Test Report. No. SHAEC Date: 19 Jul Page 1 of 14.
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1 Test Report. No. SHAEC Date: 19 Jul Page 1 of 14. NAN YA PRINTED CIRCUIT BOARD (KUNSHAN) CO.,LTD. 201 CHANG JIANG ROAD KUNSHAN, ECONOMIC&TECHNICAL DEVELOPMENT ZONE, JIANG SU, CHINA.. The following sample(s) was/were submitted and identified on behalf of the clients as : Copper plating. SGS Job No. : SP SH. Date of Sample Received :. 03 Jul Testing Period :. 03 Jul Jul Test Requested :. Test Method :. Selected test(s) as requested by client.. Please refer to next page(s).. Test Results :. Conclusion :. Please refer to next page(s).. Based on the performed tests on submitted sample(s), the results of Cadmium, Lead, Mercury, Hexavalent chromium, Polybrominated biphenyls (PBBs), Polybrominated diphenyl ethers (PBDEs) and Phthalates such as Bis(2-ethylhexyl) phthalate (DEHP), Butyl benzyl phthalate (BBP), Dibutyl phthalate (DBP) and Diisobutyl phthalate (DIBP) comply with the limits as set by RoHS Directive (EU) 2015/863 amending Annex II to Directive 2011/65/EU.. Signed for and on behalf of SGS-CSTC Standards Technical Services (Shanghai) Co., Ltd.. Marry Ma. Approved Signatory.
2 Test Report. No. SHAEC Date: 19 Jul Page 2 of 14. Test Results :. Test Part Description :. Specimen No.. SGS Sample ID. Description. SN1. SHA Coppery metal plating. Remarks :. (1) 1 mg/kg = %. (2) MDL = Method Detection Limit. (3) ND = Not Detected ( < MDL ). (4) "-" = Not Regulated. RoHS Directive (EU) 2015/863 amending Annex II to Directive 2011/65/EU. Test Method :. (1) With reference to IEC :2013, determination of Cadmium by ICP-OES. (2) With reference to IEC :2013, determination of Lead by ICP-OES. (3) With reference to IEC :2013, determination of Mercury by ICP-OES. (4) With reference to IEC :2015, determination of Hexavalent Chromium by Colorimetric Method using UV-Vis. (5)With reference to IEC :2015, determination of PBBs and PBDEs by GC-MS. (6) With reference to IEC :2017, determination of phthalates by GC-MS.. Test Item(s). Limit. Unit. MDL Cadmium (Cd). 100 mg/kg. 2 ND Lead (Pb) mg/kg. 2 ND Mercury (Hg) mg/kg. 2 ND Hexavalent Chromium (Cr(VI)). -. µg/cm² ND Sum of PBBs mg/kg. - ND Monobromobiphenyl. - mg/kg. 5 ND Dibromobiphenyl. - mg/kg. 5 ND Tribromobiphenyl. - mg/kg. 5 ND Tetrabromobiphenyl. - mg/kg. 5 ND Pentabromobiphenyl. - mg/kg. 5 ND Hexabromobiphenyl. - mg/kg. 5 ND Heptabromobiphenyl. - mg/kg. 5 ND Octabromobiphenyl. - mg/kg. 5 ND Nonabromobiphenyl. - mg/kg. 5 ND Decabromobiphenyl. - mg/kg. 5 ND Sum of PBDEs mg/kg. - ND
3 Test Report. No. SHAEC Date: 19 Jul Page 3 of 14. Test Item(s). Limit. Unit. MDL Monobromodiphenyl ether. - mg/kg. 5 ND Dibromodiphenyl ether. - mg/kg. 5 ND Tribromodiphenyl ether. - mg/kg. 5 ND Tetrabromodiphenyl ether. - mg/kg. 5 ND Pentabromodiphenyl ether. - mg/kg. 5 ND Hexabromodiphenyl ether. - mg/kg. 5 ND Heptabromodiphenyl ether. - mg/kg. 5 ND Octabromodiphenyl ether. - mg/kg. 5 ND Nonabromodiphenyl ether. - mg/kg. 5 ND Decabromodiphenyl ether. - mg/kg. 5 ND Di-butyl Phthalate (DBP) mg/kg. 50 ND Benzyl Butyl Phthalate (BBP) mg/kg. 50 ND Di-2-Ethyl Hexyl Phthalate (DEHP) mg/kg. 50 ND Diisobutyl Phthalates (DIBP) mg/kg. 50 ND Notes :. (1) The maximum permissible limit is quoted from RoHS Directive (EU) 2015/863. IEC series is equivalent to EN series ,25 (2) = a. The sample is positive for CrVI if the CrVI concentration is greater than 0.13 μg/cm². The sample coating is considered to contain CrVI b. The sample is negative for CrVI if CrVI is ND (concentration less than 0.10 μg/cm²). The coating is considered a non-crvi based coating c. The result between 0.10 μg/cm² and 0.13 μg/cm² is considered to be inconclusive - unavoidable coating variations may influence the determination Information on storage conditions and production date of the tested sample is unavailable and thus Cr(VI) results represent status of the sample at the time of testing.. Element(s). Test Method :. With reference to US EPA 3052:1996, analysis was performed by ICP-OES.. Test Item(s). Unit. MDL Arsenic (As). mg/kg. 10 ND Beryllium (Be). mg/kg. 5 ND Antimony (Sb). mg/kg. 10 ND Halogen.
4 Test Report. No. SHAEC Date: 19 Jul Page 4 of 14. Test Method :. With reference to EN 14582: 2007, analysis was performed by Ion Chromatograph (IC).. Test Item(s). Unit. MDL Fluorine (F). mg/kg. 50 ND Chlorine (Cl). mg/kg. 50 ND Bromine (Br). mg/kg. 50 ND Iodine (I). mg/kg. 50 ND Monomethyldibromodiphenylmethane, Monomethyldichlorodiphenylmethane, Monomethyltetrachlorodiphenylmethane. Test Method :. SGS In house method, analysis was performed by GC-MS.. Test Item(s). Unit. MDL Monomethyldibromodiphenylmethane. mg/kg. 10 ND Monomethyldichlorodiphenylmethane. mg/kg. 10 ND Monomethyltetrachloro-diphenylmethane. mg/kg. 10 ND Tetrabromobisphenol A (TBBP-A). Test Method :. With reference to US EPA 3540C: 1996, analysis was performed by GC-MS.. Test Item(s). Unit. MDL Tetrabromobisphenol A (TBBP-A). mg/kg. 10 ND Hexabromocyclododecane (HBCDD). Test Method :. With reference to IEC 62321:2008, analysis was performed by GC-MS.. Test Item(s). Unit. MDL Hexabromocyclododecane (HBCDD). mg/kg. 10 ND PFOS (Perfluorooctane Sulfonates) and PFOA (Perfluorooctanoic Acid). Test Method :. With reference to US EPA 3550C: 2007, analysis was performed by HPLC-MS..
5 Test Report. No. SHAEC Date: 19 Jul Page 5 of 14. Test Item(s). Limit. Unit. MDL Perfluorooctanesulfonate (PFOS)^ mg/kg. 10. ND. Perfluorooctanoic Acid (PFOA). - mg/kg. 10. ND. Notes :. (1) Max. limit specified by commission regulation (EU) No. 757/2010 amending regulation (EC) No 850/2004 (2)^ PFOS refer to Perfluorooctanesulfonic acid and its derivatives including Perfluoroctanesulfonic acid, Perfluoroctane sulfonamide, N-Methylperfluoroctane sulfonamide, N-Ethylperfluoroctane sulfonamide, N-Methylperfluoroctane sulfonamidoethanol and N-Ethylperfluoroctane sulfonamidoethanol.. Phthalates Content. Test Method :. With reference to EN 14372:2004, analysis was performed by GC-MS.. Test Item(s). CAS NO. Unit. MDL Diisononyl Phthalate (DINP) % ND. / Di-n-octyl Phthalate (DNOP) % ND. Diisodecyl Phthalate (DIDP) % ND. / Dimethyl Phthalate (DMP) % ND. Diethyl Phthalate (DEP) % ND. Di-n-pentyl Phthalates (DnPP) % ND. Dicyclohexyl Phthalate (DCHP) % ND. Diphenyl Phthalate (DPhP) % ND. Dibenzyl Phthalate (DBzP) % ND. Diisooctyl Phthalate (DiOP) % ND. Dipropyl Phthalate (DPrP) % ND. Dinonyl Phthalate (DNP) % ND. Bis(2-methoxyethyl) Phthalate (DMEP) % ND. Di-n-hexyl Phthalate (DnHP) % ND. Diisopentylphthalate (DIPP) % ND. 1,2-Benzenedicarboxylic acid, di-c7-11-branched and linear alkyl esters (DHNUP) % ND. Notes :. (1) DBP,BBP,DEHP Reference information: Entry 51 of Regulation (EC) No 552/2009 amending Annex XVII of REACH Regulation (EC) No 1907/2006 (previously restricted under Directive 2005/84/EC): i) Shall not be used as substances or in mixtures, in concentrations greater than 0.1 % by weight of the plasticised material, in toys and childcare articles.
6 Test Report. No. SHAEC Date: 19 Jul Page 6 of 14. ii) Toys and childcare articles containing these phthalates in a concentration greater than 0.1 % by weight of the plasticised material shall not be placed on the market. Please refer to Regulation (EC) No 552/2009 to get more detail information DINP, DNOP, DIDP Reference information: Entry 52 of Regulation (EC) No 552/2009 amending Annex XVII of REACH Regulation (EC) No 1907/2006 (previously restricted under Directive 2005/84/EC). i) Shall not be used as substances or in mixtures, in concentrations greater than 0.1 % by weight of the plasticised material, in toys and childcare articles which can be placed in the mouth by children. ii) Such toys and childcare articles containing these phthalates in a concentration greater than 0.1 % by weight of the plasticised material shall not be placed on the market. Please refer to Regulation (EC) No 552/2009 to get more detail information.
7 Test Report. No. SHAEC Date: 19 Jul Page 7 of 14. ATTACHMENTS Pb/Cd/Hg/Cr 6+ /PBBs/PBDEs Testing Flow Chart 1) Name of the person who made testing: Meria Jin/Gary Xu/Sean Li/Sielina Song 2) Name of the person in charge of testing: Jan Shi/Jessy Huang/Luna Xu/Shara Wang 3) These samples were dissolved totally by pre-conditioning method according to below flow chart. (Cr 6+ and PBBs/PBDEs test method excluded) Sample Preparation Sample Measurement Pb/Cd/Hg/Cr PBBs/PBDEs Cr 6+ Acid digestion with microwave / hotplate Solution Residue 1) Alkali Fusion / Dry Ashing 2) Acid to Sample solvent extraction Concentration/ Dilution of extraction solution GC-MS ABS/PC/PV Dissolving by ultrasonicatio Digesting at 60 C by ultrasonicatio Nonmetallic material Others ph adjustment Digesting at 150~160 C Separating to get aqueous phase Metallic material Boiling water extraction Adding 1,5- diphenylcarb azide for color UV-Vis. ICP-OES/AAS Adding 1,5- diphenylcarbazide for color UV-Vis
8 Test Report. No. SHAEC Date: 19 Jul Page 8 of 14. ATTACHMENTS Phthalates Testing Flow Chart 1) Name of the person who made testing: Sherlock Gao 2) Name of the person in charge of testing: Jessy Huang Sample cutting/preparation Sample measurement Solvent extraction Concentration/Dilution GC-MS
9 Test Report. No. SHAEC Date: 19 Jul Page 9 of 14. ATTACHMENTS HBCDD Testing Flow Chart 1) Name of the person who made testing: Gary Xu 2) Name of the person in charge of testing: Jessy Huang Sample cutting/preparation Sample measurement Solvent extraction Concentration/Dilution GC-MS
10 Test Report. No. SHAEC Date: 19 Jul Page 10 of 14. ATTACHMENTS Halogen Testing (oxygen bomb) Flow Chart 1) Name of the person who made testing: Kevin Xu 2) Name of the person in charge of testing: Sisily Yin Sample cutting/preparation Sample measurement Combustion in oxygen bomb Dissolved in an absorption solution Analyzed by ion chromatography. Double confirm by other instruments, if necessary
11 Test Report. No. SHAEC Date: 19 Jul Page 11 of 14. ATTACHMENTS PFOS/PFOA Testing Flow Chart 1) Name of the person who made testing: Jane Yang 2) Name of the person in charge of testing: Myra Ma Sample cutting/preparation Sample measurement Solvent extraction Concentration/Dilution LC-MS
12 Test Report. No. SHAEC Date: 19 Jul Page 12 of 14. ATTACHMENTS Elements Testing Flow Chart 1) Name of the person who made testing: Meria Jin/Sielina Song 2) Name of the person in charge of testing: Luna Xu/Jan Shi Sample cutting/preparation Sample measurement Acid digestion Solution ICP-OES/AAS
13 Test Report. No. SHAEC Date: 19 Jul Page 13 of 14. ATTACHMENTS TBBP-A Testing Flow Chart 1) Name of the person who made testing: Gary Xu 2) Name of the person in charge of testing: Jessy Huang Sample cutting/preparation Sample measurement Solvent extraction Derivatization Liquid-liquid extraction Concentration/Dilution GC-MS
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