Test Report No. F690101/LF-CTSAYAA

Transcription

1 Test Report No. F690101/LF-CTSAYAA Page 1 of 1 SAMSUNG ELECTRO-MECHANICS CO., LTD. 10 Maeyoung-ro, Yeoungtong-gu Suwon-si, Gyeonggi-do Korea The following sample(s) was/were submitted and identified by/on behalf of the client as:- SGS File No. Product Name : AYAA : MLCC A(XR) J(JIS-B) X(X6S) TYPE Item No./Part No. : N/A Received Date : Test Period : Test Comments to : By the applicant's specific request, the sampling and testing was performed only for the part indicated in the photo without disassembly. Test Results : For further details, please refer to following page(s) SGS Korea Co., Ltd. Jeff Jang / Chemical Lab Mgr t +82 (0) f +82 (0)

2 Test Report No. F690101/LF-CTSAYAA Page 2 of 1 Sample No. : AYAA Sample Description : MLCC A(XR) J(JIS-B) X(X6S) TYPE Item No./Part No. : N/A Materials : N/A Heavy Metals Antimony (Sb) With reference to EPA 302(1996), US EPA 6010B(1996), ICP 10 Arsenic (As) With reference to EPA 302(1996), US EPA 6010B(1996), ICP 10 Beryllium (Be) With reference to EPA 302(1996), US EPA 6010B(1996), ICP Cadmium (Cd) With reference to IEC :2013 (Determination of Cadmium by ICP-OES) 0. Lead (Pb) With reference to IEC :2013 (Determination of Lead by ICP-OES) Mercury (Hg) With reference to IEC :2013 (Determination of Mercury by ICP-OES) 2 Hexavalent Chromium (Cr VI)* With reference to IEC :2017, determination of Hexavalent Chromium by Colorimetric Method using UV-Vis and/or with reference to IEC :2013, determination of Chromium by ICP-OES. 8 Flame Retardants-PBBs/PBDEs Monobromobiphenyl With reference to IEC :201 Dibromobiphenyl With reference to IEC :201 Tribromobiphenyl With reference to IEC :201 Tetrabromobiphenyl With reference to IEC :201 Pentabromobiphenyl With reference to IEC :201 Hexabromobiphenyl With reference to IEC :201 Heptabromobiphenyl With reference to IEC :201 Octabromobiphenyl With reference to IEC :201 Nonabromobiphenyl With reference to IEC :201 t +82 (0) f +82 (0)

3 Test Report No. F690101/LF-CTSAYAA Page 3 of 1 Sample No. : AYAA Sample Description : MLCC A(XR) J(JIS-B) X(X6S) TYPE Item No./Part No. : N/A Materials : N/A Flame Retardants-PBBs/PBDEs Decabromobiphenyl With reference to IEC :201 Monobromodiphenyl ether With reference to IEC :201 Dibromodiphenyl ether With reference to IEC :201 Tribromodiphenyl ether With reference to IEC :201 Tetrabromodiphenyl ether With reference to IEC :201 Pentabromodiphenyl ether With reference to IEC :201 Hexabromodiphenyl ether With reference to IEC :201 Heptabromodiphenyl ether With reference to IEC :201 Octabromodiphenyl ether With reference to IEC :201 Nonabromodiphenyl ether With reference to IEC :201 Decabromodiphenyl ether With reference to IEC :201 Phthalates Benzyl butyl phthalate (BBP) 0 Di-butyl phthalate (DBP) 0 Di-(2-ethylhexyl) phthalate (DEHP) 0 Di-isodecyl phthalate (DIDP) 0 Di-isononyl phthalate (DINP) 0 Di-n-octyl phthalate (DNOP) 0 Di-isobutyl phthalate (DIBP) 0 Di-ethyl phthalate(dep) 0 t +82 (0) f +82 (0)

4 Test Report No. F690101/LF-CTSAYAA Page 4 of 1 Sample No. : AYAA Sample Description : MLCC A(XR) J(JIS-B) X(X6S) TYPE Item No./Part No. : N/A Materials : N/A Phthalates Di-methyl phthalate (DMP) 0 [di(c7-c11 alkyl)phthalate] linear and branched (DHNUP) 0 [di(c6-c8 alkyl)phthalate] branched (DIHP) 0 Bis(2-methoxyethyl) phthalate (BMP, BMEP, DMEP) 0 Di-iso-pentyl phthalate(dipp) 0 Di-n-hexyl phthalate (DNHP) 0 Di-n-pentyl phthalate(dpp, DnPP) 0 Chlorinated Paraffin Alkanes, C10~13, Short Chain Chlorinated Paraffins(SCCP) With reference to ISO Chlorinated Organic Substances Polychlorinated Biphenyls (PCBs) With reference to US EPA 8082,(US EPA 30C), by GC/MS 3 Polychlorinated terphenyls (PCTs) With reference to US EPA 8082,(US EPA 30C), by GC/MS 3 Polychlorinated Naphthalene (PCN) With reference to US EPA 8081 A(US EPA 30C), by GC/MS Chlorinated Phenols PCP (Pentachlorophenol) with reference to 64 LFGB, B and ISO 17070, GC/MS 0.0 Polymer Identification t +82 (0) f +82 (0)

5 Test Report No. F690101/LF-CTSAYAA Page of 1 Sample No. : AYAA Sample Description : MLCC A(XR) J(JIS-B) X(X6S) TYPE Item No./Part No. : N/A Materials : N/A Polymer Identification PVC ** FT-IR - Negative Halogen Content Bromine(Br) With reference to EN 1482:2016, IC 30 Chlorine(Cl) With reference to EN 1482:2016, IC 30 Flame Retardants Hexabromocyclododecane (HBCDD) USEPA 340C, LC/MS Other(s) PFOS (Perfluorooctane Sulfonates-Acid/Metal Salt/Amide) US EPA 340C/30C, LC/MS 1 PFOA (Perfluorooctanoic acid) US EPA 340C/30C, LC/MS 1 NOTE: (1) = Not detected.(<mdl) (2) = ppm (3) MDL = Method Detection Limit (4) - = No regulation () Negative = Undetectable / Positive = Detectable (6) ** = Qualitative analysis (No Unit) (7) * = a. The result of Hexavalent Chromium (Cr(VI)) is ND as the result of Chromium (Cr) is ND, and confirmation test of Hexavalent Chromium (Cr(VI)) is not required. b. If the Chromium (Cr) content is greater than the MDL of Hexavalent Chromium (Cr(VI)), confirmation test of Hexavalent Chromium (Cr(VI)) is required. t +82 (0) f +82 (0)

6 Test Report No. F690101/LF-CTSAYAA Page 6 of 1 Picture of Sample as Received: AYAA t +82 (0) f +82 (0)

7 Test Report No. F690101/LF-CTSAYAA Page 7 of 1 Testing Flow Chart for RoHS:Cd/Pb/Hg/Cr 6+ /PBBs&PBDEs Testing Sample cutting / weighing Sample Preparation Cd/Pb/Hg/Cr PBBs/PBDEs 6+ Cr Acid Digestion with Microwave/Hotplate Sample Solvent Extraction Nonmetallic Material Metallic Material Filtration Concentration/Dilution of Extraction Solution Dissolving by ultrasonication Digesting at 10~160 Boiling water extraction Solution Residue 1) Alkali Fusion / Dry Ashing 2) Acid to dissolve Filtration GC/MS DATA Digestion at 60 by ultrasonication ph adjustment Separating to get aqueous phase Adding 1,-diphenylcar bazide for color UV-Vis ICP-OES/AAS Adding 1,-diphenylcarbazide for color DATA DATA UV-Vis DATA The samples were dissolved totally at the acid digestion step of the above flow chart for Cd,Pb,Hg Section Chief : Minkyu Park t +82 (0) f +82 (0)

8 Test Report No. F690101/LF-CTSAYAA Page 8 of 1 Flow Chart for Inorganic Elements Testing Inorganic Elements Mechanic_Sample Sample Measurement Acid Digestion with Microwave/Hotplate Filtration Residue Total Digestion ICP-AES DATA Major Inorganic Heavy Metals Antimony(Sb), Beryllium(Be), Phosphorus(P), Arsenic(As) etc. t +82 (0) f +82 (0)

9 Test Report No. F690101/LF-CTSAYAA Page 9 of 1 Flow Chart for Halogen Test Sample screening using XRF. Liquid containing water(>80%) Yes No Weigh the samples into the combustion boat. Add absorption solution into the bomb or tube. Admit O2 gas or O2 +Ar2 gas and start the combustion. Allow during absorption of the burnt gas. Dilute the solution (EPA300) Analyze absorbed solution using Ion Chromatography. Data t +82 (0) f +82 (0)

10 Test Report No. F690101/LF-CTSAYAA Page 10 of 1 Flow Chart for PVC Test Sample pretreatment / Separation Flame Test Sample analyzed by FT-IR Check wave number of C-CI Bonding Cl contents check (If necessary) QA / QC review / Check analysis result Data t +82 (0) f +82 (0)

11 Test Report No. F690101/LF-CTSAYAA Page 11 of 1 Flow Chart for PFOS/PFOA Test Sample pretreatment / Separation Sample extraction Concentrate/Dilute Extracted solution Analysis was performed by HPLC/MS QA / QC review / Check analysis result Data t +82 (0) f +82 (0)

12 Test Report No. F690101/LF-CTSAYAA Page 12 of 1 PCBs,PCTs,PCNs Flow Chart Sample 1.0 g Sample Size (3 x 3 x 2) mm 3 Is sample soluble? No Yes Place in a pre-washed test tube Place sample in a pre -weighed paper thimble Add ml of MC/Acetone(6:4) and tightly cap and sonicate for 3hr at 0 Soxhlet extraction for 6 hours with 80 ml of MC/Acetone(6:4) Cool to room temperature, filter(0.4 m) the extract and transfer the filtrate to autosampler vial Cool to room temperature, Concentrate to 1 ml by Rotary Vaccum Evaporator GC/MS Analysis transfer to the ml volumetric flask and make up with MC/Acetone(6:4) to the line t +82 (0) f +82 (0)

13 Test Report No. F690101/LF-CTSAYAA Page 13 of 1 SCCP Analysis Flow Chart Sample pretreatment Sample extraction by organic solvent Concentrate/Dilute Extracted solution GC/ECD analysis t +82 (0) f +82 (0)

14 Test Report No. F690101/LF-CTSAYAA Page 14 of 1 Testing Flow Chart for HBCD Sample pretreatment Sample extraction by organic solvent Concentrate/Dilute Extracted solution LC/MS analysis DATA t +82 (0) f +82 (0)

15 Test Report No. F690101/LF-CTSAYAA Page 1 of 1 Flow Chart for Phthalate Test Sample pretreatment / Separation Sample dissolved / extracted by THF Dilute Extracted solution Analysis was performed by GC/MS Data *** End of Report *** t +82 (0) f +82 (0)