Texture Analysis in MSE
|
|
|
- Hannah Neal
- 5 years ago
- Views:
Transcription
1 Texture Analysis in MSE 집합조직제어연구실 서울대학교재료공학부
2 Texture (Preferred Orientation)
3 Similarity of Texture E.T?! 한쪽을쳐다보고있는사람들여러방향을쳐다보는 Randomly Preferred Oriented
4 What a Wonderful & Beautiful Life!
5 Scientific View for Life on Earth
6 Interaction between Sun & Earth Magnetic Field around Earth protects Earth from Sun!
7 Magnetic Field around Earth
8 What Magnetic Field Does?
9 Magnetic Field Configuration Inside Earth
10 Thermodynamic Condition Inside Earth
11 Phase Diagram Inside Earth Liquid fcc hcp
12 Magnetic Field due to hcp Iron Crystals Preferentially Oriented Single Crystal Size of Order of few Hundreds Km
13 Texture as A Necessary Condition for Life on Earth
14 Technical Overview of Texture Analysis
15 X-ray Configuration
16 EBSD Configuration EDS Detector Objective Lens CCD Camera Phosphor Screen Vanguard Detector Specimen Holder Motorized Stage Kikuchi pattern acquisition in SEM Crystal orientation identification in SEM
![1] [1 1 2] 19.47 O 22.00 O 20.5 O 16.](/docs-images/96/128971392/images/17-5.jpg "1 O [1 1 4] 15.78O 8.")
![18 O [1 3 4] [1 3 3] 13.26 O 19.](/docs-images/96/128971392/images/17-6.jpg "47 O 14.3 O 15.5 O 13.9 O 18.43 O 15.")
17 Orientation Measurement by EBSD Orientation Measurement JEOL 6500F FE-SEM + EDS + EBSD SEM Image Color Code for indexin Automatic Indexing Point Click for Pattern Orientation Mapping Orientation Information [1 1 1] [1 1 2] O O 20.5 O 16.1 O [1 1 4] 15.78O 8.18 O [1 3 4] [1 3 3] O O 14.3 O 15.5 O 13.9 O O O O [0 0 1] [0 1 3] [0 2 3] [0 1 1]
18 Fine Grained IF Steel Slab 열간압연 850 C 압하율 80% 냉간압연 페라이트의결정립미세화 (5 μm) 냉간압연 압하율 75% 30분열처리 냉간압연조직발달 {111}<110>, {001}<110> 재결정열처리 75 분열처리 650 C 60 분 <111>//ND 방위증가 결정립미세화에따라경도증가
19 Strip Casting : 4.5% Si Steel Disordered Texture Controlled Cold Rolled Strip Cast 1(11.62 ) 2(11.62 ) 3(27.23 ) 4(38.18 ) 5(42.10 ) 6(2.83 ) 7(59.36 ) 8(43.56 ) 9(50.49 ) 10(15.0 ) - High Angle Boundary - 냉간압연시균열발생 - Low Angle Boundary - 냉간압연가능
20 High Strength Gold Bonding Wire : EBSD 社 1.0mil(25.4μm) Wire 와이어표면부 와이어내부 용접부분거대결정립발달 M 社 Gold Bonding Wire
![60% : 260MPa [111] 90% :](/docs-images/96/128971392/images/21-3.jpg "280MPa [111]")
21 High Strength Gold Bonding Wire : Processing 개발된와이어의단면집합조직 와이어드로잉 공정개선전 공정개선후 [111] 60% : 260MPa [111] 90% : 280MPa [111] 집합조직의비율을높여고강도금본딩와이어제작공정개발
22 Electron Mobility in ELA & SMC Orientation Misorientation CSL 0.20 Total high Total angle high angle fraction Energy level Energy Level 0.12 LA 4µm Misorientation Fraction ELA SMC Mean Surface Energy MC 30µm - High angle & CSL - Energy ELA SMC Electron mobility ELA > SMC
23 HRTEM Analysis around Ti inclusion SEM Image (a) Ferrite TEM Image (b) A B Martensite 2µm Ti 2 O 3 (c) TiN (d) Ti 1µ m Ti 0.5µ m 1µ m O Mg Mn N Zone Axis [42-1] : Ti 2 O 3 Zone Axis [001] : TiN
24 Modern Scale of Texture nm µm mm HRTEM JEOL 3000F 300kV FEG TEM 0.17nm(0.1nm) Res. 극미세집합조직관찰 SEM/EBSD Opal/JSM μm Res. 미세조직 / 집합조직동시관찰 Pole figure Seifert 3000PTS 60kV, 80mA, 3.5kW 벌크재료집합조직
25 NOVA NanoLab (Full Configuration)
26 What are FIB Man doing Now?
27 Sample FIB Configuration SEM:Imaging Sample Plane FIB: Cutting EDS Cross Section SEM Column FIB SEM EDS Magnum Stage GIS Detector GIS
28 Schematic of Focused Ga Ion Beam (FIB) iquid Ga Metal Ceramic Base oom Temperature Operation Filament Support Pins hr Sources igh Vacuum Compatible arge Ion for Sputtering Filament Tip Secondary Electrons Secondary Ions (i + or i - ) or Neutral Atoms (n 0 )
29 FIB Configuration SEM SE GIS FIB EDS EBSD
30 Texture Analysis of Gold Bonding Wire Random Area Measurement Difficulties in Handling Many Sample Required Expected Area Measurement Easy Preparation FIB Can!
31 Cu Damascene : FIB Assisted EBSD Cu Electro-deposit 배선폭에따른재결정집합조직변화 Trench : 500/500nm 140nm Line 300nm Line Blanket ( ) over plated Cu electrodepo. Cu sputter-dep. Cu {111}<110> {111} Fiber FSG FSG LD LD TaN Si 3 N 4 Si wafer ND ND
32 3D- Reconstruction of Grain Orientation High Speed EBSD + FIB Auto Slice
33 REDS (Reprocessing of EBSD Data in SNU) FEM Graphics ODF(WIMV) BSD ystem Orientation Data Set Physics Montage Mosaic Analysis + + =
34 EBSD 장비운영 EBSD 활용및홈페이지운영 - 주요연구서비스 - 정기 EBSD Workshop 개최 -EBSD 장비를통한공동연구 연구기간내 EBSD 대내외활용현황 구분년도 2001 이전 상반기 계 건수 시료수 활용건수 이용자수 이용기관수 Ferrous Metal Non-Ferrous Metal Thin Film ( 상반기 )
35 Dimensional Material Analysis Scalable Analysis + Thermodynamic Analysis y 2D analysis EBSD, SEM UHV Chamber z 3D sectional analysis- FIB t 4DTEM x τ : Time with in-situ heating f : Environmental factor (Deformation, Coating)
36 Interactive Analysis System in SNU EBSD FE-SEM EDS FIB STM HR-EM TEM EDS HAADF Heating Low Energy Ion Milling UHV Chamber Deformation Coating Capable of Quasi in-situ Experiments!
37 Possible Example of FIB Related Analysis FIB I want to See this Area EBSD TEM
38 E Gold Bonding Wire Measured by U Texture Control Lab. FIB Sculpture for Fun chool of Materials Science and Engineering, Seoul National University. K Electron Co. Ltd, Kumeo-Li 316-2, Pogok-Myeon, Yongin-Si, Kyeonggi-Do.
39 Traditional Sculpture with FIB Jade Sculpture by J.W. Jang
40 현재계획 년 3월 NOVA 200 NanoLab 설치 년상반기시험운용운영방안 - 내부 : 교육과연구를통한보편화 - 외부 : 연구협력을통한운영 Education of Students through Challenging Research FIB Men 강석훈, 이상훈, More Students, FEI Members FIB FIB Operation Schedule 년장비의설치및안정화 서비스개시 년 1학기대학원특수문제연구 ( 집속이온공학 ) 개설 - 집속이온공학연구회모임추진
41 END
42 발표자료만드는법 1. One Page : One Content 2. One Line : One Statement 3. Not full statement : Abridged Words 4. Not Paragraph : Picture or Movie 5. Not Art Color : Simple Color 6. Not Equation : Final Equation
Focused Ion Beam CENTRE INTERDISCIPLINAIRE DE MICROSCOPIE ELECTRONIQUE. Marco Cantoni, EPFL-CIME CIME ASSEMBLEE GENERALE 2007
Focused Ion Beam @ CENTRE INTERDISCIPLINAIRE DE MICROSCOPIE ELECTRONIQUE Present situation and vision Marco Cantoni, EPFL-CIME Dual Beam Nova 600 Nanolab from FEI Company FE-SEM & FIB: Ga LMIS 4 Gas Injector
In-situ Heating Characterisation Using EBSD
Webinar In-situ Heating Characterisation Using EBSD Speakers Dr. Ali Gholinia Dr. Neil Othen Dr. Jenny Goulden Topics Introduction to EBSD Why do in-situ experiments? EBSD equipment requirements for in-situ
3D-EBSD an CrossBeam-Systemen
FIB- Workshop 3.-4. July 2008 3D-EBSD an CrossBeam-Systemen Ulrike Zeile 1, Ali Gholinia 2 and Frank Bauer 3 Arbeitskreis FIB SSOM DGM/DGE ASEM Hotel Seeburg, Luzern, Switzerland 1. Carl Zeiss NTS 2. Oxford
Supplementary Materials for
www.sciencemag.org/cgi/content/full/336/6084/1007/dc1 Supplementary Materials for Unidirectional Growth of Microbumps on (111)-Oriented and Nanotwinned Copper Hsiang-Yao Hsiao, Chien-Min Liu, Han-wen Lin,
EBSD Basics EBSD. Marco Cantoni 021/ Centre Interdisciplinaire de Microscopie Electronique CIME. Phosphor Screen. Pole piece.
EBSD Marco Cantoni 021/693.48.16 Centre Interdisciplinaire de Microscopie Electronique CIME EBSD Basics Quantitative, general microstructural characterization in the SEM Orientation measurements, phase
Observation in the GB (Gentle Beam) Capabilities
A field-emission cathode in the electron gun of a scanning electron microscope provides narrower probing beams at low as well as high electron energy, resulting in both improved spatial resolution and
Microtexture measurement of copper damascene line with EBSD
Material Science Forum Vols. 408-412(2002) pp. 529-534 2002 Trans Tech Publications, Switzerland Microtexture measurement of copper damascene line with EBSD Dong-Ik Kim 1*, Jong-Min Paik 1, Young-Chang
EBSD Electron BackScatter Diffraction Principle and Applications
EBSD Electron BackScatter Diffraction Principle and Applications Dr. Emmanuelle Boehm-Courjault EPFL STI IMX Laboratoire de Simulation des Matériaux LSMX emmanuelle.boehm@epfl.ch 1 Outline! Introduction!
Effect of titanium additions to low carbon, low manganese steels on sulphide precipitation
University of Wollongong Thesis Collections University of Wollongong Thesis Collection University of Wollongong Year 2008 Effect of titanium additions to low carbon, low manganese steels on sulphide precipitation
Specimen configuration
APPLICATIONNOTE Model 1040 NanoMill TEM specimen preparation system Specimen configuration Preparing focused ion beam (FIB) milled specimens for submission to Fischione Instruments. The Model 1040 NanoMill
John de Laeter Centre
John de Laeter Centre Major research infrastructure hub at Curtin University, Perth, W.A. ~$30M worth of microscopes, spectrometers, diffractometers and experimental facilities AuScope partner, Microscopy
Grain Contrast Imaging in UHV SLEEM
Materials Transactions, Vol. 51, No. 2 (2010) pp. 292 to 296 Special Issue on Development and Fabrication of Advanced Materials Assisted by Nanotechnology and Microanalysis #2010 The Japan Institute of
Cross sectional TEM analysis of duplex HIPIMS and DC magnetron sputtered Mo and W doped carbon coatings
Cross sectional TEM analysis of duplex HIPIMS and DC magnetron sputtered Mo and W doped carbon coatings SHARP, J, MULLER, I Castillo, MANDAL, P, ABBAS, A, WEST, G, RAINFORTH, W M, EHIASARIAN, Arutiun
Cross sectional TEM analysis of duplex HIPIMS and DC magnetron sputtered Mo and W doped carbon coatings
Cross sectional TEM analysis of duplex HIPIMS and DC magnetron sputtered Mo and W doped carbon coatings SHARP, J, MULLER, I Castillo, MANDAL, P, ABBAS, A, WEST, G, RAINFORTH, W M, EHIASARIAN, Arutiun and
Changes in Microstructure of Al/AlN Interface during Thermal Cycling
Materials Transactions, Vol. 49, No. 12 (2008) pp. 2808 to 2814 #2008 The Japan Institute of Metals Changes in Microstructure of / Interface during Thermal Cycling Yoshiyuki Nagatomo 1, Takeshi Kitahara
Specimen Preparation Technique for a Microstructure Analysis Using the Focused Ion Beam Process
Specimen Preparation Technique for a Microstructure Analysis Using the Focused Ion Beam Process by Kozue Yabusaki * and Hirokazu Sasaki * In recent years the FIB technique has been widely used for specimen
Introduction to Electron Backscattered Diffraction. TEQIP Workshop HREXRD Feb 1 st to Feb 5 th 2016
Introduction to Electron Backscattered Diffraction 1 TEQIP Workshop HREXRD Feb 1 st to Feb 5 th 2016 SE vs BSE 2 Ranges and interaction volumes 3 (1-2 m) http://www4.nau.edu/microanalysis/microprobe/interact-effects.html
Carnegie Mellon MRSEC
Carnegie Mellon MRSEC Texture, Microstructure & Anisotropy, Fall 2009 A.D. Rollett, P. Kalu 1 ELECTRONS SEM-based TEM-based Koseel ECP EBSD SADP Kikuchi Different types of microtexture techniques for obtaining
INVESTIGATION OF PHOSPHOROUS EFFECT ON THE FRACTURE TOUGHNESS OF HIGH STRENGTH SPRING STEELS BY INTEGRATED ELECTRON SPECTROSCOPY TECHNIQUES
INVESTIGATION OF PHOSPHOROUS EFFECT ON THE FRACTURE TOUGHNESS OF HIGH STRENGTH SPRING STEELS BY INTEGRATED ELECTRON SPECTROSCOPY TECHNIQUES M Jenko 1, V Leskovšek 1, B Senčič 2 and N Pukšič 1 1 Institute
A Quantitative Evaluation of Microstructure by Electron Back-Scattered Diffraction Pattern Quality Variations
Microsc. Microanal. 19, S5, 83 88, 2013 doi:10.1017/s1431927613012397 A Quantitative Evaluation of Microstructure by Electron Back-Scattered Diffraction Pattern Quality Variations SukHoonKang, 1 Hyung-Ha
Supporting information. In-situ TEM observation of phase transition of nanoscopic patterns on. baroplastic block copolymer film during nanoindentation
Supporting information In-situ TEM observation of phase transition of nanoscopic patterns on baroplastic block copolymer film during nanoindentation Ara Jo, Gil Ho Gu, Hong Chul Moon, Sung Hyun Han, Sang
In Situ Observation of Dislocation Nucleation and Escape in a Submicron Al Single Crystal
Supplementary Information for In Situ Observation of Dislocation Nucleation and Escape in a Submicron Al Single Crystal Sang Ho Oh*, Marc Legros, Daniel Kiener and Gerhard Dehm *To whom correspondence
Crystallographic Textures Measurement
Crystallographic Textures Measurement D. V. Subramanya Sarma Department of Metallurgical and Materials Engineering Indian Institute of Technology Madras E-mail: vsarma@iitm.ac.in Macrotexture through pole
Crystallographic Orientation Relationship between Discontinuous Precipitates and Matrix in Commercial AZ91 Mg Alloy
Materials Transactions, Vol. 52, No. 3 (2011) pp. 340 to 344 Special Issue on New Trends for Micro- and Nano Analyses by Transmission Electron Microscopy #2011 The Japan Institute of Metals Crystallographic
A NEW APPROACH TO STUDYING CAST CB2 STEEL USING SLOW AND VERY SLOW ELECTRONS
A NEW APPROACH TO STUDYING CAST CB2 STEEL USING SLOW AND VERY SLOW ELECTRONS Šárka Mikmeková 1 Josef Kasl 2 Dagmar Jandová 2 Ilona Müllerová 1 Luděk Frank 1 1 Institute of Scientific Instruments of the
NEMI Sn Whisker Modeling Group Part 2:Future Work
NEMI Sn Whisker Modeling Group Part 2:Future Work IPC/NEMI Meeting Maureen Williams, NIST Irina Boguslavsky, NEMI Consultant November 7, 2002 New Orleans, LA Capabilities of NEMI Modeling Group NEMI Fundamental
Electron channelling contrast imaging (ECCI) an amazing tool for observations of crystal lattice defects in bulk samples
Electron channelling contrast imaging (ECCI) an amazing tool for observations of crystal lattice defects in bulk samples Stefan Zaefferer with contributions of N. Elhami, (general & steels) Z. Li F. Ram,
Applications of EBSD
Applications of EBSD Dr. V. Subramanya Sarma Department of Metallurgical and Materials Engineering Indian Institute of Technology Madras E-mail: vsarma@iitm.ac.in Applications of EBSD Grain size distribution
Influence of Alloy Microstructure on Oxide Growth in HCM12A in Supercritical Water
Mater. Res. Soc. Symp. Proc. Vol. 1125 2009 Materials Research Society 1125-R06-05 Influence of Alloy Microstructure on Oxide Growth in HCM12A in Supercritical Water Jeremy Bischoff 1, Arthur T. Motta
Characterization of Cold Drawn Gold bonding Wire with EBSD
499 Material Science Forum Vols. 408-412(2002) pp. 499-504 2002 Trans Tech Publications, Switzerland Characterization of Cold Drawn Gold bonding Wire with EBSD Jae-Hyung Cho 1,2, J.S. Cho 3, J.T. Moon
Supplementary Information. Probing of 2 dimensional confinement-induced structural transitions in amorphous oxide thin film
Supplementary Information Probing of 2 dimensional confinement-induced structural transitions in amorphous oxide thin film Sung Keun Lee 1* and Chi Won Ahn 2 1School of Earth and Environmental Sciences,
SUPPLEMENTARY INFORMATIONS
SUPPLEMENTARY INFORMATIONS Dynamic Evolution of Conducting Nanofilament in Resistive Switching Memories Jui-Yuan Chen, Cheng-Lun Hsin,,, Chun-Wei Huang, Chung-Hua Chiu, Yu-Ting Huang, Su-Jien Lin, Wen-Wei
Development of bimodal grain structures in microalloyed steels:
Development of bimodal grain structures in microalloyed steels: Niobium and titanium are added to high strength low alloy (HSLA) steels to provide grain boundary pinning precipitates to help produce the
In situ TEM Characterization of Shear Stress-Induced Interlayer. Sliding in the Cross Section View of Molybdenum Disulfide
In situ TEM Characterization of Shear Stress-Induced Interlayer Sliding in the Cross Section View of Molybdenum Disulfide Juan Pablo Oviedo, Santosh KC, Ning Lu, Jinguo Wang, Kyeongjae Cho, Robert M. Wallace,
{001} Texture Map of AA5182 Aluminum Alloy for High Temperature Uniaxial Compression
Materials Transactions, Vol., No. (00) pp. 6 to 67 #00 The Japan Institute of Light Metals {00} Texture Map of AA8 Aluminum Alloy for High Temperature Uniaxial Compression Hyeon-Mook Jeong*, Kazuto Okayasu
METHOD FOR IMPROVING FIB PREPARED TEM SAMPLES BY VERY LOW ENERGY Ar + ION MILL POLISHING
METHOD FOR IMPROVING FIB PREPARED TEM SAMPLES BY VERY LOW ENERGY Ar + ION MILL POLISHING Yaron Kauffmann, Tzipi Cohen-Hyams, Michael Kalina, Hila Sadan-Meltzman and Wayne D. Kaplan Dept. of Materials Engineering
In-situ TEM Observation on Cu/MoOx Resistive Switching RAM
In-situ TEM Observation on Cu/MoOx Resistive Switching RAM * Masaki Kudo 1), Yuuki Ohno 2), Kouichi Hamada 3), Masashi Arita 4), and Yasuo Takahashi 5) 1), 2), 3), 4), 5) Graduate school of Information
Microstructural characterisation of as-deposited and reheated weld metal High Strength Steel Weld Metals
Microstructural characterisation of as-deposited and reheated weld metal High Strength Steel Weld Metals Enda Keehan, Leif Karlsson, Mattias Thuvander, Eva-Lena Bergquist Abstract ESAB AB, Gothenburg,
Diffraction Contrast Tomography. Unlocking Crystallographic Information from Laboratory X-ray Microscopy. Technical Note
Diffraction Contrast Tomography Unlocking Crystallographic Information from Laboratory X-ray Microscopy Technical Note Diffraction Contrast Tomography Unlocking Crystallographic Information from Laboratory
Dissimilar Metals Welding of Galvanized Steel and Aluminum
Transactions of JWRI, Vol.43 (04), No. Dissimilar Metals Welding of Galvanized Steel and Aluminum NISHIMOTO Koji*, KAWAHITO Yousuke** and KATAYAMA Seiji*** Abstract Dissimilar metals joints of galvanized
Supplementary Material
Supplementary Material Self-patterning Gd nano-fibers in Mg-Gd alloys Yangxin Li 1,2, Jian Wang 3, Kaiguo Chen 4, Meiyue Shao 2, Yao Shen 1 *, Li Jin 2 *, Guozhen Zhu 1 * 1 State Key Laboratory of Metal
Equilibria in Materials
2009 fall Advanced Physical Metallurgy Phase Equilibria in Materials 09.01.2009 Eun Soo Park Office: 33-316 Telephone: 880-7221 Email: espark@snu.ac.kr Office hours: by an appointment 1 Text: A. PRINCE,
Crystal structure of the material :- the manner in which atoms, ions, or molecules are spatially.
Crystal structure A crystalline material :- is one in which the atoms are situated in a repeating or periodic array over large atomic distances. Crystal structure of the material :- the manner in which
Chapter 3 Silicon Device Fabrication Technology
Chapter 3 Silicon Device Fabrication Technology Over 10 15 transistors (or 100,000 for every person in the world) are manufactured every year. VLSI (Very Large Scale Integration) ULSI (Ultra Large Scale
Visualization of Nano-precipitate in Low-alloy Steel by Using Energy-filtered Transmission Electron Microscopy
UDC 620. 186. 1 : 620. 187 Visualization of Nano-precipitate in Low-alloy Steel by Using Energy-filtered Transmission Electron Microscopy Yoichi IKEMATSU* 1 Genichi SHIGESATO* 1 Masaaki SUGIYAMA* 1 Abstract
Tutorial 2 : Crystalline Solid, Solidification, Crystal Defect and Diffusion
Tutorial 1 : Introduction and Atomic Bonding 1. Explain the difference between ionic and metallic bonding between atoms in engineering materials. 2. Show that the atomic packing factor for Face Centred
Nanostructuring 1 Billion Tons: Combining Rapid Alloy Prototyping, Multiscale Models, and Characterization for Advanced Manufacturing
Nanostructuring 1 Billion Tons: Combining Rapid Alloy Prototyping, Multiscale Models, and Characterization for Advanced Manufacturing D. Raabe, H. Springer, P. Eisenlohr, C. Tasan, I. Gutierrez, P. Choi,
Microstructures and dislocations in the stressed AZ91D magnesium alloys
Materials Science and Engineering A344 (2002) 279/287 www.elsevier.com/locate/msea Microstructures and dislocations in the stressed AZ91D magnesium alloys R.M. Wang a,b,, A. Eliezer a, E. Gutman a a Ben-Gurion
Electron Microscopy Studies of Niobium Thin Films on Copper
Electron Microscopy Studies of Niobium Thin Films on Copper Roy Crooks 1, Greg Thompson 2, Robb Morris 2, Michelle Adams Hughes 3, Daudi Waryoba 3, and Peter Kalu 3 1 Black Laboratories, L.L.C., Newport
Electric Flame-Off Characteristics and Fracture Properties of 20 m Thin Copper Bonding Wire
Materials Transactions, Vol. 5, No. 2 (29) pp. 293 to 298 #29 The Japan Institute of Metals Electric Flame-Off Characteristics and Fracture Properties of 2 m Thin Copper Bonding Wire Fei-Yi Hung 1; *,
Formation of texture and anisotropy of shape memory effect in Fe-Mn-Si-Co-Cr alloy
J. Phys. IVFrance 11 (200fc) Pr8-211 EDP Sciences, Les Ulis Formation of texture and anisotropy of shape memory effect in Fe-Mn-Si-Co-Cr alloy K.K. Jee, J.O. Song 1, W.Y. Jang 2, M.C. Shin and C.S. Choi
Study of the Initial Stage and an Anisotropic Growth of Oxide Layers Formed on Zircaloy-4
16 th International Symposium on Zirconium in the Nuclear Industry, Chengdu, P. R. China, May 10-13, 2010 Study of the Initial Stage and an Anisotropic Growth of Oxide Layers Formed on Zircaloy-4 B. X.
Transmission Electron Microscopy (TEM) Prof.Dr.Figen KAYA
Transmission Electron Microscopy (TEM) Prof.Dr.Figen KAYA Transmission Electron Microscope A transmission electron microscope, similar to a transmission light microscope, has the following components along
Chapter 8 Strain Hardening and Annealing
Chapter 8 Strain Hardening and Annealing This is a further application of our knowledge of plastic deformation and is an introduction to heat treatment. Part of this lecture is covered by Chapter 4 of
(51) Int Cl.: C22C 38/06 ( ) C22C 38/38 ( ) C21D 8/02 ( ) C21D 9/46 ( ) C23C 2/06 ( ) C23C 2/28 (2006.
(19) TEPZZ 99887A_T (11) EP 2 99 887 A1 (12) EUROPEAN PATENT APPLICATION published in accordance with Art. 13(4) EPC (43) Date of publication: 0.06.13 Bulletin 13/23 (21) Application number: 11811.2 (22)
Silver Diffusion Bonding and Layer Transfer of Lithium Niobate to Silicon
Chapter 5 Silver Diffusion Bonding and Layer Transfer of Lithium Niobate to Silicon 5.1 Introduction In this chapter, we discuss a method of metallic bonding between two deposited silver layers. A diffusion
Advances in Nano-Level Materials Characterization Technology
UDC 543. 5 Advances in Nano-Level Materials Characterization Technology Misao HASHIMOTO* 1 Abstract The recent development of nano-level materials analyses technologies such as three-dimensional atom probing
ASE324: Aerospace Materials Laboratory
ASE324: Aerospace Materials Laboratory Instructor: Rui Huang Dept of Aerospace Engineering and Engineering Mechanics The University of Texas at Austin Fall 2003 Lecture 3 September 4, 2003 Iron and Steels
AN EBSD STUDY OF THE MICRO STRUCTURAL DEVELOPMENT DURING ANNEALING OF A FOLDED SUPER DUPLEX STAINLESS STEEL SHEET SAMPLE.
AN EBSD STUDY OF THE MICRO STRUCTURAL DEVELOPMENT DURING ANNEALING OF A FOLDED SUPER DUPLEX STAINLESS STEEL SHEET SAMPLE. H S Ubhi 1), J R Saithala 2) and H Jiang 1) 1) Oxford Instruments, High Wycombe.
CHARACTERIZATION OF SILICON CARBIDE AND PYROCARBON COATINGS FOR FUEL PARTICLES FOR HIGH TEMPERATURE REACTORS (HTR)
CHARACTERIZATION OF SILICON CARBIDE AND PYROCARBON COATINGS FOR FUEL PARTICLES FOR HIGH TEMPERATURE REACTORS (HTR) D. Hélary 1,2, X. Bourrat 1, O. Dugne 2, G. Maveyraud 1,2, F. Charollais 3, M. Pérez 4,
3D Nano-analysis Technology for Preparing and Observing Highly Integrated and Scaled-down Devices in QTAT
Hitachi Review Vol. 54 (2005), No. 1 27 3D Nano-analysis Technology for Preparing and Observing Highly Integrated and Scaled-down Devices in QTAT Toshie Yaguchi Takeo Kamino Tsuyoshi Ohnishi Takahito Hashimoto
Evolution of Microstructure and Texture Associated with Ridging in Ferritic Stainless Steels
, pp. 100 105 Evolution of Microstructure and Texture Associated with Ridging in Ferritic Stainless Steels SooHo PARK, KwangYuk KIM, YongDeuk LEE and ChanGyung PARK 1) Stainless Steel Research Group, Technical
MEMS 487. Class 04, Feb. 13, K.J. Hemker
MEMS 487 Class 04, Feb. 13, 2003 Materials Come As:!Amorphous Glasses, polymers, some metal alloys Processing can result in amorphous structures! Crystalline Single crystals Textured crystals Polycrystalline
MICROSTRUCTURE CHARACTERIZATION OF GOES AFTER HOT ROLLING AND COLD ROLLING + DECARBURIZATION ANNEALING
MICROSTRUCTURE CHARACTERIZATION OF GOES AFTER HOT ROLLING AND COLD ROLLING + DECARBURIZATION ANNEALING Vlastimil VODÁREK 1, Jan HOLEŠINSKÝ 1, Anastasia MASLOVA 1, František FILUŠ 1, Šárka MIKLUŠOVÁ 2,
Previous Lecture. Vacuum & Plasma systems for. Dry etching
Previous Lecture Vacuum & Plasma systems for Dry etching Lecture 9: Evaporation & sputtering Objectives From this evaporation lecture you will learn: Evaporator system layout & parts Vapor pressure Crucible
STUDY & ANALYSIS OF ALUMINIUM FOIL AND ANATASE TITANIUM OXIDE (TiO2) USING TRANSMISSION ELECTRON MICROSCOPY
STUDY & ANALYSIS OF ALUMINIUM FOIL AND ANATASE TITANIUM OXIDE (TiO2) USING TRANSMISSION ELECTRON MICROSCOPY Ayush Garg Department of Chemical and Materials Engineering, University of Auckland, Auckland,
Ag 2 S: Fabrication and Characterization Techniques
2 2 S: Fabrication and Characterization Techniques This chapter describes two fabrication methods used for the growth of 2 S thin films. The specific growth parameters are presented for each method as
More Thin Film X-ray Scattering and X-ray Reflectivity
Stanford Synchrotron Radiation Laboratory More Thin Film X-ray Scattering and X-ray Reflectivity Mike Toney, SSRL 1. Introduction (real space reciprocal space) 2. Polycrystalline film (no texture) RuPt
CRYSTAL STRUCTURE DETERMINATION OF PHARMACEUTICALS WITH ELECTRON DIFFRACTION
CRYSTAL STRUCTURE DETERMINATION OF PHARMACEUTICALS WITH ELECTRON DIFFRACTION Dr. Partha Pratim Das Application Specialist, NanoMEGAS SPRL, Belgium pharma@nanomegas.com www.nanomegas.com This document was
Supplementary Figure S1 Crystal structure of the conducting filaments in sputtered SiO 2
Supplementary Figure S1 Crystal structure of the conducting filaments in sputtered SiO 2 based devices. (a) TEM image of the conducting filament in a SiO 2 based memory device used for SAED analysis. (b)
Evolution of Recrystallization Texture in Aluminum Alloy Sheets by Asymmetric-Warm-Rolling
技術論文 Evolution of Recrystallization Texture in Aluminum Alloy Sheets by Asymmetric-Warm-Rolling Yoshikazu Suzuki Osamu Noguchi Yoshiki Miki Yoichi Ueno Katsumi Koyama Toshio Komatsubara Abstract : Asymmetric-warm-rolling
Transzmissziós és pásztázó elektronmikroszkópos minták készítése ionsugaras vékonyítással
Transzmissziós és pásztázó elektronmikroszkópos minták készítése ionsugaras vékonyítással Radi Zsolt Technoorg Linda Kft., Budapest Oktatói és Doktorandusz Konferencia Visegrád, 2012 State-of-the-art materials
In-situ Electron Microscopy Mechanical Testing for Steels
Technical Report UDC 621. 385. 2 : 620. 17 : 669. 14 In-situ Electron Microscopy Mechanical Testing for Steels Shunsuke TANIGUCHI* Gerhard DEHM Abstract This paper outlines the techniques of in-situ electron
Additive manufacturing
Comparison Between Microstructures, Deformation Mechanisms and Micromechanical Properties of 316L Stainless Steel Consolidated by Laser Melting I. Heikkilä, O. Karlsson, D. Lindell, A. Angré, Y. Zhong,
The Study of SEM Examination of Crept Ceramic Samples Prepared by Cross Polishing Method
The Study of SEM Examination of Crept Ceramic Samples Prepared by Cross Polishing Method Alper Uludag Faculty of Aeronautics and Astronautics Anadolu University Eskisehir, Turkey alperuludag@anadolu.edu.tr
Microstructural Controls on Trace Element Variability in Ore Minerals
2 Microstructural Controls on Trace Element Variability in Ore Minerals Question: Does EBSD provide new insight into ore mineral microstructure and the chemical enrichment of elements in hydrothermal ore
MODEL SEM Mill. Two independently adjustable TrueFocus ion sources
MODEL 1060 SEM Mill A state-of-the-art ion milling and polishing system. It is compact, precise, and consistently produces high-quality scanning electron microscopy (SEM) samples for a wide variety of
Rapid Imaging of Microstructure using Spatially Resolved Acoustic Spectroscopy
Rapid Imaging of Microstructure using Spatially Resolved Acoustic Spectroscopy Steve Sharples, Matt Clark, Wenqi Li, Mike Somekh Applied Optics Group School of Electrical & Electronic Engineering University
atoms = 1.66 x g/amu
CHAPTER 2 Q1- How many grams are there in a one amu of a material? A1- In order to determine the number of grams in one amu of material, appropriate manipulation of the amu/atom, g/mol, and atom/mol relationships
Structural change during cold rolling of electrodeposited copper
Materials Science Forum Vols. 539-543 (2007) pp. 5013-5018 online at http://www.scientific.net (2007) Trans Tech Publications, Switzerland Structural change during cold rolling of electrodeposited copper
Application of Scanning Electron Microscope to Dislocation Imaging in Steel
Application of Scanning Electron Microscope to Dislocation Imaging in Steel Masaaki Sugiyama and Masateru Shibata Advanced Technology Research Laboratories, Nippon Steel Corporation SM Business Unit, JEOL
Supplementary. N. Akhtar a,b, M.Y. Emran a, M. A. Shenashen a,, T. Osaka b, A. Faheem c, T. Homma b, H. Kawarada. , S. A.
Electronic Supplementary Material (ESI) for Journal of Materials Chemistry B. This journal is The Royal Society of Chemistry 2017 Supplementary Fabrication of Photo-electrochemical biosensor for ultrasensitive
Ultra-high material-quality silicon pillars on glass. IEEE Photovoltaic Specialists Conference Conference Record. Copyright IEEE.
Title Ultra-high material-quality silicon pillars on glass Author(s) Liu, F; AI-Jassim, MM; Young, DL Citation The 35th IEEE Photovoltaic Specialists Conference (PVSC 2010), Honolulu, HI., 20-25 June 2010.
ORIENTATION DETERMINATION BY EBSP IN AN ENVIRONMENTAL SCANNING ELECTRON MICROSCOPE
Pergamon PII S1359-6462(99)00086-X Scripta Materialia, Vol. 41, No. 1, pp. 47 53, 1999 Elsevier Science Ltd Copyright 1999 Acta Metallurgica Inc. Printed in the USA. All rights reserved. 1359-6462/99/$
Development of New Generation Of Coatings with Strength-Ductility Relationship, Wear, Corrosion and Hydrogen Embrittlement Resistance Beyond the
Development of New Generation Of Coatings with Strength-Ductility Relationship, Wear, Corrosion and Hydrogen Embrittlement Resistance Beyond the Current Materials Accomplishments till date As the structural
LA-UR-01-3685 Approved for public release; distribution is unlimited. Title: USING A MULTI-DISCIPLINARY APPROACH, THE FIRST ELECTRON BACKSCATTERED KIKUCHI PATTERNS WERE CAPTURED FOR A PLUTONIUM ALLOY Author(s):
MME 2001 MATERIALS SCIENCE
MME 2001 MATERIALS SCIENCE 1 20.10.2015 crystal structures X tal structure Coord. # Atoms/ unit cell a=f(r) APF % SC 6 1 2R 52 BCC 8 2 4R/ 3 68 FCC 12 4 2R 2 74 HCP 12 6 2R 74 Theoretical Density, knowing
SUPPLEMENTARY INFORMATION
High Electrochemical Activity of the Oxide Phase in Model Ceria- and Ceria-Ni Composite Anodes William C. Chueh 1,, Yong Hao, WooChul Jung, Sossina M. Haile Materials Science, California Institute of Technology,
Deformation Microstructure and Texture in a Cold-Rolled Austenitic Steel with Low Stacking-Fault Energy
Materials Transactions, Vol. 51, No. 4 (2010) pp. 620 to 624 Special Issue on Crystallographic Orientation Distribution and Related Properties in Advanced Materials II #2010 The Japan Institute of Metals
Recrystallization textures in metals and alloys
Recrystallization textures in metals and alloys Uniaxial deformation Aluminium wire F.C.C. Metals and alloys FCC wires retain deformation texture ([111]+[100]) upon recrystallisation Composition / Purity
Applications of Energy-Assistance to the formation of novel surface coatings
Innovation Into Success; The quarterly Journal of the UK Science Park Association Issue No 17 Spring 2015 p65-8 (www.scienceparks.co.uk) Applications of Energy-Assistance to the formation of novel surface
SUPERFICIAL DEFECTS ON AISI 1118 STEEL PLATES
SUPERFICIAL DEFECTS ON AISI 1118 STEEL PLATES A.T.DUMITRESCU, A.CATANGIU University Valahia Targoviste Email: atdumitrescu@gmail.com, acatangiu@yahoo.co.uk Abstract: Even in the case of well established
Model Plasma Cleaner. Effectively cleans specimens for electron microscopy EXCELLENCE MAGNIFIED
Model 1020 Plasma Cleaner Effectively cleans specimens for electron microscopy EXCELLENCE MAGNIFIED Model 1020 Plasma Cleaner Simultaneously cleans specimen and specimen holder. Cleans highly contaminated
Stacking fault energy measurements in modified Cantor alloys
Stacking fault energy measurements in modified Cantor alloys C. Reinhart Ruhr-Universität Bochum 14 February 2018 14.02.2018 1/17 (a) Full dislocation with Burgers Vector b of type ½ (b) Beginning
Microstructure Analysis by Means of the Orthogonallyarranged
Hitachi Review Vol. 65 (2016), No. 7 201 Special Contributions Microstructure Analysis by Means of the Orthogonallyarranged FIB-SEM Toru Hara, Dr. Eng. OVERVIEW: Serial sectioning using a combined FIB
Effect of barrier layers on the texture and microstructure of Copper films
Mat. Res. Soc. Symp. Proc. Vol. 766 2003 Materials Research Society E2.2.1 Effect of barrier layers on the texture and microstructure of Copper films Tejodher Muppidi and David P Field School of MME, Washington
Growth of monocrystalline In 2 O 3 nanowires by seed orientation dependent vapour-solid-solid mechanism
Electronic Supplementary Material (ESI) for Journal of Materials Chemistry C. This journal is The Royal Society of Chemistry 2014 Electronic Supplementary Information (ESI) Growth of monocrystalline In
ME 254 MATERIALS ENGINEERING 1 st Semester 1431/ rd Mid-Term Exam (1 hr)
1 st Semester 1431/1432 3 rd Mid-Term Exam (1 hr) Question 1 a) Answer the following: 1. Do all metals have the same slip system? Why or why not? 2. For each of edge, screw and mixed dislocations, cite
Relation Between Internal Stress and Surface Roughness of Titanium Nitride Films Deposited by HCD Ion Plating
No.22,28 65 Relation Between Internal Stress and Surface Roughness of Titanium Nitride Films Deposited by HCD Ion Plating Itsuo Ishigami Ken-ichi Miura Hideaki Hoshino Tomoyuki Mizukoshi (28 6 17 ) An
Packing of atoms in solids
MME131: Lecture 6 Packing of atoms in solids A. K. M. B. Rashid Professor, Department of MME BUET, Dhaka Today s topics Atomic arrangements in solids Points, directions and planes in unit cell References: