Test Report No Rev01 Dated 11 Mar 2017

Transcription

1 Note: This report is issued subject to the Testing and Certification Regulations of the TÜV SÜD Group and the General Terms and Conditions of Business of TÜV SÜD Malaysia Sdn Bhd. In addition, this report is governed by the terms set out within this report. SUBJECT Chemical Analysis CLIENT DYNACRAFT INDUSTRIES SDN BHD 255-A, BLOCK D, PHASE 2, BAYAN LEPAS INDUSTRIAL ZONE PENANG SAMPLE RECEIVING DATE / TEST DATE 28 Feb 2017 / 06 Mar Mar 2017 DESCRIPTION OF SAMPLE / CONDITION OF SAMPLE RECEIVED Product Name WO Number : R STK Number : ES101665AASA Manufacturing Date : 24/01/2017 Sample Condition METHOD OF TEST : Ag Plating Leadframe using copper blank C194 : The samples are received in good condition, no scratch or damage was observed. The samples were tested in accordance with customer requirement. TESTED/PREPARED BY SIGNATORY Wan Mohd Effendi Engineer Goh Chun Yeong Lab Manager Laboratory: TÜV SÜD Malaysia Sdn Bhd No 18, Jalan Astaka U8/82, Bukit Jelutong, Shah Alam, Selangor, Malaysia.. Phone : Fax : enquiry@tuv-sud.my Regional Head Office: TÜV SÜD Asia Pacific Pte. Ltd. 3 Science Park Drive #04-01/0 The Franklin, Singapore Page 1 of 14

2 TABLE OF CONTENTS CONTENTS PAGE TEST SUMMARY 3 TEST RESULTS 4 PICTURE OF TEST SAMPLE 7 FLOW CHART 8 TERMS AND CONDITION Rev01 DYNACRAFT INDUSTRIES SDN BHD Page 2 of 14

3 TEST SUMMARY The sample was tested in accordance with customer specification. Test Summary Test Standard Test Description Judgment IEC Ed. 1.0: ICP-OES IEC Ed. 1.0: ICP-OES IEC Ed. 1.0: UV Spectrophotometer IEC Ed. 1.0: GC-MS BS EN : 2007 Ion Chromatography RoHS 1: Cadmium (Cd), Lead (Pb), Mercury (Hg), Hexavalent Chromium (Cr 6+ ), Polybrominated Piphenyl (PBB), Polybrominated Diphenylethers (PBDE). Chlorine (as Cl-) as Screening Test for PCB/ PCN/ PCT & Chlorinated Paraffins (C10-C13) BS EN : 2007 Ion Chromatography Halogen: Chlorine (as Cl-), Bromine (as Br - ), Iodine (as I - ), Fluorine (as F - ) BS EN 14582:2007 Ion Chromatography USEPA Method 3052 USEPA Method 6010C USEPA Method 3052 USEPA Method 6010C USEPA Method 3052 USEPA Method 6010C IEC Ed. 1.0: ICP-OES PFOS/PFOA Total Antimony (as Antimony Oxide) Total Beryllium (as Beryllium Oxide) Total Tin as Screening Test for Organotin Compounds (TBT/TPT/TBTO/DBT/DOT) PVC USEPA Method 3540C GC-MS Phthalates (DBP, DEHP, DNOP, DINP, DIDP, BBP, DIBP, DNHP, DIHP, DHNUP, DMEP) USEPA Method 3540C GC-MS HBCDD Rev01 DYNACRAFT INDUSTRIES SDN BHD Page 3 of 14

4 Parameter Method MDL Result Cadmium (as Cd) IEC mg/kg ND(<0.5) mg/kg RoHS Limit; mg/kg TEST RESULTS Judgment 100 Lead (as Pb) IEC mg/kg ND(<1) mg/kg 1000 Mercury (as Hg) IEC mg/kg ND(<5) mg/kg 1000 Hexavalent Chromium (Qualitative) IEC Negative/ Positive/ Inconclusive negative 1000 Monobromobiphenyl IEC mg/kg ND(<5) mg/kg - Dibromobiphenyl IEC mg/kg ND(<5) mg/kg - Tribromobiphenyl IEC mg/kg ND(<5) mg/kg - Tetrabromobiphenyl IEC mg/kg ND(<5) mg/kg - Pentabromobiphenyl IEC mg/kg ND(<5) mg/kg - Hexabromobiphenyl IEC mg/kg ND(<5) mg/kg - Heptabromobiphenyl IEC mg/kg ND(<5) mg/kg - Octabromobiphenyl IEC mg/kg ND(<5) mg/kg - Nonabromobiphenyl IEC mg/kg ND(<5) mg/kg - Decabromobiphenyl IEC mg/kg ND(<5) mg/kg - Sum of PBBs - - ND(<5) 1000 Monobromodiphenyl ether IEC mg/kg ND(<5) mg/kg - Dibromodiphenyl ether IEC mg/kg ND(<5) mg/kg - Tribromodiphenyl ether IEC mg/kg ND(<5) mg/kg - Tetrabromodiphenyl ether IEC mg/kg ND(<5) mg/kg - Pentabromodiphenyl ether IEC mg/kg ND(<5) mg/kg - Hexabromodiphenyl ether IEC mg/kg ND(<5) mg/kg - Heptabromodiphenyl ether IEC mg/kg ND(<5) mg/kg - Octabromodiphenyl ether IEC mg/kg ND(<5) mg/kg - Nonabromodiphenyl ether IEC mg/kg ND(<5) mg/kg - Decabromodiphenyl ether IEC mg/kg ND(<5) mg/kg - Sum of PBDEs - - ND(<5) 1000 Parameter Method MDL Result Judgment Chlorine (as Cl ~ ) BS EN mg/kg ND(<5) mg/kg Bromine (as Br ~ ) BS EN mg/kg ND(<5) mg/kg Iodine (as I ~ ) BS EN mg/kg ND(<10) mg/kg Fluorine (as F ~ ) BS EN mg/kg ND(<10) mg/kg PFOS BS EN mg/kg ND(<10) mg/kg PFOA BS EN mg/kg ND(<10) mg/kg Rev01 DYNACRAFT INDUSTRIES SDN BHD Page 4 of 14

5 TEST RESULTS Parameter Method MDL Result Judgment Antimony (as Sb) USEPA Method 3052 USEPA Method 6010C Beryllium (as Be) USEPA Method 3052 USEPA Method 6010C 5 mg/kg ND(<5) mg/kg 1 mg/kg ND(<1) mg/kg Parameter Method MDL Result Judgment Total Tin (as Sn) USEPA Method 3052 USEPA Method 6010C 5 mg/kg 405 mg/kg Parameter Method Result Judgment Bis (2-ethylhexyl) Phthalate (as DEHP) USEPA Method 3540C ND(<0.01) % Benzyl Butyl Phthalate (as BBP) USEPA Method 3540C ND(<0.01) % Dibutyl Phthalate (as DBP) USEPA Method 3540C ND(<0.01) % Diisononyl Phthalate (as DINP) USEPA Method 3540C ND(<0.01) % Diisodecyl Phthalate (as DIDP) USEPA Method 3540C ND(<0.01) % Di-n-octyl Phthalate (as DNOP) USEPA Method 3540C ND(<0.01) % Di-n-hexyl phthalate (as DNHP) USEPA Method 3540C ND(<0.01) % Diisobutyl Phthalate (as DIBP) USEPA Method 3540C ND(<0.01) % Bis (2-methoxyethyl) Phthalate (as DMEP) USEPA Method 3540C ND(<0.01) % Diisoheptyl Phthalate (as DIHP) USEPA Method 3540C ND(<0.01) % Total - N/A Parameter Method MDL Result Judgment Chlorine (as Cl-) as Screening Test for PCB/ PCN/PCT and Chlorinated Paraffins Hexabromocyclododecane (as HBCDD) BS EN mg/kg ND(<10) mg/kg USEPA Method 3540C 5 mg/kg ND(<5) mg/kg Parameter Method Result Judgment PVC IEC No significant level of PVC was detected in Ag Plating Leadframe using copper blank C194 (Matching Percentage 16.95%) Rev01 DYNACRAFT INDUSTRIES SDN BHD Page 5 of 14

6 TEST RESULTS FTIR Spectrum of Ag Plating Leadframe using copper blank C194 ATR %T cm-1 Comparison FTIR spectrum of Ag Plating Leadframe using copper blank C194 with PVC Ag Plating Leadframe %T PVC 16.95% matches cm Note: I. The test portion was Totally Dissolved for Cadmium, Lead & Mercury Test by using pre-conditioning method. II. % = Percentage by weight III. Expression result for Hexavalent Chromium: Concentration of Hexavalent Chromium Expression of Result <0.10 µg/cm2 Negative Sample coating is consider non Cr(VI) based coating 0.10 and 0.13 µg/cm2 Inconclusive Unavoidable coating variations may influence the determination 0.13µg/cm2 Positive Sample coating is consider to contain Cr(VI) Rev01 DYNACRAFT INDUSTRIES SDN BHD Page 6 of 14

7 PICTURE OF TEST SAMPLE Photo of Test Sample Rev01 DYNACRAFT INDUSTRIES SDN BHD Page 7 of 14

8 FLOW CHART Flow chart for method IEC Hexavalent Chromium Sample Mechanical Sample Preparation Size reduction by manual cutting, grinding or milling Homogenized samples specimens and sub-sampling test portion Cr 6+ (Metals) Cr 6+ (Polymers and electronics) Boiling water extraction According to IEC Screening for total chromium IEC Color development with Diphenylcarbazide Colorimetric method According to IEC 62321:2008 (Annex C) No colour change Reporting of Result A red color indicates the presence of Cr 6+. If necessary, confirm with UV- UV/VIS Spectrophotometer measurement Color development with Diphenylcarbazide Reporting of Result Note : Detected with suspected level of concentration Rev01 DYNACRAFT INDUSTRIES SDN BHD Page 8 of 14

9 FLOW CHART Flow chart for method IEC Cadmium (as Cd), Lead (as Pb), Mercury (as Hg) Sample Mechanical Sample Preparation Size reduction by manual cutting, grinding or milling Homogenized samples specimens and sub-sampling test portion Pb, Cd and Hg (Polymers, metals and electronics) Polymer IEC IEC Metals and Electronics IEC IEC Insoluble matter appeared Test portion totally dissolved Filtration Solution Residue Redissolved residue in solution Other acids treatment or alkali Combine both solutions Test portion totally dissolved Element determination by ICP-AES/Cold Vapour-AAS and QC Standard check measurement Reporting of Result Note : Detected with suspected level of concentration Rev01 DYNACRAFT INDUSTRIES SDN BHD Page 9 of 14

10 FLOW CHART Flow chart for method IEC PBBs, PBDEs Sample Mechanical Sample Preparation Size reduction by manual cutting, grinding or milling Homogenized samples specimens and sub-sampling test portion Solvent extraction According to IEC (PBB/PBDE) Extracted Solution Extracted sample residue Clean up filtration and preconcentration/ dilution Discard Gas Chromatography- Mass Spectrometry Measurement Reporting of Result Note : Detected with suspected level of concentration Rev01 DYNACRAFT INDUSTRIES SDN BHD Page 10 of 14

11 FLOW CHART Flow chart for BS EN : 2007 Bromine (as Br ~ ), Chlorine (as Cl~), Iodine (as I~), Fluorine (as F~), PFOS, PFOA, Chlorine (as Cl-) as Screening Test for PCB/ PCN/PCT and Chlorinated Paraffins Sample Mechanical Sample Preparation Size reduction by manual cutting, grinding or milling Homogenized samples specimens and sub-sampling test portion Oxygen combustion in closed system as per Method BS EN :2007 Absorption of gases in alkaline solution Filtration Measurement by using Ion-Chromatography (IC) Reporting of Result Rev01 DYNACRAFT INDUSTRIES SDN BHD Page 11 of 14

12 FLOW CHART Flow chart for USEPA Method 3052 / 6010C Antimony (as Sb), Beryllium (as Be), Total Tin (as Sn) Sample Mechanical Sample Preparation Size reduction by manual cutting, grinding or milling Homogenized samples specimens and sub-sampling test portion For Heavy Metal determination as per listed at USEPA Method 3052 Microwave assisted acid digestion (HCL + H 2 O 2 + HNO 3 ) As per USEPA Method 3052 Insoluble matter appeared (with residue) (without residue) Filtration Solution without residue Residue Combine both solutions Test portion totally dissolved Redissolved residue in solution Other acids treatment or alkali dissolution Test portion totally dissolved Element determination by ICP-AES and QC Standard check measurement Reporting of Result Rev01 DYNACRAFT INDUSTRIES SDN BHD Page 12 of 14

13 FLOW CHART Flow chart for USEPA Method 3540C DEHP, BBP, DBP, DINP, DIDP, DNOP, DNHP, DIBP, DMEP, DIHP, Hexabromocyclododecane (as HBCDD) Sample Mechanical Sample Preparation Size reduction by manual cutting, grinding or milling Homogenized samples specimens and sub-sampling test portion Suitable extraction with solvent As Per USEPA Method 3540C Extracted sample residue Extracted Solution Discard Clean up filtration and preconcentration Gas Chromatography-Mass Spectrometry Analysis Reporting of results Rev01 DYNACRAFT INDUSTRIES SDN BHD Page 13 of 14

14 Please note that this Report is issued under the following terms : 1. This report applies to the sample of the specific product/equipment given at the time of its testing/calibration. The results are not used to indicate or imply that they are applicable to other similar items. In addition, such results must not be used to indicate or imply that TÜV SÜD Malaysia Sdn Bhd approves, recommends or endorses the manufacturer, supplier or user of such product/equipment, or that TÜV SÜD Malaysia Sdn Bhd in any way guarantees the later performance of the product/equipment. Unless otherwise stated in this report, no tests were conducted to determine long term effects of using the specific product/equipment. 2. The sample/s mentioned in this report is/are submitted/supplied/manufactured by the Client. TÜV SÜD Malaysia Sdn Bhd therefore assumes no responsibility for the accuracy of information on the brand name, model number, origin of manufacture, consignment or any information supplied. 3. Nothing in this report shall be interpreted to mean that TÜV SÜD Malaysia Sdn Bhd has verified or ascertained any endorsement or marks from any other testing authority or bodies that may be found on that sample. 4. This report shall not be reproduced wholly or in parts and no reference shall be made by the Client to TÜV SÜD Malaysia Sdn Bhd or to the report or results furnished by TÜV SÜD Malaysia Sdn Bhd in any advertisements or sales promotion. February Rev01 DYNACRAFT INDUSTRIES SDN BHD Page 14 of 14