromobisphenol A (TBBP-A). Test Method :. With reference to US EPA 3540C: 1996, analysis was performed by GC-MS.. Test Item(s). Unit. MDL Tetrabromobisphenol A (TBBP-A). mg/kg. 10 ND Hexabromocyclododecane (HBCDD). Test Method :. With reference to IEC 62321:2008, analysis was performed by GC-MS..

5 Test Report. No. SHAEC Date: 24 Jul Page 5 of 13. Test Item(s). Unit. MDL Hexabromocyclododecane (HBCDD). mg/kg. 10 ND Notes :. (1) CAS No.: & PFOS (Perfluorooctane Sulfonates) and PFOA (Perfluorooctanoic Acid). Test Method :. With reference to US EPA 3550C: 2007, analysis was performed by HPLC-MS.. Test Item(s). Limit. Unit. MDL Perfluorooctanesulfonate (PFOS)^ mg/kg. 10. ND. Perfluorooctanoic Acid (PFOA). - mg/kg. 10. ND. Notes :. (1) Max. limit specified by commission regulation (EU) No. 757/2010 amending regulation (EC) No 850/2004 (2)^ PFOS refer to Perfluorooctanesulfonic acid and its derivatives including Perfluoroctanesulfonic acid, Perfluoroctane sulfonamide, N-Methylperfluoroctane sulfonamide, N-Ethylperfluoroctane sulfonamide, N-Methylperfluoroctane sulfonamidoethanol and N-Ethylperfluoroctane sulfonamidoethanol..

6 Test Report. No. SHAEC Date: 24 Jul Page 6 of 13. Pb/Cd/Hg/Cr 6+ /PBBs/PBDEs Testing Flow Chart 1) Name of the person who made testing: Meria Jin/Gary Xu/ Xiaolong Yang/Sielina Song 2) Name of the person in charge of testing: Jan Shi/Myra Ma/Luna Xu/Shara Wang 3) These samples were dissolved totally by pre-conditioning method according to below flow chart. (Cr 6+ and PBBs/PBDEs test method excluded) Sample Preparation Sample Measurement Pb/Cd/Hg/Cr PBBs/PBDEs Cr 6+ Acid digestion with microwave / hotplate Sample solvent extraction Nonmetallic material Metallic material Solution Residue 1) Alkali Fusion / Dry Ashing 2) Acid to dissolve Concentration/ Dilution of extraction solution GC-MS ABS/PC/PVC Dissolving by ultrasonication Digesting at 60 C by ultrasonication Others ph adjustment Digesting at 150~160 C Separating to get aqueous phase Boiling water extraction Adding 1,5- diphenylcarba zide for color development UV-Vis ICP-OES/AAS Adding 1,5- diphenylcarbazide for color development UV-Vis

7 Test Report. No. SHAEC Date: 24 Jul Page 7 of 13. Phthalates Testing Flow Chart 1) Name of the person who made testing: Sherlock Gao 2) Name of the person in charge of testing: Jessy Huang Sample cutting/preparation Sample measurement Solvent extraction Concentration/Dilution GC-MS

8 Test Report. No. SHAEC Date: 24 Jul Page 8 of 13. HBCDD Testing Flow Chart 1) Name of the person who made testing: Gary Xu 2) Name of the person in charge of testing: Myra ma Sample cutting/preparation Sample measurement Solvent extraction Concentration/Dilution GC-MS

9 Test Report. No. SHAEC Date: 24 Jul Page 9 of 13. Halogen Testing (oxygen bomb) Flow Chart 1) Name of the person who made testing: Kevin Xu 2) Name of the person in charge of testing: Anne Huang Sample cutting/preparation Sample measurement Combustion in oxygen bomb Dissolved in an absorption solution Analyzed by ion chromatography. Double confirm by other instruments, if necessary

10 Test Report. No. SHAEC Date: 24 Jul Page 10 of 13. PFOS/PFOA Testing Flow Chart 1) Name of the person who made testing: Richer Yu 2) Name of the person in charge of testing: Jessy Huang Sample cutting/preparation Sample measurement Solvent extraction Concentration/Dilution LC-MS

11 Test Report. No. SHAEC Date: 24 Jul Page 11 of 13. Elements Testing Flow Chart 1) Name of the person who made testing: Meria Jin/Sielina Song 2) Name of the person in charge of testing: Luna Xu/Jan Shi Sample cutting/preparation Sample measurement Acid digestion Solution ICP-OES/AAS

12 Test Report. No. SHAEC Date: 24 Jul Page 12 of 13. TBBP-A Testing Flow Chart 1) Name of the person who made testing: Gary Xu 2) Name of the person in charge of testing: Myra ma Sample cutting/preparation Sample measurement Solvent extraction Derivatization Liquid-liquid extraction Concentration/Dilution GC-MS

13 Test Report. No. SHAEC Date: 24 Jul Page 13 of 13. Sample photo:. SHAEC SHA SGS authenticate the photo on original report only. *** End of Report ***.