Test Report No. F690101/LF-CTSAYGU

Transcription

1 Page 1 of 12 HAESUNGDS CO., LTD. (Seongju-dong) 726 Ungnam-ro,Seongsan-gu Chang-won-si,Gyeongsangnam-do Korea The following sample(s) was/were submitted and identified by/on behalf of the client as:- SGS File No. Product Name : AYGU : LEAD FRAME Item No./Part No. : C151-Ag Received Date : Test Period : Test Comments to : By the applicant's specific request, the sampling and testing was performed only for the part indicated in the photo without disassembly. Test Results : For further details, please refer to following page(s) SGS Korea Co., Ltd. / Gimhae Laboratory Thomas Hwang / Lab Manager 205, GBMC, 88 Somang-gil, Juchon-myeon, Gimhae-si, Gyeongnam, Korea 969

2 Page 2 of 12 Sample No. : AYGU Sample Description : LEAD FRAME Item No./Part No. : C151-Ag Materials : Metal Alloy Heavy Metals Cadmium (Cd) With reference to IEC :2013(Determination of Cadmium by ICP-OES) Lead (Pb) With reference to IEC :2013(Determination of Lead by ICP-OES) Mercury (Hg) With reference to IEC :2013(Determination of Mercury by ICP-OES) Hexavalent Chromium (Cr VI) * Antimony (Sb) Beryllium (Be) Arsenic (As) µg/cm² With reference to IEC :2015 (Determination of CrVI by UV-Vis) With reference to EPA 3052(1996), US EPA 6010B(1996), ICP With reference to EPA 3052(1996), US EPA 6010B(1996), ICP With reference to EPA 3052(1996), US EPA 6010B(1996), ICP MDL Results Flame Retardants-PBBs/PBDEs Monobromobiphenyl With reference to IEC :2015 (Determination Dibromobiphenyl With reference to IEC :2015 (Determination Tribromobiphenyl With reference to IEC :2015 (Determination Tetrabromobiphenyl With reference to IEC :2015 (Determination Pentabromobiphenyl With reference to IEC :2015 (Determination Hexabromobiphenyl With reference to IEC :2015 (Determination Heptabromobiphenyl With reference to IEC :2015 (Determination Octabromobiphenyl With reference to IEC :2015 (Determination Nonabromobiphenyl With reference to IEC :2015 (Determination Decabromobiphenyl With reference to IEC :2015 (Determination MDL Results 205, GBMC, 88 Somang-gil, Juchon-myeon, Gimhae-si, Gyeongnam, Korea 969

3 Sample No. : AYGU Sample Description : LEAD FRAME Item No./Part No. : C151-Ag Materials : Metal Alloy Flame Retardants-PBBs/PBDEs Page 3 of 12 Monobromodiphenyl ether With reference to IEC :2015 (Determination Dibromodiphenyl ether With reference to IEC :2015 (Determination Tribromodiphenyl ether With reference to IEC :2015 (Determination Tetrabromodiphenyl ether With reference to IEC :2015 (Determination Pentabromodiphenyl ether With reference to IEC :2015 (Determination Hexabromodiphenyl ether With reference to IEC :2015 (Determination Heptabromodiphenyl ether With reference to IEC :2015 (Determination Octabromodiphenyl ether With reference to IEC :2015 (Determination Nonabromodiphenyl ether With reference to IEC :2015 (Determination Decabromodiphenyl ether With reference to IEC :2015 (Determination MDL Results Phthalates Di-butyl phthalate (DBP) MDL Results Benzyl butyl phthalate (BBP) Di-(2-ethylhexyl) phthalate (DEHP) Di-isobutyl phthalate (DIBP) [di(c6-c8 alkyl)phthalate] branched (DIHP) [di(c7-c11 alkyl)phthalate] linear and branched (DHNUP) Bis(2-methoxyethyl) phthalate (BMP, BMEP, DMEP) Di-isononyl phthalate (DINP) Di-isodecyl phthalate (DIDP) Di-n-octyl phthalate (DNOP) Di-n-hexyl phthalate (DNHP) 205, GBMC, 88 Somang-gil, Juchon-myeon, Gimhae-si, Gyeongnam, Korea 969

4 Page 4 of 12 Sample No. : AYGU Sample Description : LEAD FRAME Item No./Part No. : C151-Ag Materials : Metal Alloy Phthalates MDL Results Di-n-pentyl phthalate(dpp) Halogen Contents MDL Results Bromine(Br) EN 14582:2007, IC 30 Chlorine(Cl) EN 14582:2007, IC 30 Fluorine(F) EN 14582:2007, IC 30 Iodine(I) EN 14582:2007, IC PFCs MDL Results Perfluorootanoic acid (PFOA) CEN/TS : 2010, LC/MS/MS 1 PFOS^ CEN/TS : 2010, LC/MS/MS 1 ^ PFOS refer to Perfluorooctanesulfonic acid and its derivatives including Perfluoroctanesulfonic acid, Perfluoroctane sulfonamide, N-Methylperfluoroctane sulfonamide, N-Ethylperfluoroctane sulfonamide, N-Methylperfluoroctane sulfonamidoethanol and N-Ethylperfluoroctane sulfonamidoethanol Flame Retardants MDL Results Hexabromocyclododecane (HBCDD, HBCD) USEPA 3540C, GC/MS 5 NOTE: (1) = Not detected.(<mdl) (2) = ppm (3) MDL = Method Detection Limit (4) - = No regulation (5) Negative = Undetectable / Positive = Detectable (6) ** = Qualitative analysis (No ) (7) * = a. The sample is positive for CrVI if the CrVI concentration is greater than 0.13 ug/cm2. The sample coating is considered to contain CrVI. b. The sample is negative for CrVI if CrVI is n.d. (concentration less than 0.10 ug/cm2). The coating is considered a non-crvi based coating. c. The result between 0.10 ug/cm2 and 0.13 ug/cm2 is considered to be inconclusive - unavoidable coating variations may influence the determination. 205, GBMC, 88 Somang-gil, Juchon-myeon, Gimhae-si, Gyeongnam, Korea 969

5 Page 5 of 12 Picture of Sample as Received: 205, GBMC, 88 Somang-gil, Juchon-myeon, Gimhae-si, Gyeongnam, Korea 969

6 Page 6 of 12 Testing Flow Chart for RoHS:Cd/Pb/Hg/Cr 6+ /PBBs&PBDEs Testing Cd/Pb/Hg Mechanic_Sample PBBs/PBDEs Mechanic_Sample Cr 6+ Mechanic_Sample Sample Measurement Sample Measurement Sample Measurement Acid Digestion with Microwave/Hotplate Filtration Residue Total Digestion ICP-OES/AAS/MS DATA Solvent Extraction of the Sample Screen Analysis Concentration/Dilution of Extraction Solution Filtration GC/MS DATA Nonmetallic Material Adding Extraction Solution Heating to 90~95 C for Extraction Filtration and ph Adjustment Adding 1,5-Diphenylcarbazide for Color Development UV-Vis DATA The samples were dissolved totally by pre-conditioning method according to above flow chart for Cd,Pb,Hg. Section Chief : Sharpless Park 205, GBMC, 88 Somang-gil, Juchon-myeon, Gimhae-si, Gyeongnam, Korea 969

7 Cr6+ Mechanic_Sample Page 7 of 12 Sample Measurement Metallic Material Boiling water extraction ( ± 5) cm2 ml DI water Remove sample after boiling for 10 min Filter the solution by 0.45 µm if necessary 1 ml orthophosphoric acid 25 ml as sample blank 25 ml as sample 1 ml diphenylcarbazide aci UV-VIS Absorbance Value <0.1 µg/cm2 0.1 µg/cm2 Absorbance Value 0.13 µg/cm2 Absorbance Value >0.13 µg/cm2 Negative result Inconclusive Positive result 205, GBMC, 88 Somang-gil, Juchon-myeon, Gimhae-si, Gyeongnam, Korea 969

8 Page 8 of 12 Flow Chart for Inorganic Elements Testing Inorganic Elements Mechanic_Sample Sample Measurement Acid Digestion with Microwave/Hotplate Filtration Residue Total Digestion ICP-AES DATA Major Inorganic Heavy Metals Antimony(Sb), Beryllium(Be), Phosphorus(P), Arsenic(As) etc. 205, GBMC, 88 Somang-gil, Juchon-myeon, Gimhae-si, Gyeongnam, Korea 969

9 Page 9 of 12 Flow Chart for Halogen Test Sample screening using XRF. Liquid containing water(>80%) Yes No Weigh the samples into the combustion boat. Add absorption solution into the bomb or tube. Admit O2 gas or O2 +Ar2 gas and start the combustion. Allow during absorption of the burnt gas. Dilute the solution (EPA300) Analyze absorbed solution using Ion Chromatography. Data 205, GBMC, 88 Somang-gil, Juchon-myeon, Gimhae-si, Gyeongnam, Korea 969

10 Page 10 of 12 Flow Chart for Phthalate Test Sample pretreatment / Separation Sample extraction by soxhlet method Concentrate/Dilute Extracted solution Analysis was performed by GC/MS QA / QC review / Check analysis result Data 205, GBMC, 88 Somang-gil, Juchon-myeon, Gimhae-si, Gyeongnam, Korea 969

11 Page 11 of 12 Flow Chart for PFOS/PFOA Test Sample pretreatment / Separation Sample extraction Concentrate/Dilute Extracted solution Analysis was performed by HPLC/MS QA / QC review / Check analysis result Data 205, GBMC, 88 Somang-gil, Juchon-myeon, Gimhae-si, Gyeongnam, Korea 969

12 Page 12 of 12 Testing Flow Chart for HBCD Sample pretreatment Sample extraction by organic solvent Concentrate/Dilute Extracted solution LC/MS analysis DATA *** End of Report *** 205, GBMC, 88 Somang-gil, Juchon-myeon, Gimhae-si, Gyeongnam, Korea 969