PHASE II LIMITED SUBSURFACE INVESTIGATION REPORT OF FINDINGS

Transcription

1 20 YEARS PHASE II LIMITED SUBSURFACE INVESTIGATION REPORT OF FINDINGS SITECH Germantown 4301 NYS Route 9G Germantown, Columbia County, New York PES Project No Report Completed: August 2015 Prepared For: Mr. Simon List SITECH Consulting, P.C Breeland Way Raleigh, North Carolina Schenectady, New York Primax Properties, LLC 1100 E Morehead Street Charlotte, NC Prepared By: PRECISION ENVIRONMENTAL SERVICES, INC. 831 NYS Route 67, Lot 38A Ballston Spa, New York 12020

2 TABLE OF CONTENTS 1.0 Introduction Limited Subsurface Investigation Geologic/Hydrologic Findings Laboratory Analytical Results Summary of Findings Recommendations Disclaimer..5 Enclosures: ATTACHMENT A - FIGURES Figure 1 Site Map ATTACHMENT B - TABLES Table 1 Summary of Soil Analytical Results ATTACHMENT C Test Pit Logs ATTACHMENT D Laboratory Analytical Report

3 Mr. Simon List, SITECH Consulting, P.C. Page NYS Route 9G, Germantown, Columbia County, NY Limited Subsurface Investigation Report, PES Project No INTRODUCTION Precision Environmental Services, Inc. (PES) has prepared this report for SITECH Consulting, P.C., Primax Properties, LLC., and Dollar General, Inc. to document the findings of a limited subsurface investigation at the property located at 4301 NYS Route 9G, Germantown, NY, hereafter referred to as the Site (see Attachment A, Figure 1 for site location detail). Work tasks completed and documented in this report were initiated as part of a real estate transaction between Primax Properties and the current property owner and include the installation of five (5) soil test pits and the collection and submission of soil samples from installed test pits for laboratory analysis. 1.2 Site Description and Background Please Note: The following discussion is limited to PES s findings as they relate solely to the limits of the authorized scope of work. Specifically, information presented will address only those areas of the site where PES performed investigative work (i.e. installation of test pits, etc.) see Figures 1 for site plan details. The Site is located at 4301 NYS Route 9G, Germantown, Columbia County, New York. The property is situated in a mixed rural, commercial, and residential area. In general, the land surfaces at the Site are relatively flat with a slight dip to the west. The results of a completed Phase 1 Environmental Site Assessment and geotechnical evaluation (completed by others) indicated fill material had historically been applied to the site. In accordance with the request of the local municipality, a limited subsurface investigation was prescribed to collect environmental quality data pertaining to the nature of the fill material. The results of this investigation are summarized below. 2.0 LIMITED SUBSURFACE INVESTIGATION 2.1 General On July 30, 2015 PES initiated a subsurface investigation consisting of the installation of five (5) soil test pits (TP-1 through 5) with the primary objective of assessing and characterizing areas alleged to contain fill material. It is unknown when the fill material was placed onsite based on our review of readily available documents. Historical aerials of the Site from 1956, 1978, 1985, 1994, 2006, 2008, 2009, and 2011 do not provide indications of fill placement or disturbance of the Site, other than those associated with current uses of the property by a landscaping company. PES generally followed NYSDEC DER-10 Technical Guidance for Site Investigation and Remediation, May 2010, Chapter 3 Site Characterization and Remedial Investigation, Section 3.11 Historic Fill Material (DER-10 Technical Guidance) while completing the site work described below. Test pits were installed utilizing a mini excavator. In general, test pits were advanced to a maximum depth of nine-feet below the existing site grade or until practical refusal. The excavation equipment retrieved soils at one to two foot stratigraphic intervals. The retrieved soils were visually classified and field screened utilizing a calibrated photo-ionization detector (PID) to determine the presence of volatile organic compounds (VOCs). Soil samples were collected and monitored on a continuous basis for all test pits. See Attachment C Test Pit Logs for details.

4 Mr. Simon List, SITECH Consulting, P.C. Page NYS Route 9G, Germantown, Columbia County, NY Limited Subsurface Investigation Report, PES Project No Field Screening Results Throughout the subsurface investigation a PES geologist was present with a properly calibrated PID to monitor subsurface soils for the presence of VOCs. Screening involved sealing representative portions of the acquired sample in clean plastic bags, allowing for equilibration, and scanning the headspace using a PID. The PID was calibrated with an isobutylene standard gas to provide a benzene response factor before it was brought to the site. Grab samples were collected continuously throughout the vertical extent of the installed test pits. The test pit locations were selected based on the results of the August 2014 geotechnical evaluation and existing onsite structures. It should be noted that the field instrument used has a sensitivity of one-tenth (0.1) parts per million (ppm). During the subsurface investigation, background readings were recorded at a range of non-detect to 0.5 ppm; the maximum soil PID responses were at 0.5 ppm. Dark soils (brown to black) were encountered in fill materials in several test pits; however, no staining and/or olfactory evidence of contamination was observed/documented in examined soils. Please see Attachment C Test Pit Logs for encountered soil description. Results of the field soil screening procedures are as follows: Subsurface Investigation May 28, 2015 Soil Boring ID Maximum Headspace Depth Response (PPM) (Feet) TP TP TP TP TP Total Depth (Feet) Soil samples were collected for laboratory analysis from the vertical extent of the encountered fill material. Soil samples collected from TP-2 through TP-5 were submitted for laboratory analysis via Total Petroleum Hydrocarbons Diesel Range Organics (TPH-DRO), Total Petroleum Hydrocarbons Gasoline Range Hydrocarbons (TPH-GRO), 13 Priority Pollutant Metals, and EPA Priority Pollutant Polyaromatic Hydrocarbons (PAHs) in accordance with NYSDEC DER-10 Technical Guidance. The soil samples were placed in clean glass jars supplied by the analytical facility. The sample containers were labeled, sealed, and placed immediately in iced storage for transport to Phoenix Environmental Laboratories, Inc. (Phoenix) of Manchester, CT. Soil collected from TP-3 was also submitted for laboratory analysis via Polychlorinated Biphenyls (PCBs) following receipt and review of the preliminary laboratory analytical results. A copy of the chain of custody is included with the Laboratory Analytical Report as Attachment D. 3.0 GEOLOGIC/HYDROLOGIC FINDINGS 3.1 Regional Geology The subject property is located within the Lower Hudson Physiographic Province. The overburden soils in the surrounding area are described as being till deposits. Till deposits are commonly characterized

5 Mr. Simon List, SITECH Consulting, P.C. Page NYS Route 9G, Germantown, Columbia County, NY Limited Subsurface Investigation Report, PES Project No by variable texture (i.e. clay, silt-clay, boulder-clay), usually poorly sorted diamict, relatively impermeable, and a variable clast content (Cadwell et al, 1989). The bedrock geology at the Site is cited being of the Austin Glen Formation, which is comprised of greywacke and shale of Middle Ordovician age (Fisher et al, 1970). 3.2 Site Geology Subsurface soils were investigated at the Site through the installation of test pits during the July 2015 limited subsurface investigation. The depth of overburden exploration reached approximately nine feet below grade. Native soils encountered at the Site were generally composed of tan/brown fine sand and silt with varying clay content, which are in accordance with regionally described surficial deposits. Fill material was identified in several of the installed test pits, particularly TP-2 and TP-3. The fill material encountered at the Site was generally composed of black to tan, poorly sorted, coarse to fine sand with fine to medium gravel mixed and variable clay and silt content vertically and laterally. A slight to moderate amount of debris, including asphalt, coal, and brick, was documented in the fill material. Bedrock (greywacke) was encountered in TP-1 (5.5 feet below grade) and in TP-4 (6.5 below grade) and appeared to be in accordance with regionally described bedrock geology. 3.3 Surface Water The nearest surface water body is the Hudson River, located approximately 1,640 feet to the west of the Site. 3.4 Site Hydrogeology No groundwater was encountered during this limited subsurface investigation. 4.0 LABORATORY ANALYTICAL RESULTS 4.1 Soil Analytical Results As Table 1 Summary of Soil Analytical Results indicates, constituents of concern for soil sample TP- 3 were detected above the laboratory minimum detection limits. The reported concentrations exceed the Unrestricted Use soil clean up objectives ascribed by the NYSDEC Regulation 6 NYCRR Subpart Remedial Program Soil Cleanup Objectives (Soil SCOs); however, the reported soil analytical results do not exceed Restricted Use Commercial Soil SCOs. All submitted soil analytical results for the 13 Priority Pollutant Metals were reported below Soil SCOs, and the results for TPH-GRO and TPH-DRO were reported as non-detect. PCBs were reported as non-detect for TP-3, as well. The analytical report for the submitted soil samples is included with Attachment D Laboratory Analytical Report. 5.0 SUMMARY OF FINDINGS On July 30, 2015, PES performed a limited subsurface investigation that included the installation of five (5) test pits to characterize the nature of fill material previously documented at the subject property.

6 Mr. Simon List, SITECH Consulting, P.C. Page NYS Route 9G, Germantown, Columbia County, NY Limited Subsurface Investigation Report, PES Project No Test pit locations were determined by the borings results of the August 2014 geotechnical evaluation and existing onsite structures. Soil Screening and sampling took place during test pit installation and soil sampling procedures. Soil samples from select test pits were submitted for laboratory analysis. As described in Section 2.0 Subsurface Investigation, subsection 2.2 Field Screening Results, soils collected from installed test pits were screened for elevated headspace responses. Documented maximum headspace responses for soils examined from soil borings ranged from 0.1 to 0.5 ppm. See Attachment C Test Pit Logs for details regarding soil description, observations, and acquired headspace values. During the installation of test pits, asphalt and brick were observed in TP-2 at two to three-feet below grade. A buried grass layer was also encountered in TP-2 at six feet below grade, which suggests a previous surface grade prior to the application of fill material, as native soils were present below the grass layer. It should be stated that the lateral extent of this grass layer was not explored beyond the limits of TP-2, nor was it determined if the layer existed prior to or was a result of historic fill application. Brick, asphalt, and coal were observed in TP-3 from grade to four feet below grade. NYSDEC Commissioner Policy CP-51 provides framework for selecting specific soil cleanup levels for each of the remedial programs in NYSDEC s Division of Environmental Remediation. There are several approaches utilized to determine site-specific soil cleanup objectives. Primary factors attributable to the selected approach are protection of public health and the environment and prevention of off-site migration of waste. Thus, it is necessary to look at each of these factors, as they relate to the Site and the proposed development of it. It is our understanding that the proposed development of 4301 NYS Route 9G includes construction of a 9,100 SF retail store to be utilized for commercial use. Given the current proposed plan, approximately 50% of the Site will be covered with relatively impermeable materials such as building materials, concrete, and asphalt. Thus, it is reasonable to assume that direct contact with soils by the general public will be prevented following the proposed site development. Proposed development should also eliminate off site migration potential of contaminants. Given these factors and in light of the fact that this is an unclassified site and has not previously and is not currently assigned to a NYSDEC remedial program administered by the Division of Environmental Remediation, PES opines it is appropriate to utilize the Restricted Use SCOs as found in 6 NYCRR Table (b). Given this approach, the SCO is determined based on the applicable land use category for protection of public health, which in this particular case would be commercial use. When the analytical results are compared to the corresponding SCOs, as provided in Table 1, it becomes apparent that soil sample analytical results from the July 2015 subsurface investigation indicate that reported concentrations of PAHs in the soil samples from TP-3, specifically benzo(k)fluoranthene (870 ppb) and indeno(1,2,3-cd)pyrene (680 ppb), were not reported above the Soil SCO s Protection of Public Health, Commercial Use. Please refer to Attachment D Laboratory Analytical Reports for soil analytical results. According to the USEPA, most PAHs are formed during the incomplete burning of coal, oil and gas, garbage, or other organic substances, like tobacco or charbroiled meat. Some are manufactured and are found in coal tar, crude oil, creosote, and roofing tar. There were no specific substances found within the

7 Mr. Simon List, SITECH Consulting, P.C. Page NYS Route 9G, Germantown, Columbia County, NY Limited Subsurface Investigation Report, PES Project No fill material that could accurately determine the cause for the elevated PAH concentrations. Several possible sources identified include urban-type fill deposits consisting of coal slag and fly ash and asphaltic materials including cementitious asphalt and asphalt sealer that were present in buried asphalt unearthed during test pit excavation. Heavy metals detected in each of the samples were reported below the Restricted Use SCOs and even below Unrestricted SCOs. These metals are naturally occurring and thus could be indigenes to the area. To accurately determine the source of their presence, further testing of soils within the general area of the site to determine background levels would be necessary, including off-site locations. PES believes this is not necessary, as the levels of metals detected onsite were below the recommended SCOs. 6.0 RECOMMENDATIONS Based on the results of the July 2015 limited subsurface investigation, recommendations include notification of the current property owner regarding the results of the limited subsurface investigation, and notification of the NYSDEC regarding the results of the limited subsurface investigation. The need to further assess contaminants found during the course of the investigation should be based on, in part, input from the NYSDEC and the information presented in this report. PES recommends assigning the site a No Further Action status under the pretense that onsite soils remain undisturbed during the prescribed site development. In the event that onsite soils require handling, we recommend PES (or other qualified environmental professional) be contracted to oversee handling and processing of existing site soils and fill whether they be used onsite as suitable borrow or disposed offsite. A site management plan should be considered, so workers are prepared and possess the training necessary to deal with possible contaminants, as they may be encountered during intrusive work at the Site in areas of identified fill deposits. Should fill deposits be required to leave the Site, it is recommended that they be fully excavated, stockpiled, and further characterized through laboratory analysis. Should further analysis determine the material contains contaminants that exceed Unrestricted Use SCOs, they should be property disposed of in a Subtitle D landfill that is capable of properly managing the waste. 7.0 DISCLAIMER Any statement or opinion contained in this Report prepared by Precision Environmental Services, Inc. (PES) shall not be construed to create any warranty or representation that the real or personal property on which the investigation was conducted is free of pollution or complies with any or all applicable regulatory or statutory requirements, or that the property is fit for any particular purpose. Unless otherwise indicated in this Report, PES did not independently determine the compliance of present or past owners of the site with federal, state or local laws and regulations. The conclusions presented in this Report were based upon the services described, within the time and budgetary constraints imposed by the client, and not on scientific tasks or procedures beyond the scope of those described services. PES shall not be responsible for conditions or consequences arising from any facts that were concealed, withheld or not fully disclosed by any person at the time the evaluation was performed.

8 Mr. Simon List, SITECH Consulting, P.C. Page NYS Route 9G, Germantown, Columbia County, NY Limited Subsurface Investigation Report, PES Project No Any person or entity considering the acquisition, use or other involvement or activity concerning the property that is the subject of this Report shall be solely responsible for determining the adequacy of the property for any and all such purposes. The person or entity should enter into any such acquisition or use relying solely on its own judgment and personal investigation of the property, and not upon reliance of any representation by PES regarding the property or the character, quality or value thereof. Should you have any questions regarding the above report, please feel free to contact us at Sincerely, PRECISION ENVIRONMENTAL SERVICES, INC. Daniel R. Nierenberg Project Manager/Geologist John J. Johnson Senior Hydrogeologist

9 ATTACHMENT A Figures

10 TP-4 TP-2 TP-3 TP-1 TP-5 PRECISION ENVIRONMENTAL SERVICES, INC. 831 RT. 67,LOT 38 BALLSTON SPA, NY TEL: FAX: CERTIFIED WOMEN-OWNED BUSINESS ENTERPRISE SITECH - GERMANTOWN SITE MAP Location: 4301 NYS Route 9G, Germantown, Columbia County, New York Project No.: PES Job No Scale: 1 : 40 Date: July 31, 2015 Figure: 2

11 ATTACHMENT B Tables

12 Primax - SITECH - Germantown 4301 Route 9G, Germantown, Columbia County, New York PES Job No Sampling Date: July 30, 2015 Parameter Method Units TABLE 2 Summary of Soil Boring Analytical Results NYSDEC Subpart Remedial Program Soil Cleanup Objectives Soil Boring Identification Restricted Use Protection of Public Health Protection of Protection of Unrestricted Use Restricted Ecological TP-2 TP-3 TP-4 TP-5 Residential Commercial Industrial Groundwater Residential Resources Silver 13 Priority Pollutant Metals mg/kg ND ND ND ND ,500 6, Arsenic 13 Priority Pollutant Metals mg/kg Beryllium 13 Priority Pollutant Metals mg/kg , Cadmium 13 Priority Pollutant Metals mg/kg ND ND ND ND Trivalent Chromium 13 Priority Pollutant Metals mg/kg NS Hexavalent Chromium 13 Priority Pollutant Metals mg/kg ND ND ND ND Copper 13 Priority Pollutant Metals mg/kg , ,720 Mercury 13 Priority Pollutant Metals mg/kg ND 0.06 ND Nickel 13 Priority Pollutant Metals mg/kg , Lead 13 Priority Pollutant Metals mg/kg ,000 6, Antimony 13 Priority Pollutant Metals mg/kg ND ND ND ND 10,000* 4 10,000* 4 10,000* 4 10,000* 4 10,000* 4 10,000* 4 10,000* 4 Selenium 13 Priority Pollutant Metals mg/kg ND ND ND ND ,500 6, Thallium 13 Priority Pollutant Metals mg/kg ND ND ND ND 10,000* 4 10,000* 4 10,000* 4 10,000* 4 10,000* 4 10,000* 4 10,000* 4 Zinc 13 Priority Pollutant Metals mg/kg ,200 10,000 10,000 10, ,480 TPH GRO TPH GRO mg/kg ND ND ND ND TPH DRO TPH DRO mg/kg ND ND ND ND Total Compounds Total Petroleum Hydrocarbons mg/kg ND ND ND ND 2-Methylnaphthalene EPA Priority Pollutant PAHs μg/kg ND ND ND ND 100,000* 1 410* 5 100,000* 1 500,000* 2 1,000,000* 3 100,000* 1 1,000,000* 3 Acenaphthalene EPA Priority Pollutant PAHs μg/kg ND ND ND ND 20, , , ,000 1,000,000 20,000 20,000 Acenaphthylene EPA Priority Pollutant PAHs μg/kg ND ND ND ND 100, , , ,000 1,000,000 NS 100,000 Anthrancene EPA Priority Pollutant PAHs μg/kg ND ND ND ND 100, , , ,000 1,000,000 NS 100,000 Benz(a)anthracene EPA Priority Pollutant PAHs μg/kg ND ND ND 1,000 1,000 1,000 5,600 11,000 NS 1,000 Benzo(a)pyrene EPA Priority Pollutant PAHs μg/kg ND ND ND 1,000 1,000 1,000 1,000 1,100 2,600 1,000 Benzo(b)fluoranthene EPA Priority Pollutant PAHs μg/kg ND ND ND 1,000 1,000 1,000 5,600 11,000 NS 1,000 Benzo(g,h,i)perylene EPA Priority Pollutant PAHs μg/kg ND ND ND 100, , , ,000 1,000,000 NS 100,000 Benzo(k)fluoranthene EPA Priority Pollutant PAHs μg/kg ND ND ND 800 1,000 3,900 56, ,000 NS 800 Chrysene EPA Priority Pollutant PAHs μg/kg ND ND ND 1,000 1,000 3,900 56, ,000 NS 1,000 Dibenz(a, h)anthracene EPA Priority Pollutant PAHs μg/kg ND ND ND ND ,100 NS 330 Fluoranthene EPA Priority Pollutant PAHs μg/kg ND ND ND 100, , , ,000 1,000,000 NS 100,000 Fluorene EPA Priority Pollutant PAHs μg/kg ND ND ND ND 30, , , ,000 1,000,000 30,000 30,000 Indeno(1, 2, 3-cd)pyrene EPA Priority Pollutant PAHs μg/kg ND ND ND ,600 11,000 NS 500 Naphthalene EPA Priority Pollutant PAHs μg/kg ND ND ND ND 12, , , ,000 1,000,000 NS 12,000 Phenanthrene EPA Priority Pollutant PAHs μg/kg ND ND ND ND 100, , , ,000 1,000,000 NS 100,000 Pyrene EPA Priority Pollutant PAHs μg/kg ND ND ND 100, , , ,000 1,000,000 NS 100,000 Total Compounds EPA Priority Pollutant PAHs μg/kg ND 7, ND ND Analytical Facility - Phoenix Environmental Laboratories, Inc - Manchester, NY ND indicates values reported below the laboratory minimum detection limits Values in BOLD indicate values reported above the laboratory minimum detection limits NA indicates no data available * 1 NYSDEC - Subpart Development or Modification of Soil Cleanup Objective (b)(2)(i) * 2 NYSDEC - Subpart Development or Modification of Soil Cleanup Objective (b)(2)(ii) * 3 NYSDEC - Subpart Development or Modification of Soil Cleanup Objective (b)(2)(iiii) * 4 NYSDEC - Subpart Development or Modification of Soil Cleanup Objective (b)(3) *5 NYSDEC Final Commisioner Policy, CP-51 - Table 1: Supplemental Soil Cleanup Objectives Page 1 of 2

13 ATTACHMENT C Test Pit Logs

14 PES P R E C I S I O N Environmental Services, Inc. Lot 38A, Curtis Industrial Park 831 Route 67 Ballston Spa, NY TEL: FAX: Project: SITECH - Germantown Client: SITECH Project No: Location: 4301 Route 9G, Germantown, NY Operator: Carl Graves Drilling Contractor: PES Date Installed: 7/30/15 TOC Elevation: - Logged by: Dan Nierenberg Installation Method: Excavator Date Developed: - Total Depth of Hole: 5.5 Boring Diameter: - Screen Diameter: - Length: - Slot Size: - Riser Diameter: - Length: - Type: Test Pit Sand Pack: - Bentonite Seal: - Protective Casing: - DRILLING LOG Test Pit No.: TP-1 See Site Map Page of 1 5 Depth (ft.) Well Construction Notes Sample Type/ # PID (ppm) Description / Soil Classification 0 (Grade) : grass, organics; changing to tan/brown/grey fine SAND and SILT, little to no CLAY, dry : brown fine SAND and SILT, with medium SAND mix, some to little CLAY, dry : tan/brown/grey fine SAND and SILT, tight, with little CLAY, increasing moisture with depth 2-3 : tan/brown fine SAND and SILT, with increasing medium SAND content with depth; changing to grey/brown, dry : brown/tan fine SAND and SILT, with little medium SAND mix, little CLAY, dry, bedrock stone (graywacke?), Refusal at 5.5 BG TP-1 COMPLETED AT 5.5 REFUSAL AT 5.5 BELOW GRADE NO SOIL SAMPLES COLLECTED FROM TP-1 SUBMITTED FOR LABORATORY ANALYSES. TP-1 BACKFILLED WITH CLEAN, NATIVE MATERIAL AMBIENT AIR PID READINGS = NON-DETECT ND = No VOCs Detected By PID analysis = Sample Submitted for Laboratory Analysis *

15 PES P R E C I S I O N Environmental Services, Inc. Lot 38A, Curtis Industrial Park 831 Route 67 Ballston Spa, NY TEL: FAX: Project: SITECH - Germantown Client: SITECH Project No: Location: 4301 Route 9G, Germantown, NY Operator: Carl Graves Drilling Contractor: PES Date Installed: 7/30/15 TOC Elevation: - Logged by: Dan Nierenberg Installation Method: Excavator Date Developed: - Total Depth of Hole: 9 Boring Diameter: - Screen Diameter: - Length: - Slot Size: - Riser Diameter: - Length: - Type: Test Pit Sand Pack: - Bentonite Seal: - Protective Casing: - DRILLING LOG Test Pit No.: TP-2 See Site Map Page of 2 5 Depth (ft.) Well Construction Notes Sample Type/ # PID (ppm) Description / Soil Classification 0 (Grade) : black mulch; changing to brown/tan coarse/medium/fine SAND, poorly sorted, with rock and fine gravel mix, some to little SILT, no CLAY, dry : grey/brown coarse/medium/fine SAND, poorly sorted, with medium/fine gravel mix, few large stones, section of asphalt, section of old drainage pipe encountered : brown/grey coarse/medium/fine SAND, poorly sorted, with SILT and CLAY mix, some fine gravel mix, decreasing large rock content, increasing CLAY and SILT content with depth : brown/tan coarse/medium/fine SAND, poorly sorted, with rock and fine gravel mix, some to little SILT, no CLAY, dry, decreasing large stone content with depth 4-5 : grey/dark grey coarse/medium/fine SAND, poorly sorted, with SILT and CLAY mix, some fine gravel mix, with lenses of clayey SILT/SAND with organics 5-7 : above; grass mat at 6 BG, brown/tan medium/fine SAND, with some SILT and little CLAY 7-8 : tan/brown/grey fine SAND with SILT and CLAY, with little fine/medium gravel mix, moist 8-9 : tan/grey fine SAND and SILT, with some CLAY, tight, dry TP-2 COMPLETED AT 9 SOIL SAMPLES TP-2 SUBMITTED FOR LABORATORY ANALYSES VIA TPH DRO, TPH GRO, 13 PRIORITY POLLUTANT METALS, AND EPA PRIORITY POLLUTANT PAHS TP-2 BACKFILLED WITH CLEAN, NATIVE MATERIAL AMBIENT AIR PID READINGS = NON-DETECT ND = No VOCs Detected By PID analysis = Sample Submitted for Laboratory Analysis *

16 PES P R E C I S I O N Environmental Services, Inc. Lot 38A, Curtis Industrial Park 831 Route 67 Ballston Spa, NY TEL: FAX: Project: SITECH - Germantown Client: SITECH Project No: Location: 4301 Route 9G, Germantown, NY Operator: Carl Graves Drilling Contractor: PES Date Installed: 7/30/15 TOC Elevation: - Logged by: Dan Nierenberg Installation Method: Excavator Date Developed: - Total Depth of Hole: 9 Boring Diameter: - Screen Diameter: - Length: - Slot Size: - Riser Diameter: - Length: - Type: Test Pit Sand Pack: - Bentonite Seal: - Protective Casing: - DRILLING LOG Test Pit No.: TP-3 See Site Map Page of 3 5 Depth (ft.) Well Construction Notes Sample Type/ # PID (ppm) Description / Soil Classification 0 (Grade) : tan fine SAND and SILT, no CLAY, dry, with medium/fine gravel mixed, brick : dark brown/brown medium/fine/coarse SAND, well sorted, with increasing SILT content with depth, little to no CLAY, coal : tan fine SAND and SILT, no CLAY, with medium/fine gravel mixed; changing to brown/tan with increasing medium/coarse SAND content with depth, dry 2-3 : dark brown/brown medium/fine/coarse SAND, well sorted, with little to no SILT or CLAY, no odors, dry 4-6 : dark brown/brown medium/fine/coarse SAND, well sorted, with little SILT, little to no CLAY, changing to black/grey fine SAND and SILT, with some CLAY content, moist(?) 6-7 : black medium/fine SAND, poorly sorted, with some CLAY, little SAND, moist, some lenses of fine SAND and SILT/CLAY; changing to grey fine SAND and SILT/CLAY at depths with organics (grass) 7-8 : black medium/fine/coarse SAND, poorly sorted, with some to little CLAY, little SILT, moist, organics 8-9 : brown/tan fine SAND and SILT, with little to some CLAY, dry TP-3 COMPLETED AT 9 SOIL SAMPLES TP-3 SUBMITTED FOR LABORATORY ANALYSES VIA TPH DRO, TPH GRO, 13 PRIORITY POLLUTANT METALS, EPA PRIORITY POLLUTANT PAHS, AND PCBS TP-3 BACKFILLED WITH CLEAN, NATIVE MATERIAL AMBIENT AIR PID READINGS = NON-DETECT ND = No VOCs Detected By PID analysis = Sample Submitted for Laboratory Analysis *

17 PES P R E C I S I O N Environmental Services, Inc. Lot 38A, Curtis Industrial Park 831 Route 67 Ballston Spa, NY TEL: FAX: Project: SITECH - Germantown Client: SITECH Project No: Location: 4301 Route 9G, Germantown, NY Operator: Carl Graves Drilling Contractor: PES Date Installed: 7/30/15 TOC Elevation: - Logged by: Dan Nierenberg Installation Method: Excavator Date Developed: - Total Depth of Hole: 6.5 Boring Diameter: - Screen Diameter: - Length: - Slot Size: - Riser Diameter: - Length: - Type: Test Pit Sand Pack: - Bentonite Seal: - Protective Casing: - DRILLING LOG Test Pit No.: TP-4 See Site Map Page of 4 5 Depth (ft.) Well Construction Notes Sample Type/ # PID (ppm) Description / Soil Classification 0 (Grade) ND : tan/brown coarse/medium/fine SAND, poorly sorted, with little SILT, little to no CLAY, dry, with large stone and medium gravel, asphalt 1-2 : tan/brown coarse/medium/fine SAND, poorly sorted, with little SILT, little to no CLAY, dry, with large stone and medium gravel 2-3 : above with increasing large rock content; changing to tan/brown fine SAND and CLAY, with little SILT and medium SAND mixed 3-5 : brown coarse/medium/fine SAND, poorly sorted, with some CLAY and SILT content, moist : brown coarse/medium/fine SAND, poorly sorted, with some CLAY and SILT content, bedrock refusal at 6.5 BG TP-4 COMPLETED AT 6.5 REFUSAL AT 6.5 BELOW GRADE SOIL SAMPLES TP-4 SUBMITTED FOR LABORATORY ANALYSES VIA TPH DRO, TPH GRO, 13 PRIORITY POLLUTANT METALS, AND EPA PRIORITY POLLUTANT PAHS TP-4 BACKFILLED WITH CLEAN, NATIVE MATERIAL AMBIENT AIR PID READINGS = NON-DETECT ND = No VOCs Detected By PID analysis = Sample Submitted for Laboratory Analysis *

18 PES P R E C I S I O N Environmental Services, Inc. Lot 38A, Curtis Industrial Park 831 Route 67 Ballston Spa, NY TEL: FAX: Project: SITECH - Germantown Client: SITECH Project No: Location: 4301 Route 9G, Germantown, NY Operator: Carl Graves Drilling Contractor: PES Date Installed: 7/30/15 TOC Elevation: - Logged by: Dan Nierenberg Installation Method: Excavator Date Developed: - Total Depth of Hole: 6 Boring Diameter: - Screen Diameter: - Length: - Slot Size: - Riser Diameter: - Length: - Type: Test Pit Sand Pack: - Bentonite Seal: - Protective Casing: - DRILLING LOG Test Pit No.: TP-5 See Site Map Page of 5 5 Depth (ft.) Well Construction Notes Sample Type/ # PID (ppm) Description / Soil Classification 0 (Grade) : brown coarse/medium/fine SAND, poorly sorted, with little to no SILT, no CLAY, stone mixed : grey/tan fine SAND and SILT, little to no CLAY, no stone/gravel, dry, tight, dense : brown coarse/medium/fine SAND, poorly sorted, with little to no SILT, no CLAY, stone mixed 2-3 : brown medium/coarse/fine SAND, poorly sorted, with little SILT and CLAY content, large stone throughout, bony, dry 4-5 : grey/tan fine SAND and SILT, little to no CLAY, no stone/gravel, dry, tight : grey/tan fine SAND and SILT, little to no CLAY, no stone/gravel, dry, tight TP-5 COMPLETED AT 6 REFUSAL AT 5.5 BELOW GRADE SOIL SAMPLES TP-5 SUBMITTED FOR LABORATORY ANALYSES VIA TPH DRO, TPH GRO, 13 PRIORITY POLLUTANT METALS, AND EPA PRIORITY POLLUTANT PAHS TP-5 BACKFILLED WITH CLEAN, NATIVE MATERIAL AMBIENT AIR PID READINGS = NON-DETECT ND = No VOCs Detected By PID analysis = Sample Submitted for Laboratory Analysis *

19 ATTACHMENT D Laboratory Analytical Reports

20 Draft Progress Report Sample Information Matrix: Location Code: Rush Request: P.O.#: Project ID: Client ID: Parameter August 07, 2015 SOIL PRECISIN 24 Hour RT 9G GERMANTOWN TP-2 Environmental Laboratories, Inc. 587 East Middle Turnpike, P.O.Box 370, Manchester, CT Tel. (860) Fax (860) Result FOR: Custody Information Collected by: Received by: Analyzed by: LB Laboratory Data Attn: Mr. Dan Nierenberg Precision Env. Services, Inc. 831 Route 67 Lot 38A Ballston Spa, NY see "By" below Date 07/30/15 07/31/15 Time 11:15 17:50 SDG ID: GBJ66838 Phoenix ID: BJ66838 RL/ PQL Units Dilution Date/Time By Reference Silver < mg/kg 1 08/04/15 LK SW6010C Arsenic mg/kg 1 08/04/15 LK SW6010C Beryllium mg/kg 1 08/04/15 LK SW6010C Cadmium < mg/kg 1 08/04/15 LK SW6010C Chromium mg/kg 1 08/04/15 LK SW6010C Copper mg/kg 1 08/04/15 LK SW6010C Mercury < mg/kg 1 08/04/15 MA SW7471B Nickel mg/kg 1 08/04/15 LK SW6010C Lead mg/kg 1 08/04/15 LK SW6010C Antimony < mg/kg 1 08/04/15 LK SW6010C Selenium < mg/kg 1 08/04/15 LK SW6010C Thallium < mg/kg 1 08/04/15 LK SW6010C Trivalent Chromium mg/kg 1 08/07/15 KH Calculation Zinc mg/kg 1 08/04/15 LK SW6010C Percent Solid 80 % 07/31/15 I SW846-%Solid Chromium, Hexavalent < mg/kg 1 08/07/15 KH SW7196A ph - Soil ph Units 1 08/06/15 21:45 DH/KDB SW Redox Potential mv 1 08/06/15 DH/KDB SM2580B-09 1 Soil Extraction SVOA PAH Completed 08/03/15 JJ/VH SW3545A Mercury Digestion Completed 08/04/15 I/I SW7471B Total Metals Digest Completed 08/03/15 G/AG SW3050B Extraction of TPH SM Completed 08/03/15 BC/V SW3545A Gasoline Range Hydrocarbons (C6-C10) GRO (C6-C10) ND 8.8 mg/kg 50 08/04/15 LA SW8015D MOD 1 QA/QC Surrogates % 2,5-Dibromotoluene (FID) 110 % 50 08/04/15 LA % Page 1 of 10 Ver 1

21 Project ID: 4301 RT 9G GERMANTOWN Client ID: TP-2 Parameter TPH DRO (C10-C28) Result Phoenix I.D.: BJ66838 RL/ PQL Units Dilution Date/Time By Reference Diesel Range Organics (C10-C28) ND 62 mg/kg 1 08/05/15 JRB SW8015D DRO QA/QC Surrogates % n-pentacosane 74 % 1 08/05/15 JRB % Polynuclear Aromatic HC 2-Methylnaphthalene ND 290 ug/kg 1 08/04/15 DD SW8270D Acenaphthene ND 290 ug/kg 1 08/04/15 DD SW8270D Acenaphthylene ND 290 ug/kg 1 08/04/15 DD SW8270D Anthracene ND 290 ug/kg 1 08/04/15 DD SW8270D Benz(a)anthracene ND 290 ug/kg 1 08/04/15 DD SW8270D Benzo(a)pyrene ND 290 ug/kg 1 08/04/15 DD SW8270D Benzo(b)fluoranthene ND 290 ug/kg 1 08/04/15 DD SW8270D Benzo(ghi)perylene ND 290 ug/kg 1 08/04/15 DD SW8270D Benzo(k)fluoranthene ND 290 ug/kg 1 08/04/15 DD SW8270D Chrysene ND 290 ug/kg 1 08/04/15 DD SW8270D Dibenz(a,h)anthracene ND 290 ug/kg 1 08/04/15 DD SW8270D Fluoranthene ND 290 ug/kg 1 08/04/15 DD SW8270D Fluorene ND 290 ug/kg 1 08/04/15 DD SW8270D Indeno(1,2,3-cd)pyrene ND 290 ug/kg 1 08/04/15 DD SW8270D Naphthalene ND 290 ug/kg 1 08/04/15 DD SW8270D Phenanthrene ND 290 ug/kg 1 08/04/15 DD SW8270D Pyrene ND 290 ug/kg 1 08/04/15 DD SW8270D QA/QC Surrogates % 2-Fluorobiphenyl 53 % 1 08/04/15 DD % % Nitrobenzene-d5 51 % 1 08/04/15 DD % % Terphenyl-d14 70 % 1 08/04/15 DD % 1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time. RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level Comments: The regulatory hold time for ph is immediately. This ph was performed in the laboratory and may be considered outside of hold-tim Hexavalent Chromium: This sample is in a reducing state. All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments. If there are any questions regarding this data, please call Phoenix Client Services at extension 200. This report must not be reproduced except in full as defined by the attached chain of custody. PLEASE NOTE: THIS PROGRESS REPORT IS CONSIDERED PRELIMINARY DATA. THE RESULTS ENTERED HAVE NOT BEEN EXAMINED BY OUR QA/QC DEPARTMENT. Phyllis Shiller, Laboratory Director August 07, 2015 Page 2 of 10 Ver 1

22 Draft Progress Report Sample Information Matrix: Location Code: Rush Request: P.O.#: Project ID: Client ID: Parameter August 07, 2015 SOIL PRECISIN 24 Hour RT 9G GERMANTOWN TP-3 Environmental Laboratories, Inc. 587 East Middle Turnpike, P.O.Box 370, Manchester, CT Tel. (860) Fax (860) Result FOR: Custody Information Collected by: Received by: Analyzed by: LB Laboratory Data Attn: Mr. Dan Nierenberg Precision Env. Services, Inc. 831 Route 67 Lot 38A Ballston Spa, NY see "By" below Date 07/30/15 07/31/15 Time 12:10 17:50 SDG ID: GBJ66838 Phoenix ID: BJ66839 RL/ PQL Units Dilution Date/Time By Reference Silver < mg/kg 1 08/04/15 LK SW6010C Arsenic mg/kg 1 08/04/15 LK SW6010C Beryllium mg/kg 1 08/04/15 LK SW6010C Cadmium < mg/kg 1 08/04/15 LK SW6010C Chromium mg/kg 1 08/04/15 LK SW6010C Copper mg/kg 1 08/04/15 LK SW6010C Mercury mg/kg 1 08/04/15 MA SW7471B Nickel mg/kg 1 08/04/15 LK SW6010C Lead mg/kg 1 08/04/15 LK SW6010C Antimony < mg/kg 1 08/04/15 LK SW6010C Selenium < mg/kg 1 08/04/15 LK SW6010C Thallium < mg/kg 1 08/04/15 LK SW6010C Trivalent Chromium mg/kg 1 08/07/15 KH Calculation Zinc mg/kg 1 08/04/15 LK SW6010C Percent Solid 83 % 07/31/15 I SW846-%Solid Chromium, Hexavalent < mg/kg 1 08/07/15 KH SW7196A ph - Soil ph Units 1 08/06/15 21:45 DH/KDB SW Redox Potential mv 1 08/06/15 DH/KDB SM2580B-09 1 Soil Extraction for PCB Completed 08/05/15 CC/H SW3545A Soil Extraction SVOA PAH Completed 08/03/15 JJ/VH SW3545A Mercury Digestion Completed 08/04/15 I/I SW7471B Total Metals Digest Completed 08/03/15 G/AG SW3050B Extraction of TPH SM Completed 08/03/15 BC/V SW3545A Gasoline Range Hydrocarbons (C6-C10) GRO (C6-C10) ND 10 mg/kg 50 08/04/15 LA SW8015D MOD 1 QA/QC Surrogates % 2,5-Dibromotoluene (FID) 113 % 50 08/04/15 LA % Page 3 of 10 Ver 1

23 Project ID: 4301 RT 9G GERMANTOWN Client ID: TP-3 Parameter Polychlorinated Biphenyls Result Phoenix I.D.: BJ66839 RL/ PQL Units Dilution Date/Time By Reference PCB-1016 ND 400 ug/kg 10 08/06/15 AW SW8082A PCB-1221 ND 400 ug/kg 10 08/06/15 AW SW8082A PCB-1232 ND 400 ug/kg 10 08/06/15 AW SW8082A PCB-1242 ND 400 ug/kg 10 08/06/15 AW SW8082A PCB-1248 ND 400 ug/kg 10 08/06/15 AW SW8082A PCB-1254 ND 400 ug/kg 10 08/06/15 AW SW8082A PCB-1260 ND 400 ug/kg 10 08/06/15 AW SW8082A PCB-1262 ND 400 ug/kg 10 08/06/15 AW SW8082A PCB-1268 ND 400 ug/kg 10 08/06/15 AW SW8082A QA/QC Surrogates % DCBP 104 % 10 08/06/15 AW % % TCMX 88 % 10 08/06/15 AW % TPH DRO (C10-C28) Diesel Range Organics (C10-C28) ND 60 mg/kg 1 08/05/15 JRB SW8015D DRO QA/QC Surrogates % n-pentacosane 92 % 1 08/05/15 JRB % Polynuclear Aromatic HC 2-Methylnaphthalene ND 280 ug/kg 1 08/04/15 DD SW8270D Acenaphthene ND 280 ug/kg 1 08/04/15 DD SW8270D Acenaphthylene ND 280 ug/kg 1 08/04/15 DD SW8270D Anthracene ND 280 ug/kg 1 08/04/15 DD SW8270D Benz(a)anthracene ug/kg 1 08/04/15 DD SW8270D Benzo(a)pyrene ug/kg 1 08/04/15 DD SW8270D Benzo(b)fluoranthene ug/kg 1 08/04/15 DD SW8270D Benzo(ghi)perylene ug/kg 1 08/04/15 DD SW8270D Benzo(k)fluoranthene ug/kg 1 08/04/15 DD SW8270D Chrysene ug/kg 1 08/04/15 DD SW8270D Dibenz(a,h)anthracene ND 280 ug/kg 1 08/04/15 DD SW8270D Fluoranthene ug/kg 1 08/04/15 DD SW8270D Fluorene ND 280 ug/kg 1 08/04/15 DD SW8270D Indeno(1,2,3-cd)pyrene ug/kg 1 08/04/15 DD SW8270D Naphthalene ND 280 ug/kg 1 08/04/15 DD SW8270D Phenanthrene ND 280 ug/kg 1 08/04/15 DD SW8270D Pyrene ug/kg 1 08/04/15 DD SW8270D QA/QC Surrogates % 2-Fluorobiphenyl 54 % 1 08/04/15 DD % % Nitrobenzene-d5 51 % 1 08/04/15 DD % % Terphenyl-d14 54 % 1 08/04/15 DD % Page 4 of 10 Ver 1

24 Project ID: 4301 RT 9G GERMANTOWN Client ID: TP-3 Parameter Comments: Result Phoenix I.D.: BJ66839 RL/ PQL Units Dilution Date/Time By Reference 1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time. RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level The regulatory hold time for ph is immediately. This ph was performed in the laboratory and may be considered outside of hold-tim Hexavalent Chromium: This sample is in a reducing state. All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments. If there are any questions regarding this data, please call Phoenix Client Services at extension 200. This report must not be reproduced except in full as defined by the attached chain of custody. PLEASE NOTE: THIS PROGRESS REPORT IS CONSIDERED PRELIMINARY DATA. THE RESULTS ENTERED HAVE NOT BEEN EXAMINED BY OUR QA/QC DEPARTMENT. Phyllis Shiller, Laboratory Director August 07, 2015 Page 5 of 10 Ver 1

25 Draft Progress Report Sample Information Matrix: Location Code: Rush Request: P.O.#: Project ID: Client ID: Parameter August 07, 2015 SOIL PRECISIN 24 Hour RT 9G GERMANTOWN TP-4 Environmental Laboratories, Inc. 587 East Middle Turnpike, P.O.Box 370, Manchester, CT Tel. (860) Fax (860) Result FOR: Custody Information Collected by: Received by: Analyzed by: LB Laboratory Data Attn: Mr. Dan Nierenberg Precision Env. Services, Inc. 831 Route 67 Lot 38A Ballston Spa, NY see "By" below Date 07/30/15 07/31/15 Time 12:47 17:50 SDG ID: GBJ66838 Phoenix ID: BJ66840 RL/ PQL Units Dilution Date/Time By Reference Silver < mg/kg 1 08/04/15 LK SW6010C Arsenic mg/kg 1 08/04/15 LK SW6010C Beryllium mg/kg 1 08/04/15 LK SW6010C Cadmium < mg/kg 1 08/04/15 LK SW6010C Chromium mg/kg 1 08/04/15 LK SW6010C Copper mg/kg 1 08/04/15 LK SW6010C Mercury < mg/kg 1 08/04/15 MA SW7471B Nickel mg/kg 1 08/04/15 LK SW6010C Lead mg/kg 1 08/04/15 LK SW6010C Antimony < mg/kg 1 08/04/15 LK SW6010C Selenium < mg/kg 1 08/04/15 LK SW6010C Thallium < mg/kg 1 08/04/15 LK SW6010C Trivalent Chromium mg/kg 1 08/07/15 KH Calculation Zinc mg/kg 1 08/04/15 LK SW6010C Percent Solid 93 % 07/31/15 I SW846-%Solid Chromium, Hexavalent < mg/kg 1 08/07/15 KH SW7196A ph - Soil ph Units 1 08/06/15 21:45 DH/KDB SW Redox Potential mv 1 08/06/15 DH/KDB SM2580B-09 1 Soil Extraction SVOA PAH Completed 08/03/15 JJ/VH SW3545A Mercury Digestion Completed 08/04/15 I/I SW7471B Total Metals Digest Completed 08/03/15 G/AG SW3050B Extraction of TPH SM Completed 08/03/15 BC/V SW3545A Gasoline Range Hydrocarbons (C6-C10) GRO (C6-C10) ND 5.5 mg/kg 50 08/04/15 LA SW8015D MOD 1 QA/QC Surrogates % 2,5-Dibromotoluene (FID) 95 % 50 08/04/15 LA % Page 6 of 10 Ver 1

26 Project ID: 4301 RT 9G GERMANTOWN Client ID: TP-4 Parameter TPH DRO (C10-C28) Result Phoenix I.D.: BJ66840 RL/ PQL Units Dilution Date/Time By Reference Diesel Range Organics (C10-C28) ND 53 mg/kg 1 08/05/15 JRB SW8015D DRO QA/QC Surrogates % n-pentacosane 74 % 1 08/05/15 JRB % Polynuclear Aromatic HC 2-Methylnaphthalene ND 250 ug/kg 1 08/04/15 DD SW8270D Acenaphthene ND 250 ug/kg 1 08/04/15 DD SW8270D Acenaphthylene ND 250 ug/kg 1 08/04/15 DD SW8270D Anthracene ND 250 ug/kg 1 08/04/15 DD SW8270D Benz(a)anthracene ND 250 ug/kg 1 08/04/15 DD SW8270D Benzo(a)pyrene ND 250 ug/kg 1 08/04/15 DD SW8270D Benzo(b)fluoranthene ND 250 ug/kg 1 08/04/15 DD SW8270D Benzo(ghi)perylene ND 250 ug/kg 1 08/04/15 DD SW8270D Benzo(k)fluoranthene ND 250 ug/kg 1 08/04/15 DD SW8270D Chrysene ND 250 ug/kg 1 08/04/15 DD SW8270D Dibenz(a,h)anthracene ND 250 ug/kg 1 08/04/15 DD SW8270D Fluoranthene ND 250 ug/kg 1 08/04/15 DD SW8270D Fluorene ND 250 ug/kg 1 08/04/15 DD SW8270D Indeno(1,2,3-cd)pyrene ND 250 ug/kg 1 08/04/15 DD SW8270D Naphthalene ND 250 ug/kg 1 08/04/15 DD SW8270D Phenanthrene ND 250 ug/kg 1 08/04/15 DD SW8270D Pyrene ND 250 ug/kg 1 08/04/15 DD SW8270D QA/QC Surrogates % 2-Fluorobiphenyl 49 % 1 08/04/15 DD % % Nitrobenzene-d5 46 % 1 08/04/15 DD % % Terphenyl-d14 60 % 1 08/04/15 DD % 1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time. RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level Comments: The regulatory hold time for ph is immediately. This ph was performed in the laboratory and may be considered outside of hold-tim Hexavalent Chromium: This sample is in a reducing state. All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments. If there are any questions regarding this data, please call Phoenix Client Services at extension 200. This report must not be reproduced except in full as defined by the attached chain of custody. PLEASE NOTE: THIS PROGRESS REPORT IS CONSIDERED PRELIMINARY DATA. THE RESULTS ENTERED HAVE NOT BEEN EXAMINED BY OUR QA/QC DEPARTMENT. Phyllis Shiller, Laboratory Director August 07, 2015 Page 7 of 10 Ver 1

27 Draft Progress Report Sample Information Matrix: Location Code: Rush Request: P.O.#: Project ID: Client ID: Parameter August 07, 2015 SOIL PRECISIN 24 Hour RT 9G GERMANTOWN TP-5 Environmental Laboratories, Inc. 587 East Middle Turnpike, P.O.Box 370, Manchester, CT Tel. (860) Fax (860) Result FOR: Custody Information Collected by: Received by: Analyzed by: LB Laboratory Data Attn: Mr. Dan Nierenberg Precision Env. Services, Inc. 831 Route 67 Lot 38A Ballston Spa, NY see "By" below Date 07/30/15 07/31/15 Time 13:15 17:50 SDG ID: GBJ66838 Phoenix ID: BJ66841 RL/ PQL Units Dilution Date/Time By Reference Silver < mg/kg 1 08/04/15 LK SW6010C Arsenic mg/kg 1 08/04/15 LK SW6010C Beryllium mg/kg 1 08/04/15 LK SW6010C Cadmium < mg/kg 1 08/04/15 LK SW6010C Chromium mg/kg 1 08/04/15 LK SW6010C Copper mg/kg 1 08/04/15 LK SW6010C Mercury mg/kg 1 08/04/15 MA SW7471B Nickel mg/kg 1 08/04/15 LK SW6010C Lead mg/kg 1 08/04/15 LK SW6010C Antimony < mg/kg 1 08/04/15 LK SW6010C Selenium < mg/kg 1 08/04/15 LK SW6010C Thallium < mg/kg 1 08/04/15 LK SW6010C Trivalent Chromium mg/kg 1 08/07/15 KH Calculation Zinc mg/kg 1 08/04/15 LK SW6010C Percent Solid 84 % 07/31/15 I SW846-%Solid Chromium, Hexavalent < mg/kg 1 08/07/15 KH SW7196A ph - Soil ph Units 1 08/06/15 21:45 DH/KDB SW Redox Potential mv 1 08/06/15 DH/KDB SM2580B-09 1 Soil Extraction SVOA PAH Completed 08/03/15 JJ/VH SW3545A Mercury Digestion Completed 08/04/15 I/I SW7471B Total Metals Digest Completed 08/03/15 G/AG SW3050B Extraction of TPH SM Completed 08/03/15 BC/V SW3545A Gasoline Range Hydrocarbons (C6-C10) GRO (C6-C10) ND 9.0 mg/kg 50 08/04/15 LA SW8015D MOD 1 QA/QC Surrogates % 2,5-Dibromotoluene (FID) 87 % 50 08/04/15 LA % Page 8 of 10 Ver 1

28 Project ID: 4301 RT 9G GERMANTOWN Client ID: TP-5 Parameter TPH DRO (C10-C28) Result Phoenix I.D.: BJ66841 RL/ PQL Units Dilution Date/Time By Reference Diesel Range Organics (C10-C28) ND 58 mg/kg 1 08/05/15 JRB SW8015D DRO QA/QC Surrogates % n-pentacosane 88 % 1 08/05/15 JRB % Polynuclear Aromatic HC 2-Methylnaphthalene ND 270 ug/kg 1 08/04/15 E SW8270D Acenaphthene ND 270 ug/kg 1 08/04/15 E SW8270D Acenaphthylene ND 270 ug/kg 1 08/04/15 E SW8270D Anthracene ND 270 ug/kg 1 08/04/15 E SW8270D Benz(a)anthracene ND 270 ug/kg 1 08/04/15 E SW8270D Benzo(a)pyrene ND 270 ug/kg 1 08/04/15 E SW8270D Benzo(b)fluoranthene ND 270 ug/kg 1 08/04/15 E SW8270D Benzo(ghi)perylene ND 270 ug/kg 1 08/04/15 E SW8270D Benzo(k)fluoranthene ND 270 ug/kg 1 08/04/15 E SW8270D Chrysene ND 270 ug/kg 1 08/04/15 E SW8270D Dibenz(a,h)anthracene ND 270 ug/kg 1 08/04/15 E SW8270D Fluoranthene ND 270 ug/kg 1 08/04/15 E SW8270D Fluorene ND 270 ug/kg 1 08/04/15 E SW8270D Indeno(1,2,3-cd)pyrene ND 270 ug/kg 1 08/04/15 E SW8270D Naphthalene ND 270 ug/kg 1 08/04/15 E SW8270D Phenanthrene ND 270 ug/kg 1 08/04/15 E SW8270D Pyrene ND 270 ug/kg 1 08/04/15 E SW8270D QA/QC Surrogates % 2-Fluorobiphenyl 32 % 1 08/04/15 E % % Nitrobenzene-d5 29 % 1 08/04/15 E % 3 % Terphenyl-d14 40 % 1 08/04/15 E % Page 9 of 10 Ver 1