ANAMA Package & Container Testing Services, Inc.

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1 ANAMA Package & Container Testing Services, Inc. 607 Fayette Avenue, Mamaroneck, NY Tel: (914) Fax: (914) DEPARTMENT OF TRANSPORTATION PERFORMANCE ORIENTED PACKAGE TESTING CERTIFICATION Page 1 of 18 Testing Performed by: ANAMA Package & Container Testing Services, Inc. (+CM) Approval 607 Fayette Avenue Mamaroneck, NY (914) Testing Performed for: County Road 1000 Godley, TX Mr. Matt Holzer (817) matt.holzer@corelab.com 4G Design Re-Qualification Testing DW Fibreboard Box with kg Gross Weight Tubing Cutter Box ID: SMALL CUTTER BOX u n 4G / Y 2.7 / S / ** USA / +CM0238 ** insert year the packaging is manufactured Anton Cotaj, Certification Officer

2 ANAMA Package & Container Testing Services, Inc. 607 Fayette Avenue, Mamaroneck, NY Tel:(914) Fax: (914) SECTION 1 - CERTIFICATION 4G Design Re-Qualification Testing of the, Godley, TX 4G Design Re-Qualification Testing DW Fibreboard Box with kg Gross Weight Tubing Cutter Page 2 of 18 Requesting Party: Tel: (817) County Road 1000, PO Box matt.holzer@corelab.com Godley, TX Attn: Mr. Matt Holzer ANAMA Packaging & Container Testing Services, Inc. is a current DOT UN Third-Party Certification Agency under and certifies that the, Godley, TX packaging prepared as for transport, referenced above and tested in September & October has passed the Standards of the US Department of Transportation, Title 49CFR, Performance Oriented Packaging Standards; Section 178. This package is also certified under IMDG and UN Recommendations of the Committee of Experts on the Transportation of Dangerous Goods. It is the responsibility of the shipper / end user to ensure appropriate use. The use of other packaging methods or components other than those documented in this report may render this report invalid. SUMMARY OF PERFORMANCE TESTS Test Specification Test Level Time Results Drop 49 CFR m N/A Pass Stacking 49 CFR kg 24 Hours Pass Cobb 49 CFR gr/m² 30 Minutes Pass Vibration 49 CFR CPM 60 Minutes Pass Test Report #0238 UN Marking (49 CFR ) 4G / Y 2.7 / S / ** USA / +CM0238 Package Identification Code 4G - Fibreboard Box (49 CFR ) Performance Standard Y - Packaging meets Packing Group II and III Tests Authorized Gross Mass 2.7 kg (5.94 lbs) "S" Designation Denotes Inner Packaging Year of Manufacture ** Insert year the packaging is manufactured Country Authorizing The Mark USA DOT UN Third-Party Certification Agency (+CM) ANAMA Package & Container Testing Services, Inc. Approval Third Party Packaging Identification Number +CM0238 Anton Cotaj, Certification Officer

3 Page 3 of 18 SECTION 2 - Description of The Tested Package One (1) 1.68 kg gross weight anti-static bubble-wrapped metal cylindrical tubing cutter assembly inner packaging wrapped around with anti-static bubble sheet and inserted into a center special slotted fibreboard container (International Box Code 0204) outer packaging. The use of other packaging methods or components may render this report invalid. INNER PACKAGING DETAIL #1 Reference Section 8 for drawings Type Bubble Wrap Count 1 Style/Description Anti-static bubble wrap Supplier Uline, Inc., Waukegan, IL Part # S-5270 Type 3/16" Bubble Antistatic LDPE Nominal Thickness 4.8 mm (3/16") Dimension (mm, OD) flat 300 x 880 Tare Weight 12.4 grams INNER PACKAGING DETAIL #2 Reference Section 8 for drawings Type Steel Cylinder with Screw On Lid Count 1 Style/Description Machined steel cylindrical shape with steel cover Manufacturer Owen Oil Tools, Godley, TX Dimension (mm, OD) 52.5 x 160 ( with lid) Dimension (mm, OD) 50.7 x (without lid) Print/Label CUT R00; Gross Weight (as tested) grams with lid Lid Dimension (mm, OD) 52.5 x 61.4 Gross Weight (as tested) kg Note This article was placed wrapped around with bubble sheet

4 Page 4 of 18 INNER PACKAGING DETAIL #3 Reference Section 8 for drawings Type Anti-Stat Zip-Lock Bag Count 1 Style/Description Zip-lock bag with heat-sealed side seams Manufacturer Uline, Inc., Waukegan, IL Material of Construction Pink anti-stat LDPE, 3 Mil nominal gauge Minimum Thickness mm Nominal Thickness mm Dimension (mm, OD), W X L, flat 76 x 127 Side Seam Width, mm 1.5 mm Top Seam Width, mm 2.5 mm, 17.3 mm away from top edge Tare Weight 2.4 grams Gross Weight (as tested) 5 grams Print None Method of Closure Gasket was inserted into bag, then bag was press-and-seal closed. This bag was folded and inserted into steel cylinder INNER PACKAGING DETAIL #4 Type Gasket1 Count 1 Style/Description O-style rubber gasket Manufacturer Owen Oil Tools, Godley, TX Diameter 50 mm OD Cross Section 4.0 mm diameter Tare Weight 2.6 grams Note This gasket was placed inside the zip-locked bag PRODUCT/ARTICLES ADDITIONAL WEIGHT TEST MATERIAL DETAIL Type Metal Blocks Count 2 Style/Description Solid steel block Dimension (mm, OD), D X H 76 x 76 x 9.4, grams each Overall Gross Weight 840 grams Note These steel blocks were placed inside the box to reach the desired weight Overall Inner Package Gross Weight (IPGW) 2540 grams

5 Page 5 of 18 OUTER PACKAGING - UN 4G (Reference Section 8 for drawings) Type Fiberboard Box Style Center Special Slotted Container (CSSC), FEDCO Style: 0204 Manufacturer/Supplier DanHil Containers, LTD, Temple, TX Part # File # 9551 DanHil # XXx Material of Construction Kraft/Kraft Vertical Corrugated, 40H Michelman outside with MRA Dimension (mm, OD), L X W X H 113 x 113 x 253 Dimension (mm, ID), L X W X H 100 x 100 x 229 Number of Walls - Flute Type Double-Wall BC-Flute BMC (Box Marked Certification) 275# (42/26/26/26/42) Tare Weight grams Tested Basis Weight (lbs/1000ft²) ( ) Tested Caliper 6.53 mm Method of Joining Panels Folded inside and stitched with seven (7) 12.5 mm wide staples Mfr's Joint Flap Size 42 mm Mfr's Joint Location 5-2 corner as per the ASTM diagram Top Flap Gap/Meet Inner: Meet Outer: Meet Bottom Flap Gap/Meet Inner: Meet Outer: Meet Print Owen Closure Method (Refer to Section 7 for Closing Instruction and Section 8 for Specs) Closure 3/4" C34 Stick Staples Description 18 mm (3/4") long, 31 mm (1-1/4") crown galvanized metal staples Manufacturer/Supplier Uline, Inc. Waukegan, IL Uline Item # S-1396 Owen Part # STA S Top Closure Two (2) 0.8 grams each staples along the flap seam, 38 mm (1-1/2") away from boxes outside edges, 38 mm (1-1/2") apart Bottom Closure Two (2) 0.8 grams each staples along the flap seam, 38 mm (1-1/2") away from boxes outside edges, 38 mm (1-1/2") apart Method of Closure See Section 7.2 OUTER PACKAGING DETAILS Reference Section 8 for drawings Type Bubble Wrap Count 1 Style/Description Anti-static bubble wrap Supplier Uline, Inc., Waukegan, IL Part # S-5270 Type 3/16" Bubble Antistatic LDPE Nominal Thickness 4.8 mm (3/16") Dimension (mm, OD) flat 305 x1840 Tare Weight 22.4 grams Note This bubble sheet was folded in half and wraps around inner article Overall Outer Package Tare Weight (OPTW) grams

6 Page 6 of 18 SECTION 3 - Test Description and Test Results Drop Test 49 CFR Test Specimen/Contents Characteristics Number of Packages Tested 5 Product Specific Gravity 1.2 Packing Group Number PG II State Solid Dummy Load Steel cylinders/segments Drop Height Multiplier 0.67 for PG III; 1 for PG II & 1.5 for PG I Drop Height 1.2 m Conditioning of Outer Packaging - 49 CFR (d) F & 50 % R.H. Content (Dummy Load) Test Temperature 73 F & 50 % R.H. Drop Test Method: The inner packaging were filled to 95% overflow capacity with dummy load. The packages were assembled as per closing instruction (Reference Section 7). Five (5) assembled packages, were subjected to a free fall drop test from a height of 1.2 meter onto a solid steel plated concrete floor as described below. Drops were conducted within 60 seconds of removal of the outer packagings from the conditioning chamber. Drop Test Results Sample Test Sample # Weight (kg) Orientation Top (mfr's) corner (Corner 1-2-5) Top surface (Face 1) Long side (Face 2) Short side (Face 6) Bottom surface (Face 3) Results Box outside impact corner was slightly crushed around, approximately 2" in diameter, however box was still in-tact and capable and safe for further handling. There was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance There was no visible damage to the outer packaging, there was no leakage of the filling substance

7 Page 7 of 18 Pass/Fail Criteria - A package is considered to successfully pass the drop tests if for each sample tested: For packaging containing liquid, there is no leakage of the filling substance from the inner packaging. There is no damage to the outer packaging likely to adversely affect safety during transport. Inner receptacles, inner packagings or articles must remain completely within the outer packaging. Any discharge from a closure is slight and ceases immediately after impact or pressure equalization with no further leakage. No rupture is permitted in packagings for materials in Class 1 which would permit spillage of loose explosive substances or articles from the outer packaging. Stacking Test - 49 CFR (See Section 5.2 for Calculation) Test Specimen/Contents Characteristics Number of Packages Tested 3 Product State Solid Dummy Load Steel cylinders/segments Conditioning of Outer Packaging - 49 CFR (d) F & 50 % R.H. Test Temperature 73 F & 50 % R.H. Test Method Free standing, static (dead weight) test Test Duration 24 hours Minimum calculated stacking test weight 70.2 kg (154 lbs) per package Actual stacking test weight 72.6 kg (160 lbs) per package Test Duration 24 hours Stacking Test Method: The inner packaging were filled to 95% overflow capacity with dummy load. The packages were assembled as per closing instruction (Reference Section 7). Stacking test load (dead weight) of 72.6 kg was applied individually to the top of the three assembled packages using wood load spreaders and the weight was maintained for 24 hours. Stacking Test Results Test Sample # Test Sample Weight (kg) Test Load (Kg) Duration Stacking Test Results Hours Hours Hours Boxes did not show any signs of deterioration or distortion, there was no leakage of the filling substance Pass/Fail Criteria - A package is considered to successfully pass the stack tests if for each sample tested: No test sample shows any deterioration or distortion that could adversely affect safety during transport causing instability in stacks of packages, or cause damage to inner packagings that is likely to reduce safety in transport. There no leakage of the filling substance from the inner receptacle, or inner packaging

8 Page 8 of 18 Vibration Test - 49 CFR Test Specimen/Contents Characteristics Number of Packages Tested Product State Dummy Load Conditioning of Outer Packaging - 49 CFR (d) Test Temperature Test Method Test Duration Test Frequency 3 (Simultaneously), same samples used for stacking test Solid Steel cylinders/segments F & 50 % R.H. Ambient ASTM D Rotary Motion Vibration 60 minutes 235 CPM Vibration Test Method: The inner packagings were filled to 95% overflow capacity with dummy load. The packages were re-assembled as per closing instruction (Reference Section 7). Three (3) assembled packages were simultaneously placed on a rotary vibration table platform having 25.4 mm peak-topeak displacement and vibrated in normal shipping orientation for one (1) hour at 235 CPM such that a 1.6 mm thickness could be passed between the bottom of the samples and the platform. Immediately thereafter, the packages were removed from the platform and turned on its side for examination. Vibration Test Results Test Sample # Test Sample Weight (kg) Frequency (CPM) Duration (Minutes) Vibration Test Results There was no rupture or deterioration of boxes, there was no leakage of the filling substance Pass/Fail Criteria - A package is considered to successfully pass the vibration test, if for each sample tested after it was immediately removed from table platform and turned on its side: There is no leakage or rupture from any of the packaging. No test sample shows any deterioration which could adversely affect safety or container strength, during transport liable to reduce packaging strength.

9 Page 9 of 18 Cobb (Water Absorption) Test - 49 CFR [ISO International Standard (E)] Test Specimen/Contents Characteristics Number of Samples Tested 5 Test Duration 30 Minutes Test Intensity 100 ml Distilled Water Conditioning of Test Samples F & 50 % R.H. Test Method ISO 535, Cobb Method Cobb Test Results Sample # #1 #2 #3 #4 #5 Average Results grams/m² Pass Pass/Fail Criteria An increase in mass of greater than 155 grams/m² over the 30 minute duration of the tests represents an unacceptable level of water absorption. SECTION 4 - Shippers Responsibility It is the responsibility of the end shipper to determine authorization for use under these regulations. It is the shippers responsibility to determine if the packaging is compatible for products to be shipped. Use of the marking of this certification for any variations without further testing as allowed under US DOT 49 CFR Section will be at complete responsibility of the shipper. By continuing to place the UN Markings on Packagings, the packaging manufacturer or shipper is certifying that each packaging is constructed in the same manner as the originally tested and certified packaging, and that each packaging is capable of withstanding the prescribed performance tests. According to 49 CFR Section (g) (1) Variation 1 - variations are permitted in inner packaging of a tested combination packaging without further testing of the package, provided an equivalent level of performance is maintained as described in (g) (1) Variation 1 (i),(a),(b),(c),(d),(e) and (F) and (ii). According to 49 CFR Section (g) (4) Variation 4 - Variations are permitted in outer packagings of a tested design-type combination packaging, without further testing, provided an equivalent level of performance is maintained and as described in (g) (4) Variation 4 (i),(ii),(iii),(iv) and (v). According to US DOT 49 CFR Section (e), the packaging manufacturer shall achieve successful test results for the periodic retesting at intervals established by the manufacturer of sufficient frequency to ensure that each packaging produced by manufacturer is capable of passing the design qualification test. Changes in retest frequency are subject to the approval of the Associate Administrator for Hazardous Materials Safety. For combination packaging, the periodic retest must be conducted at least once every 24 months.

10 Page 10 of 18 SECTION 5 - Calculations 5.1 Certified Package Gross Mass Calculations Based on Test Level Overall Inner Package Gross Weight (IPGW) 2540 grams Overall Outer Package Tare Weight (OPTW) grams Number of Inner Packaging (NIP) 1 Packing Group Number II Minimum Package Weight as Tested (PGW) 2.72 kg Packing Group Multiplication Factor (PMF) 1.0 Formula for Calculating Certified Gross Mass (CGW) Certified Package Marking CGW = Minimum PGW CGW = Minimum PGW = 2.72 kg CGW = 2.7 kg (5.94 lbs) Y = 2.7 (5.94 lbs) 5.2 Stacking Strength Test Calculations Test Load (TL) Overall Stacking Height of Packages (SH) Overall Stacking Height of Package (PH) TL (Static) TL = [(SH - PH) - 1] x CGW (static) TL = [(SH - PH) - 1] x CGW x 1.5 (dynamic) 3000 mm (10 feet) 113 mm TL = [(3000/113) - 1] x 2.7 = 26 (rounded up) x 2.7 TL = 70.2 kg (154 lbs) Rounded up to at 72.6 kg (160 lbs) per package for test purposes

11 Page 11 of 18 Regulatory Standard References: Test Appendix A Regulatory & Industry Standard References CFR UN Regulation IMDG ICAO IATA Drop Test Stacking Test Hydrostatic Pressure (c) Cobb Test Vibration Test United States Code of Federal Regulations (CFR), Title 49, Transportation, Parts The United Nations Recommendations on The Transport of Dangerous Goods Model Regulations (Orange Book) 3. International Maritime Dangerous Goods Code (IMDG) 4. Technical Instructions for the Safe Transport of Dangerous Goods by Air (ICAO) 5. International Air Transport Association (IATA), Dangerous Goods Regulations Industry Standard References: Drop Test ASTM D5276 Standard Test Method for Drop Test of Loaded Containers by Free Fall Stacking Test ASTM D4577 Standard Test Method for Compression Resistance of a Container Under Constant Load Hydrostatic Standard Guide for Conducting Internal Pressure Tests on United Nations ASTM D7660 Pressure (UN) Packagings Cobb Test ISO 535 Paper and Board Determination of Water Absorption Cobb Method Vibration Test ASTM D999 Standard Test Method for Vibration Testing of Shipping Containers American Society for Testing and Materials (ASTM) International Organization for Standardization (ISO)

12 Page 12 of 18 Appendix B Test Equipment & Instrumentation No. Test Machine, Model # and Serial # Capacity Calibration Date Re-Calibration Date 1. Drop Table, Lansmont Corporation: Model #PDT-56-ED; Serial #M " 72" 2/27/2017 2/27/ Drop Table, Gaynes Eng. Inc., Serial #G " 120" 2/27/2017 2/27/ Vibration Table, Gaynes Eng. Inc.: Model #6000V 3000 lbs 2/27/2017 2/27/ Compression Machine, TechLab Systems: Model #Validator; S/N # T lbs 2/27/2017 2/27/ Digital Thermometer, Mannix: Model #DT721 (for Conditioning, Freezer), F 2/23/2017 2/23/ Paperless Temperature & Humidity Recorder, Dickson: Model #TH660 (for Cold Chamber) F 2/23/2017 2/23/ Paperless Temperature & Humidity Recorder, F, Dickson: Model #TH635 (for Hot Chamber) 0% 95% RH 2/23/2017 2/23/ Thermometer & Hygrometer, F, Omega Engineering: Model #RH520 10% 95% RH (for Conditioning Room) 2/23/2017 2/23/ Bench Scale, SeiKo Scale Division: Model #WA200001XP; S/N# mg 20 kg 5/16/2017 5/16/ Bench Scale, Mettler Toledo: Model #ICS4x9-1; S/N# mg 30 kg 5/16/2017 5/16/ Analytical Balance, PCA, Germany: Model #AB200; S/N # mg 200 g 5/16/2017 5/16/ Bench Scale, Ohaus: Serial # XZ lbm 5/16/2017 5/16/ Caliper, General Tools & Instruments: Model # , S/N: 81PCS " 5/16/2017 5/16/ Caliper, Fowler: Model # " 5/16/2017 5/16/ Electronic Torque-Meter, Kaps-All: Model #EB-650; S/N # inch-lbs 12/19/ /19/ Toque Wrench, CDI, Model No. 301LDIN 0 30 inch-lbs 5/17/2017 5/17/ General Purpose Digital Pressure Gauge, Omega Engineering: Model #DPG psi 5/15/2017 5/15/ General Purpose Digital Pressure Gauge, Omega Engineering: Model #DPG V psi 5/15/2017 5/15/ Winters Pressure Gauge, WG psi 5/15/2017 5/15/ Ashcrof Pressure Gauge, V/300 Psi Part # ; S/N: The Mullen Tester, B.F Perkins and Son: Serial # ECT Tester, Testing Machines, Inc.: S/N 5852X Measuring Tape, Ultra-Touch: ANAMA TM1 & TM2 Measuring Tape, Stanley Power Lock, ; ANAMA TM3 Measuring Tape, Made In China; ANAMA TM4 Presto Dart Impact Tester, Model No. PCN-230; S/N: psi 10/21/ /21/ psi 5/18/2017 5/18/ lbs 5/18/2017 5/18/ Feet 5/16/2017 5/16/ Feet 5/16/2017 5/16/ Feet 5/16/2017 5/16/ " 1.7 feet 2/28/2017 2/28/2018

13 Page 13 of 18 SECTION 6 Inner & Outer Packaging Photographs Primary Inner Packaging Components Outer Packaging Components:

14 Page 14 of 18 SECTION 7 - Packaging Assembly (Closing) Instruction Note: Packages were re-assembled same way as received. Step-by-Step Packaging Assembly Demonstration

15 Page 15 of 18 Manufacturer s Closing Instructions:

16 Page 16 of 18 SECTION 8 - Package Specifications & Drawings Anti-Static Sheet Specifications

17 Page 17 of 18 Outer Box Drawing & Specifications

18 Page 18 of 18 Carton Sealing Staples Specification

ANAMA Package & Container Testing Services, Inc. DEPARTMENT OF TRANSPORTATION PERFORMANCE ORIENTED PACKAGE TESTING CERTIFICATION

ANAMA Package & Container Testing Services, Inc. DEPARTMENT OF TRANSPORTATION PERFORMANCE ORIENTED PACKAGE TESTING CERTIFICATION ANAMA Package & Container Testing Services, Inc. 607 Fayette Avenue, Mamaroneck, NY 10543 Tel: (914) 899-3300 Fax: (914) 899-3325 info@anamapackagetesting.com www.anamapackagetesting.com Page 1 of 22 DEPARTMENT

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