STANDARD OPERATING PROCEDURE INDEX
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1 CHEMTECH DOC CONTROL QAM--24 Quality Assurance 24 06/07/ /10/2013 Manual CHEMTECH DOC CONTROL Chemical Hygiene Plan-09 Chemical Hygiene Plan 9 05/19/ /30/2011 CHEMTECH DOC CONTROL Conflict of Interest Plan--7 Conflict of Interest 7 02/17/ /17/2014 CHEMTECH DOC CONTROL Affirmative Action Program Affirmative Action Plan 2 05/19/ /20/2010 Executive CHEMTECH DOC CONTROL AAP Section 503 and AAP for Disabilities 1 05/19/ /06/2009 and Veterans Extractions-NJ MSOM01.2-Sample Prep-02 Sample Preparation by 2 05/29/ /26/2007 USEPA SOM01.2 Extractions-NJ M3541-ASE Extraction-06 Extraction by Auto 6 02/10/ /25/2013 Soxhlet by method 3541 Extractions-NJ M3520C-Pest-PCB Liquid-Liquid M3520C-Pest-PCB 4 05/29/ /25/2011 extraction-04 Liquid-Liquid Extractions-NJ M3545A-Pressurized Fluid Pressurized Fluid 7 02/10/ /26/2013 Extraction-07 Extraction by 3545 Extractions-NJ M3510C,3580A-Extraction 8270 Extraction SOP 14 02/04/ /25/2014 SVOC-14 Extractions-NJ M3510C,3580A-Extraction DRO DRO Extraction SOP 7 05/29/ /23/2012 Extractions-NJ M3510C,3580A-Extraction PCB PCB Extraction SOP 10 03/27/ /31/2014 Extractions-NJ M3510C,3580A-Extraction PCB PCB Extraction SOP 10 03/27/ /25/ Extractions-NJ M3610-Alumina cln up-04 Alumina clean up by SW 4 02/10/ /04/ method 3610 Extractions-NJ M3620C-Florisil cleanup-05 Florisil clean up by 5 02/10/ /26/2013 method 3620 Extractions-NJ M3630C-Silica Gel CleanUp-05 Silica Gel Clean Up by 5 02/10/ /26/2013 method 3630 Extractions-NJ M3640A-GPC cleanup-05 GPC clean up by method 5 02/10/ /26/ Extractions-NJ M3660B-Sulfur Cleanup-05 Sulfur Clean Up by 5 02/10/ /26/2013 method 3660 Extractions-NJ M3665A-Sulfuric Acid Cleanup- Sulfuric Acid clean up 6 02/04/ /26/ by method 3665 Extractions-NJ O19-White Phosphorus So-3 White phosphorus solid 3 06/11/ /14/2013 extraction by SW3550B Extractions-NJ O20-White Phosphorus Water White phosphorus 2 06/11/ /08/2012 aqueous extraction by Extractions-NJ P.1-V1 Biological Tissue 1 05/29/ /06/2011 homogenization Extractions-NJ P.5-V1 Percent lipid 1 05/29/ /06/2011 determination in Extractions-NJ Chemtech Pore Water-Elutriate Pore Water - Elutriate 1 06/11/ /30/2012 Generation for Sediments-01 Water Generation from Extractions-NJ M3535A-HPLC Explosives 3535A Extraction for 2 05/29/ /30/2009 Preparation Explosives Extractions-NJ M8330-A-Explosives Salting 8330 Explosives 2 05/29/ /30/2009 Preparation Salting-out Extraction Extractions-NJ G.21-1 General Laboratory 1 08/22/ /20/2010 Multi Incremental Field Methods M4020-PCB Inmmunoassay-04 Screening procedure for 4 06/18/ /26/2007 PCB by Inmmunoassay per Field Methods M3815-Field GC-03 Volatile Organic 3 06/18/ /29/2005 screening on solid by GC VOA-NJ MRSK Gases by RSK /24/ /30/2013 GC VOA-NJ M8015-GRO GRO 14 10/24/ /28/2013 GCMS SVOC-NJ M625-SM6410B-BNA BNA waste water 11 05/19/ /20/2014 GCMS SVOC-NJ M8270C-D-BNA BNA 19 05/19/ /20/2014 Page 1 of 7
2 GCMS SVOC-NJ M8330A-Nitroaromatics 8330A Analysis for 11 03/25/ /29/2013 Nitroaromatic and GCMS SVOC-NJ M.5-White Phosphorus by GC-3 White phosphorus by 3 06/11/ /14/2013 SW8270-Modified GCMS SVOC-NJ MSOM01.2-SVOC-03 Determination of 3 03/25/ /29/2013 extractable SIM/SVOC GCMS SVOC-NJ L.2-V-3 Nitroaromatic and 3 06/12/ /14/2013 Nitramine Explosives by General Chem-NJ MISM01.2-Cyanide-04 Total cyanide 4 03/12/ /25/2013 by Method ISM01.2 General Chem-NJ MWBTOC-01 Total Organic Carbon in 1 01/24/ /21/2013 Soil by Walkley-Black General Chem-NJ J.21-3 Nitrocellulose 3 07/19/ /22/2013 Extraction From Soil General Chem-NJ MSM2520B-Salinity-03 Determination of 3 03/12/ /25/2013 salinity using SM2520B General Chem-NJ MSM4500-KMnO4 Potassium Determination of 2 03/12/ /25/2013 permanganate-02 Potassium permanganate General Chem-NJ MLOI-Loss on Ignition-02 Loss on Ignition by 2 03/12/ /25/2013 Chemtech SOP General Chem-NJ MISM01.3-Cyanide-02 Total cyanide 2 03/12/ /25/2013 by Method ISM01.3 General Chem-NJ MSM2150B-Odor-05 Determination of Odor 5 02/27/ /15/2013 General Chem-NJ MSM2320B-Alkalinity-10 Determination of 10 02/27/ /15/2014 Alkalinity by 2320B General Chem-NJ MSM5220D-COD-12 COD by method SM 5220D 12 02/27/ /15/2014 General Chem-NJ MSM4500HB-pH-07 ph by method 4500 H B 7 02/27/ /15/2013 General Chem-NJ MSM5540C-MBAS--8 MBAS 8 02/27/ /15/2014 General Chem-NJ M9041A-pH-06 ph by method SW /27/ /15/2013 General Chem-NJ M9056-A-Inorganic Anions-10 Inorganics Anions by 10 03/21/ /25/2014 method 9056 General Chem-NJ M9065-Phenolics--9 Phenols by /19/ /25/2014 General Chem-NJ M9071B-Oil & Grease-10 Oil & Grease by method 10 02/27/ /15/2013 SW General Chem-NJ M9080-Cation Exchange-04 Cation Exchange by 4 02/27/ /15/2013 method 9080 General Chem-NJ M9081-Cation Exchange-04 Cation Exchange by 4 02/27/ /15/2013 SW General Chem-NJ M9095A-B-Free liquids-07 Free liquid by method 7 02/27/ /15/2013 SW General Chem-NJ M-percent solids-07 Percent Solids by 7 03/12/ /25/2013 Chemtech SOP General Chem-NJ M1312-SPLP-06 SPLP extration by 6 02/27/ /15/2013 method 1312 General Chem-NJ M1664A-O&G-NPM-10 Oil & Grease 10 02/27/ /15/2013 by method 1664 General Chem-NJ MSM4500-NH3 B,G,H-Ammonia-121 Ammonia /19/ /25/2014 General Chem-NJ M9012A-B-Total, Amenable and Cyanide by 14 02/04/ /07/2014 Reactive Cyanide-14 method 9012 using General Chem-NJ M9030B-Sulfide-07 Sulfide distillation by 7 02/27/ /15/2013 method 9030 General Chem-NJ M9050-Conductivity-05 Specific Conductance by 5 03/12/ /25/2013 method 9050 General Chem-NJ M1010-A-Flash Point Flash point Closed 10 01/14/ /15/2014 Cup General Chem-NJ M1110-Corrosivity Corrosivity 5 02/14/ /15/2013 General Chem-NJ M1311-TCLP TCLP Extraction procedure 8 07/22/ /23/2013 Page 2 of 7
3 General Chem-NJ MSM2540B &160.4,SM2540G- Total Residue and Total 11 02/14/ /15/2013 TS&T&VS-11 & Fixed, Volatile General Chem-NJ M180.1 Turbidity-11 Turbidity Analysis by 11 02/14/ /15/2013 method General Chem-NJ M300.0-Inorganic Anions Inorganic Anion 14 03/19/ /25/2014 General Chem-NJ M3060A,7196A-Hex.Chromium-18 M3060,7196-Hex /13/ /14/2013 Chromium General Chem-NJ MSM3500-Cr B- Hex. Chromium Hexavelent 10 02/14/ /17/2014 Chromium General Chem-NJ M365.3&SM4500-P E,B-13 Phosphorus 13 02/26/ /15/2014 General Chem-NJ MSM5210B-BOD-CBOD--9 SM5210 BOD and CBOD 9 02/26/ /15/2014 General Chem-NJ MSM4500-Cl G-08 SM 4500 Residual 8 12/20/ /07/2012 Chlorine General Chem-NJ MSM4500 SO4 E--9 SM 4500 E Sulfate 9 02/26/ /04/2014 General Chem-NJ M9010C-Total, Amenable and 9010 Total Cyanide 14 02/26/ /15/2014 Reactive Cyanide-14 General Chem-NJ M9040B,C-pH pH 9 02/26/ /15/2013 General Chem-NJ M9045C,D-pH ph 9 02/26/ /15/2013 General Chem-NJ M9060-A-TOC TOC 16 09/11/ /14/2013 General Chem-NJ M-AVS--5 Acid volatile 5 07/19/ /22/2013 General Chem-NJ M-Lloyd Kahn--6 Lloyd Kahn- TOC 6 02/14/ /17/2014 General Chem-NJ MSM5310B-TOC--8 Total Organic Carbon by 8 03/19/ /25/2014 SM5310B General Chem-NJ M9014-Reactive Cyanide-07 Determination of 7 03/12/ /25/2013 Reactive Cyanide General Chem-NJ MSM4500 CO2 C-Carbon Carbon Dioxide in water 2 03/12/ /25/2013 Dioxide-02 and General Chem-NJ MHACH8146-Ferrous Iron--4 Determination of 4 03/20/ /25/2014 Ferrous Iron by Method General Chem-NJ MHACH8110-Formaldehyde-03 Determination of 3 03/12/ /25/2013 Formaldehyde using General Chem-NJ MD1498-Redox Potential-04 Determination of 4 05/20/ /15/2013 oxidation-reduction General Chem-NJ M-percent solids-04 () Percent solids for 4 03/12/ /25/2013 General Chem-NJ MASTM D Acidity-03 Acidity in water and 3 05/20/ /25/2013 General Chem-NJ MSM2130B-Turbidity--6 Turbidity in water and 6 02/26/ /25/2014 General Chem-NJ MSM2510B-Conductivity-06 Specific Conductance 6 03/27/ /25/2013 General Chem-NJ MSM2540C-Total Dissolved TDS in water and 6 03/20/ /25/2014 Solids--6 General Chem-NJ MSM2540D-Total Suspended SS in water and 5 03/25/ /28/2014 Solids--5 General Chem-NJ MSM2540F-Settleable Solids-04 Settleable solids in 4 03/12/ /25/2013 water and General Chem-NJ MSM2550B-Temperature-05 Determination of 5 03/12/ /25/2013 Temperature General Chem-NJ MSM4500 Cl-C E-Chloride-05 Chloride 5 03/12/ /25/2013 General Chem-NJ MSM4500-CN C,E-Cyanide--6 Total cyanide in water 6 03/20/ /25/2014 and General Chem-NJ MSM4500-CN C,G-Amenable Total Amenable cyanide 7 03/20/ /25/2014 Cyanide--7 General Chem-NJ MSM4500-O C-Dissolved Oxygen-06 Dissolved oxygen 6 03/12/ /25/2013 Page 3 of 7
4 General Chem-NJ MSM4500-O G-Dissolved Dissolved oxygen 6 03/12/ /25/2013 Oxygen-06 General Chem-NJ MSM4500-SO3 B-Sulfite--6 Sulfite 6 03/20/ /25/2014 General Chem-NJ MSM4500-NO2 B-Nitrite--6 Nitrite 6 03/20/ /25/2014 General Chem-NJ MSM4500-N Org BorC-TKN--6 Total Kjeldahl Nitrogen 6 03/20/ /25/2014 General Chem-NJ M9013-Cyanide Distillation--7 Distillation of Soluble 7 03/20/ /25/2014 Cyanide General Chem-NJ M9031-Sulfide-05 Distillation of soluble 5 03/12/ /25/2013 sulfides General Chem-NJ MSM2120B-Color--7 Color by method 2120B 7 02/27/ /15/2014 General Chem-NJ M420.1-Phenolics--8 Phenols by EPA /20/ /25/2014 General Chem-NJ M9038-Sulfate--6 Determination of 6 03/20/ /25/2014 Sulfate in waste and General Chem-NJ MILM5.4CN-Cyanide-07 Cyanide 7 03/12/ /25/2013 General Chem-NJ M120.1-Conductivity--4 Specific Conductance 4 05/19/ /24/2013 General Chem-NJ M1030-Ignitability-08 Ignitability by method 8 02/27/ /15/2013 SW General Chem-NJ M9034-SM4500 S F-Sulfide-10 Sulfide by 10 03/20/ /25/2014 method 9034 Metals-NJ M200.8-Trace Elements-13 Trace Metals 13 03/28/ /31/2014 by ICPMS by method Metals-NJ M200.7-SM3120B-Trace Metals Analysis by 13 04/10/ /14/2014 Elements Metals-NJ M3005A-Digestion-08 Water Digestion by 8 02/28/ /04/2013 method SW Metals-NJ MILM5.4HGS-Mercury in Soil-05 Mercury in Soil by 5 02/28/ /25/2013 Metals-NJ MILM5.4HGW-Mercury in Water-06 Mercury in Water by 6 02/28/ /25/2013 Metals-NJ M-Metals ICPMS-09 ICP MS Metals by 9 02/28/ /25/2013 Metals-NJ M-Trace Metals-07 ICP Trace Metals by 7 02/28/ /25/2013 Metals-NJ M A-Metals ICPMS-17 Trace Metals 17 03/28/ /31/2014 by 6020 ICPMS Metals-NJ M6010-SM2340B-Hardness--3 Total Hardness by EPA 3 04/10/ /14/2014 Method 6010 and SM2340B Metals-NJ MPM-10-Digestion-02 Acid Digestion of Air 2 02/28/ /04/2013 Filters for Total Metals-NJ M7470A-Mercury Mercury 14 01/15/ /17/2014 Metals-NJ M B-Hardness--7 M B-Hardness 7 04/10/ /14/2014 Metals-NJ M7471A-B-Mercury A Mercury 13 01/15/ /17/2014 Metals-NJ M6010B-C-Trace elements-20 Trace elements by 20 03/28/ /31/2014 method SW B Metals-NJ M245.1-SM3112B-Mercury-12 Determination of 12 01/15/ /17/2014 Mercury by Metals-NJ M3050B-Digestion-15 Digestion method by 15 03/28/ /31/ Metals-NJ M3010A-Digestion Water Metals 12 03/28/ /31/2014 Digestion Metals-NJ MISM01.3-Mercury in Water-02 Mercury in 2 02/28/ /25/2013 water by cold vapor Metals-NJ MISM01.3-Mercury in soil-02 Mercury in 2 02/28/ /25/2013 soil by cold vapor Metals-NJ MISM01.3-Trace Metals-02 ICP AES by ISM /28/ /25/2013 Page 4 of 7
5 Metals-NJ MISM01.3-Metals ICPMS--3 Trace Elemental 3 02/28/ /07/2014 by ICP-MS Metals-NJ MISM01.2-Trace Metals--1 ICP-AES by Method 1 05/19/ /17/2011 ISM01.2 Metals-NJ MISM01.2-Metals ICPMS--2 Trace elemental 2 05/19/ /01/1900 by ICP-MS Metals-NJ MISM01.2-Mercury in Water-01 Mercury in 1 05/19/ /19/2011 water by cold vapor Metals-NJ MISM01.2-Mercury in Soil--2 Mercury in 2 05/19/ /30/2012 soil by cold vapor Metals-NJ P.3--1 Biological tissue 1 05/16/ /02/2011 digestion procedure for Pesticides-NJ MOQA-QAM-025-TPH--5 TPH by method 5 03/04/ /14/2014 OQA-QAM-025 Pesticides-NJ MNJDEP-EPH--3 Determination of 3 03/04/ /21/2014 extractable TPH by Pesticides-NJ MSOM01.2-PCB-04 Determination of 4 03/24/ /22/2013 Aroclors by GC/ECD by Pesticides-NJ MSOM01.2-Pesticide-04 Determination of 4 03/04/ /22/2013 Pesticide by GC/ECD by Pesticides-NJ M EDB&DBCP by GC-3 Determination of EDB 3 09/12/ /12/2013 and DBCP in Water by Pesticides-NJ M608-Pesticide PCB Pesticide-PCB 10 03/24/ /25/2014 Pesticides-NJ M8015B-C-DRO DRO Analysis 16 03/17/ /21/2014 Pesticides-NJ M8081A-B-Pesticide Pesticide 16 03/24/ /25/2014 Pesticides-NJ M A-PCB PCB 14 03/18/ /25/2014 Pesticides-NJ M8151A-Herbicide Herbicide 15 03/26/ /21/2013 Pesticides-NJ M8015B-Fingerprint--4 SOP for Fingerprint 4 02/11/ /28/2014 Pesticides-NJ MOLC03.2-Pesticide-PCB-04 Pest/PCB by 4 03/04/ /14/2013 method OLC03.2 Procedural-NJ P229-Computer Security and Computer Security and 8 12/10/ /11/2013 Backup--8 Backup Procedural-NJ P230-Sample Aliquot-04 Sample Aliquot prep 4 06/03/ /15/2006 Procedural-NJ P231-Data Archive-07 Data Archive procedures 7 06/11/ /15/2010 Procedural-NJ P232-Data Storage-08 Electronic Data Storage 8 05/19/ /26/2012 Procedural-NJ P224-Bottle Prep-05 Sampling container Prep 5 01/15/ /14/2012 sop Procedural-NJ P204-COC Procedure--7 Chain of Custody 7 07/17/ /19/2013 Procedural-NJ P228-Storage and Disposal of Storage and Disposal 5 08/01/ /16/2013 PCBs--5 procedures for PCBs Procedural-NJ P236-fax procedure-03 Fax procedure 3 03/04/ /18/2006 Procedural-NJ P235-Worklist--4 Worklist 4 07/19/ /22/2013 Procedural-NJ P234-Field Sampling--3 P234-Field Sampling /19/ /24/2013 Procedural-NJ P241-Air Canister Cleanup-05 Air Canister Cleanup 5 05/21/ /30/2009 Procedure Procedural-NJ P251-Quotation Project Project Chronicle SOP 4 05/19/ /06/2012 Chronicle-04 Procedural-NJ P243-Manual Integration Policy Manual Integration 6 07/16/ /25/2011 and Electronic Logbook-06 Policy Procedural-NJ P244-Calibration Policy--7 Calibration Policy 7 03/04/ /04/2014 Procedural-NJ P237-Training-06 Training SOP 6 05/19/ /22/2012 Page 5 of 7
6 Procedural-NJ P238-Field Chlorine test-01 Chlorine test by field 1 05/21/ /22/2004 kit Procedural-NJ P257-Foreign Soil--2 Sample Receiving, 2 11/15/ /18/2013 Handling and Disposal Procedural-NJ P255-Maintenance-03 Maintenance for 3 03/04/ /25/2013 equipment Procedural-NJ P254-Purchasing and supplies- Purchasing and supplies 4 07/11/ /11/ Procedural-NJ P256-Storage blank-02 Storage blank 2 03/04/ /15/2009 Procedural-NJ P252-Ethics Policy-01 Ethics Policy 1 01/06/ /21/2013 Procedural-NJ P253-Uncertainty Policy--2 Uncertainty Policy 2 05/19/ /05/2007 Procedural-NJ P201-Data --17 Data 17 05/21/ /14/2013 Procedural-NJ P202-Reagent Check-06 Reagent Check 6 07/12/ /18/2013 Procedural-NJ P203-Laboratory limits and Laboratory limits 14 12/20/ /12/2012 demonstration of capability-14 Procedural-NJ P205-Chemical Waste Disposal- Waste Disposal 9 03/11/ /12/ Procedural-NJ P207-ASTM Type II Water--5 ASTM Type II Water 5 05/17/ /31/2008 Procedural-NJ P208-Thermometer Thermometer Calibration 8 06/11/ /15/2010 Calibration-08 Procedural-NJ P209-Scale Calibration-07 Scale Calibration 7 01/08/ /01/1900 Procedural-NJ P210-Corrective-Preventive Corrective Action 10 01/06/ /13/2014 Action-10 Report Procedural-NJ P211-Control Charts-08 Control Charts 8 09/17/ /17/2013 Procedural-NJ P212-Water Purity--6 Water Purity 6 05/17/ /18/2013 Procedural-NJ P213-Calibration of Auto Calibration of Auto 6 07/12/ /31/2008 Pipettes-06 Pipettes Procedural-NJ P214-Subcontracting--9 Subcontracting 9 12/10/ /11/2013 Procedural-NJ P215-Hood Calibration--5 Hood Calibration 5 07/12/ /31/2008 Procedural-NJ P216-Calibration and Calibration and 6 07/12/ /31/2008 Temperature Setting-06 Temperature Setting Procedural-NJ P217-Glassware Cleaning-08 Glassware Cleaning 8 01/06/ /18/2011 Procedural-NJ P218-Chemical Storage-06 Chemical Storage 6 01/29/ /31/2008 Procedural-NJ P219-Disposal of Chemicals--6 Disposal of Chemicals 6 05/19/ /30/2011 Procedural-NJ P220-Traceability--8 Traceability 8 05/19/ /30/2012 Procedural-NJ P222-Standard Operating Standard Operating 7 08/12/ /18/2011 Procedures Prep-07 Procedures Prep Procedural-NJ P225-Rules for Rounding--7 Rules for Rounding 7 05/19/ /30/2011 Procedural-NJ P223-Material Safety Data and Material Safety Data 5 08/12/ /31/2008 Records--5 and Records Procedural-NJ P226-Corrections-07 Corrections 7 03/12/ /20/2012 Procedural-NJ P227-Services and Daily Services and 6 06/11/ /31/2008 Maintenance--6 Maintenance Procedural-NJ P250-Log-in Procedure-18 Log-in Procedure 18 03/27/ /31/2014 VOC-NJ M524.2-DWVOA-11 SOP rev. 4 VOC-NJ M624-SM6210B-MSVOA Waste Water VOA 11 03/25/ /20/ /15/ /17/2014 Page 6 of 7
7 VOC-NJ M8260B-C-SWGCMSVOA-19 Volatile Organics by method 8260 VOC-NJ MSOM01.2-GCMS VOA-03 Low/Medium Volatile Analysis by CLP SOM01.2 VOC-NJ MSOM01.2-GCMS VOA Trace and Trace and SIM Volatile SIM-03 Analysis by CLP SOM01.2 VOC-NJ MTO-15-Air VOC--9 Volatile Organic compounds in Air by 19 03/25/ /01/ /25/ /01/ /25/ /04/ /19/ /13/2013 Page 7 of 7
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