Pesticide Control Laboratory

Transcription

1 Department of Agriculture, Food and The Marine Backweston Laboratory Campus, Young's Cross, Backweston, Celbridge, Co Kildare Testing Laboratory Registration number: 121T is accredited by the Irish National Board (INAB) to undertake testing as detailed in the Schedule bearing the Registration Number detailed above, in compliance with the International Standard ISO/IEC 17025: nd Edition General Requirements for the Competence of Testing and Calibration Laboratories (This Certificate must be read in conjunction with the Annexed Schedule of ) Date of award of accreditation: 11:12:2000 Date of last renewal of accreditation: 18:05:2015 Expiry date of this certificate of accreditation: 18:05:2020 This shall remain in force until further notice subject to continuing compliance with INAB accreditation criteria, ISO/IEC and any further requirements specified by the Irish National Board. Manager: Dr Adrienne Duff Issued on 18 May 2015 Chairperson: Mr Tom O Neill Organisations are subject to annual surveillance and are re-assessed every five years. The renewal date on this Certificate confirms the latest date of renewal of accreditation. To confirm the validity of this Certificate, please contact the Irish National Board. The INAB is a signatory of the European co-operation for (EA) Testing Multilateral Agreement (MLA) and the International Laboratory Cooperation (ILAC) Mutual Recognition Arrangement. Edition 29, 13/04/ T Page 1 of 35

2 Schedule of (Annex to Certificate) PESTICIDE CONTROL LABORATORY Initial Registration Date : 11-December-2000 Postal Address: (Address of other locations as they apply) Backweston Laboratory Campus Young's Cross Backweston Celbridge Co Kildare Telephone: +353 (1) Fax: +353 (1) sean.hyland@agriculture.gov.ie Contact Name: Sean Hyland Facilities: Normally not available for Public testing Edition 29, 13/04/ T Page 2 of 35

3 Schedule of THE IRISH NATIONAL ACCREDITATION BOARD (INAB) is the Irish body for the accreditation of organisations including laboratories. Laboratory accreditation is available to testing and calibration facilities operated by manufacturing organisations, government departments, educational institutions and commercial testing/calibration services. Indeed, any organisation involved in testing, measurement or calibration in any area of technology can seek accreditation for the work it is undertaking. Each accredited laboratory has been assessed by skilled specialist assessors and found to meet criteria which are in compliance with ISO/IEC or ISO/IEC (medical laboratories). Frequent audits, together with periodic inter-laboratory test programmes, ensure that these standards of operation are maintained. Testing and Calibration Categories: : Permanent laboratory calibration and testing where the laboratory is erected on a fixed location for a period expected to be greater than three years. Category B: Category C: Category D: Site calibration and testing that is performed by staff sent out on site by a permanent laboratory that is accredited by the Irish National Board. Site calibration and testing that is performed in a site/mobile laboratory or by staff sent out by such a laboratory, the operation of which is the responsibility of a permanent laboratory accredited by the Irish National Board. Site calibration and testing that is performed on site by individuals and organisations that do not have a permanent calibration/testing laboratory. Testing may be performed using (a) (b) (c) (d) portable test equipment a site laboratory a mobile laboratory or equipment from a mobile or site laboratory Standard Specification or Test Procedure Used: The standard specification or test procedure that is accredited is the issue that is current on the date of the most recent visit, unless otherwise stated. Glossary of Terms Facilities: Public calibration/testing service: Conditionally available for public calibration/testing: Normally not available for public calibration/testing: Commercial operations which actively seek work from others. Established for another primary purpose but, more commonly than not, is available for outside work. Unavailable for public calibration/testing more often than not. Laboratory users wishing to obtain assurance that calibration or test results are reliable and carried out to the Irish National Board criteria should insist on receiving an accredited calibration certificate or test report. Users should contact the laboratory directly to ensure that this scope of accreditation is current. INAB will, on request, verify the status and scope. Edition 29, 13/04/ T Page 3 of 35

4 INAB Classification number (P9) Materials/products tested Residues in Foods and Agricultural Materials s residues in food of - Fruit + Vegetables + Honey - Type of test/properties measured Range of measurement Screening, confirmation and quantification of pesticide residues in food of A list of pesticides as defined in Annex 1. Standard specifications Equipment/techniques used Documented in house methods Extractions (SOP 101) based on: Standard multi-residue method used based on Analytical methods for pesticide residues in foodstuffs 6th Ed Ministry of Health, Welfare and Sport, The Netherlands Analysis using GC-MS/MS (SOP227) and LC-MS/MS (SOP228) Edition 29, 13/04/ T Page 4 of 35

5 INAB Classification number (P9) Materials/products tested 752 Residues in Foods and Agricultural Materials Type of test/properties measured Range of measurement Standard specifications Equipment/techniques used.02 s Screening, confirmation and Documented in house method residues in quantification of pesticide (SOP 106) based on: Standard food of animal origin residues in food of animal multi-residue Method based on (fat) origin (i.e. animal fats) Manual of Residue Analysis Vol 1. A list of pesticides as defined in DFG Deutsche Annex 1. Forschungs Gemeinshaft Analysis using GC-MS/MS (SOP227) and LC-MS/MS (SOP228) Residues in Foods and Agricultural Materials s residues in Screening, confirmation and quantification of pesticide residues in A list of pesticides as defined Documented in-house method (SOP 111) based on standard multi-residue method - Lehotay et al JAOAC Vol 88 in Annex 1. No.2 (2005) 615 Analysis using GC-MS/MS (SOP227) Edition 29, 13/04/ T Page 5 of 35

6 INAB Classification number (P9) Materials/products tested Residues in Foods and agricultural materials s residues in food of Fruit vegetables and honey Type of test/properties measured Range of measurement Screening, confirmation and quantification of Amitraz and its metabolites, DMPF and DMF as defined in Annex 6 Standard specifications Equipment/techniques used Documented in house method (SOP 114) based on standard multi-residue method published as J. AOAC Int Steven J. Lehotay, Katerina Mastrovska & Alam R. Lightfield Analysis by LC- MS/MS 761 Agricultural Products Quantitation of active Documented in house method and materials substance in plant protection (SOP 112) based on standard products as defined in Annex 2. CIPAC/AOAC/EU1107/ Insecticides and methods acaricide formulations.12 Herbicide formulations Analysis using GC-FID (SOP224).13 Fungicide formulations Range or HPLC DAD/CoronaCAD (SOP 0-100% 207).99 Other Agricultural products - s - Biocides Edition 29, 13/04/ T Page 6 of 35

7 INAB Classification number (P9) Materials/products tested Residues in Foods and Agricultural Materials s s and PCB residues in infant formula, follow on formula and milk powder Type of test/properties measured Range of measurement Screening, confirmation and quantification of pesticide residues in infant formula, follow on formula and milk powder. A list of pesticides as defined in Annex 1 Standard specifications Equipment/techniques used Documented in-house method (SOP 115) based on standard multi-residue method - Lehotay et al JAOAC Vol 88 No Analysis using GC-MS/MS (SOP227) and LC-MS/MS (SOP228) Edition 29, 13/04/ T Page 7 of 35

8 INAB Classification number (P9) Materials/products tested Residues in Foods and agricultural materials s residues in food of Fruit vegetables and cereals Residues in Foods and agricultural materials s residues in cereals Type of test/properties measured Range of measurement Screening, confirmation and quantitation of a range of quaternary ammonium salts and other pesticides in fruit, vegetables and cereals See Annex 3 for list of salts Screening, confirmation and quantitation of Glyphosate, Glufosinate, Ethephon and some of their metabolites in cereals Standard specifications Equipment/techniques used SOP 113 based on the /meth_quppe.pdf Quick Method for the Analysis of Residues of numerous Highly Polar s in Foods of Plant Origin involving Simultaneous Extraction with Methanol and LC-MS/MS Determination (QuPPe- Method), Version 7.1 Nov SOP 116 based on N. Yoshioka, M. Asano, A. Kuse, T. Mitsuhashi, Y. Nagasaki, Y. Ueno and J of Chromatography A 1218 (2011) See Annex 4 for list of compounds 752 Residues in Foods and Screening, confirmation and SOP 110 based on FERA method agricultural materials quantitation of a range of FD s dithiocarbamates in fruit, residues in vegetables and infant pesticides.eu/library/docs/srm Fruit and vegetables formula/follow on formula /meth_dithiocarbamatescs2_e and infant urlsrm.pdf formula/follow on See Annex 5 for list of formula compounds Edition 29, 13/04/ T Page 8 of 35

9 Animal Origin 1-Naphthylacetamide LC ,4- Dichlorobenzophenone GC Abamectin LC Acephate LC Acephate GC Acetamiprid LC Acetochlor LC Aclonifen GC Acrinathrin GC Alachlor GC Aldicarb LC Aldicarb-sulfone LC Aldicarb-sulfoxide LC Aldrin GC Ametryn LC Amidosulfuron LC Aminocarb LC Atrazine LC Edition 29, 13/04/ T Page 9 of 35

10 Animal Origin Atrazine-desethyl LC Atrazine-desisopropyl LC Azaconazole GC Azamethiophos GC Azinphos-ethyl GC Azinphos-methyl GC Azoxystrobin LC Azoxystrobin GC BAC 10 LC BAC 12 LC BAC 14 LC BAC 16 LC Benalaxyl LC Bendiocarb LC Bentazone LC Benthiavalicarbisopropyl LC Benzoximate LC Bifenthrin GC Binapacryl GC Bioresmethrin LC Edition 29, 13/04/ T Page 10 of 35

11 Animal Origin Biphenyl GC Bitertanol GC Bixafen LC Boscalid LC Boscalid GC Bromacil LC Bromophos-ethyl Bromophos-methyl GC GC Bromopropylate GC Bromoxynil LC Bromuconazole LC Bupirimate LC Buprofezin LC Butocarboxim Sulfoxide LC Butoxycarboxim LC Cadusafos LC Carbaryl LC Carbendazim LC Carbofuran LC Carbofuran 3 Hydroxy LC Edition 29, 13/04/ T Page 11 of 35

12 Animal Origin Carbosulfan LC Carboxin LC Carfentrazone-ethyl LC Chlorantraniliprole LC Chlorbromuron LC Chlorbufam GC Chlordane-cis GC Chlordane-trans GC Chlorfenapyr GC Chlorfenvinphos LC Chlorfluazuron LC Chloridazon LC Chlorobenzilate GC Chlorothalonil GC Chlorotoluron LC Chloroxuron LC Chlorpropham GC Chlorpyrifos LC Chlorpyrifos Methyl GC Chlorsulfuron LC and documented procedures. For details refer to the laboratory s master list of flexible scope changes, available from the laboratory. Edition 29, 13/04/ T Page 12 of 35

13 Animal Origin Chlorthal-dimethyl GC Chlozolinate GC Clethodim LC Clodinafop-propargyl LC Clofentezine LC Clomazone LC Clothianidin LC Coumaphos GC Cyanazine LC Cyanofenphos GC Cyanophos GC Cyazofamid LC Cyclanilide LC Cycloate LC Cycloxydim LC Cyfluthrin GC Cyhalothrin-lambda GC Cymiazol LC Cymoxanil LC Cypermethrin GC Edition 29, 13/04/ T Page 13 of 35

14 Animal Origin Cyproconazole GC Cyprodinil LC DDD-op GC DDAC LC DDD-pp GC DDE-op GC DDE-pp GC DDT-op GC DDT-pp GC DEET LC Deltamethrin GC Demeton-S-mesulfone GC Demeton-S-methylsulfoxide LC Desmedipham LC Diazinon GC Dichlobenil GC Dichlofenthion LC Dichlofluanid GC Dichlorvos GC Diclobutrazol LC Edition 29, 13/04/ T Page 14 of 35

15 Animal Origin Dicloran GC Dicrotophos LC Dieldrin GC Diethofencarb LC Difenoconazole LC Diflubenzuron LC Diflufenican LC Dimethenamid LC Dimethoate GC Dimethomorph LC Dimoxystrobin GC Diniconazole LC Dinoseb LC Dinoterb LC Dioxacarb LC Diphenamid LC Diphenylamine GC Ditalimfos LC Diuron LC DMSA LC Edition 29, 13/04/ T Page 15 of 35

16 Animal Origin DMST LC DNOC LC Dodine LC Emamectin B1a LC Endosulfan sulfate LC Endosulfan-alpha GC Endosulfan-beta GC Endosulfan-ether GC Endosulfan-lacton GC Endosulfan-sulfate GC Endrin GC EPN GC Epoxyconazole LC Esfenvalerate LC Ethiofencarb LC Ethiofencarb-sulfone LC Ethiofencarb-sulfoxide LC Ethion LC Ethirimol LC Ethofumesate LC Ethoprophos GC and documented procedures. For details refer to the laboratory s master list of flexible scope changes, available from the laboratory. Edition 29, 13/04/ T Page 16 of 35

17 Animal Origin Etofenprox LC Etoxazole GC Etridazole GC Etrimfos LC Famoxadone LC Fenamidone GC Fenamiphos LC Fenamiphos-sulfone LC Fenamiphos-sulfoxide LC Fenarimol GC Fenazaquin GC Fenbuconazole GC Fenchlorphos GC Fenhexamid LC Fenitrothion GC Fenothiocarb LC Fenoxaprop-P LC Fenoxycarb LC Fenpiclonil LC Fenpropathrin GC Edition 29, 13/04/ T Page 17 of 35

18 Animal Origin Fenpropidin LC Fenpropimorph LC Fenpyroximate LC Fenthion LC Fenthion Sulfone LC Fenthion Sulfoxide LC Fenuron LC Fenvalerate GC Fipronil LC Fipronil desulfynil LC Fipronil sulfide LC Fipronil sulfone LC Flamprop-isopropyl LC Flazasulfuron LC Flonicamid LC Florasulam LC Fluazifop LC Fluazifop-P-butyl LC Fluazinam LC Flubendiamide LC Edition 29, 13/04/ T Page 18 of 35

19 Animal Origin Flucycloxuron LC Flucythrinate GC Fludioxonil LC Fludioxonil GC Flufenacet LC Flufenoxuron LC Fluopicolide LC Fluopyram LC Fluquinconazole LC Flurochloridone LC Flurtamone GC Flusilazole GC Flutolanil LC Flutriafol LC Fluvalinate-tau GC Fluxapyroxad LC Fonofos GC Forchlorfenuron LC Formothion GC Fosthiazate LC Edition 29, 13/04/ T Page 19 of 35

20 Animal Origin Fuberidazole LC Furalaxyl GC Furathiocarb LC Furmecyclox LC Haloxyfop LC Haloxyfop-methyl LC HCH-alpha GC HCH-beta GC HCH-delta GC Heptachlor GC Heptachlor endoepoxide,trans Heptachlor exoepoxide,cis GC GC Heptenophos LC Hexachlorobenzene GC Hexaconazole GC Hexaflumuron LC Hexythiazox LC Imazalil LC Imazamox LC Imidacloprid LC Edition 29, 13/04/ T Page 20 of 35

21 Animal Origin Indoxacarb LC Iodofenphos GC Iodosulfuron-methyl LC Ioxynil LC Iprodione GC Iprovalicarb GC Isazophos GC Isocarbofos GC Isodrin GC Isofenphos LC Isofenphos GC Isofenphos-methyl GC Isofenphos-oxon GC Isoprocarb LC Isoprothiolane LC Isoproturon LC Kresoxim-methyl LC Lenacil GC Lindane GC Linuron LC Edition 29, 13/04/ T Page 21 of 35

22 Animal Range Origin mg/kg Lufenuron LC Malaoxon LC Malathion LC Mandipropamid LC MCPA LC MCPA methyl ester GC MCPB LC Mecarbam GC Mecoprop LC Mefenpyr-Diethyl LC Mepanipyrim LC Mephosfolan LC Mepronil LC Mesosulfuron methyl LC Metalaxyl LC Metamitron LC Metazachlor LC Metconazole LC Methacrifos GC Methamidophos LC Methamidophos GC Edition 29, 13/04/ T Page 22 of 35

23 Animal Origin Formula/Follo w Methidathion LC Methiocarb LC Methomyl LC Methoprene LC Methoxychlor GC Methoxyfenozide LC Metobromuron LC Metolachlor LC Metosulam LC Metoxuron LC Metrafenone LC Metribuzin GC Metsulfuron-methyl LC Mevinphos GC Mirex GC Molinate GC Molinate LC Monocrotophos LC Monolinuron LC Myclobutanil LC Edition 29, 13/04/ T Page 23 of 35

24 Animal Origin Napropamide LC Naptalam LC Neburon LC Nicosulfuron LC Nitenpyram LC Nitrofen GC Nonachlor-trans GC Nuarimol GC Omethoate GC o-phenylphenol GC Oxadiazon LC Oxadixyl GC Oxamyl LC Oxamyl Oxime LC Oxychlordane GC Oxyfluorfen LC Paclobutrazol LC Paraoxon methyl GC Paraoxon-ethyl LC Parathion-ethyl GC Edition 29, 13/04/ T Page 24 of 35

25 Animal Origin Parathion-methyl GC PCB 101 GC PCB 118 GC PCB 138 GC PCB 153 GC PCB 180 GC PCB 28 GC PCB 52 GC Penconazole LC Pencycuron LC Pendimethalin GC Pentachloroaniline GC Permethrin GC Pethoxamid LC Phenmedipham LC Phenthoate GC Phorate Sulfoxide LC Phosalone GC Phosmet GC Phosphamidon GC Edition 29, 13/04/ T Page 25 of 35

26 Animal Origin Phoxim LC Picoxystrobin LC Piperonyl butoxide LC Pirimicarb GC Pirimicarb desmethyl GC Pirimiphos-ethyl LC Pirimiphos-methyl LC Prochloraz GC Procymidone GC Profenofos GC Promecarb LC Promethryn LC Prometon LC Propachlor GC Propamocarb LC Propanil GC Propaquizafop LC Propargite GC Propazine LC Propetamphos GC Edition 29, 13/04/ T Page 26 of 35

27 Animal Origin Propham GC Propiconazole GC Propoxur LC Propoxycarbazone LC Propyzamide LC Proquinazid LC Prosulfocarb LC Prosulfuron LC Prothioconazole desthio LC Prothiofos GC Pymetrozine LC Pyraclostrobin LC Pyrazophos LC Pyrethrins LC Pyridaben LC Pyridaben GC Pyridaphenthion LC Pyrifenox GC Pyrimethanil LC Pyriproxifen LC Edition 29, 13/04/ T Page 27 of 35

28 Animal Origin Quinalphos LC Quinoxyfen LC Quintozene GC Quizalofop LC Quizalofop-ethyl LC Resmethrin GC Rimsulfuron LC Rotenone LC Silthiofam GC Simazine LC Simetryn LC Spinosyn A LC Spinosyn D LC Spirodiclofen LC Spirodiclofen GC Spiromesifen LC Spirotetramat LC Spiroxamine LC Sulfentrazone LC Sulfotep LC Edition 29, 13/04/ T Page 28 of 35

29 Animal Origin Sulprofos LC Tebuconazole LC Tebufenozide LC Tebufenpyrad LC Tecnazene GC Teflubenzuron LC Tefluthrin GC Terbumeton LC Terbuthylazine LC Terbuthylazine-2- hydroxy Terbuthylazinedesethyl LC LC Terbutryn LC Tetraconazole GC Tetradifon GC Tetramethrin GC Thiabendazole LC Thiacloprid LC Thiamethoxam LC Thifensulfuron-methyl LC Thiobencarb LC Edition 29, 13/04/ T Page 29 of 35

30 Animal Origin Thiodicarb LC Thionazin LC Tolclofos-methyl GC Tolyfluanid GC Triadimefon GC Triadimenol GC Tri-Allat LC Triasulfuron LC Triazophos LC Triclopyr LC Tricyclazole LC Trifloxystrobin LC Triflumizole LC Triflumizole GC Triflumuron LC Trifluralin GC Triflusulfuron-methyl LC Triticonazole LC Vamidothion LC Vinclozolin GC Zoxamide LC Edition 29, 13/04/ T Page 30 of 35

31 ANNEX 2 Quantitation of active substance in plant protection products. GC-FID & LC-DAD Range % Range % Range % Abamectin Chlorpropham Difenoconazole Acetamiprid Chlorpyrifos Diflufenican alpha-cypermethrin Chlorpyrifos-methyl Dimethenamid-P Amidosulfuron Clodinafop Dimethoate Aminopyralid Chlomazone Dimethomorph Amisulbrom Clopyralid Dimoxystrobin Asulam Cloquintocet-mexyl Diquat (dibromide) Azoxystrobin Clothianidin Diuron Bentazone Cyazofamid Dodine Bendiovalicarb-isopropyl Cycloxydim Epoxiconazole Bifenthrin Cymoxanil Esfenvalerate Bixafen Cypermethrin Ethamesulfuron-me Boscalid Chloralose Ethofumesate Bromadiolone Cyproconazole Fenpropidin Bromoxynil Cyprodinil Fenpropimorph Bupirimate d-phenotrin Fenamidone Carbendazim Daminozide Fenhexamid Carfentrazone-ethyl Deltamethrin Fenoxaprop-P (ethyl) Chloridazon Desmedipham Flazasulfuron Chlorfenapyr Dicamba Flonicamid Chlormequat Dichlobenil Florasulam Chlorothalonil Difenacoum Fluazinam Flexible Scope: Additional substances and may be added an extended in accordance with the laboratory s approved and documented procedures. For details refer to the laboratory s master list of flexible scope changes, available from the laboratory. Edition 29, 13/04/ T Page 31 of 35

32 ANNEX 2 Quantitation of active substance in plant protection products. GC-FID & LC-DAD Range % Range % Range % Fluazifop-P-butyl Ioxynil Metconazole Fludioxonil Iprodione Methiocarb Flufenacet Isoproturon Metrafenone Flumioxazin Isopyrazam Metribuzin Fluopicolide Isoxaben Metsulfuron (-methyl) Fluoxastrobin Isoxaflutole Myclobutanil Flupyrsulfuron Methyl Kresoxim Methyl Nicosulfuron Fluroxypyr lambda-cyhalothrin Octanoate Flusilazole Lenacil Oxadiazon Flutolonil Linuron Oxyfluorfen Fluxapyroxad Malathion Paclobutrazol Folpet MCPA Pencycuron Fosetyl (-aluminium) Mecoprop Pendimethalin Fosthiazate Mecoprop-P Penthiopyrad Glufosinate (- ammonium) Mefenpyr Diethyl Permethrin Glyphosate Mepiquat Chloride Phenmedipham Imazalil Mesosulfuron - Methyl Picolinafen Imidacloprid Mesotrione Picoxystrobin Imazamox Metalaxyl M Pinoxaden Imazaquin Metaldehyde Piperonyl butoxide Indoxacarb Metamitron Pirimicarb Iodosulfuron-methylsodium Metazachlor Pirimiphos-me Flexible Scope: Additional substances may be added and ranges extended in accordance with the laboratory s approved and documented procedures. For details refer to the laboratory s master list of flexible scope changes, available from the laboratory. Edition 29, 13/04/ T Page 32 of 35

33 ANNEX 2 Quantitation of active substance in plant protection products. GC-FID & LC-DAD Range % Range % Range % Prochloraz Spiroxamine Fluroxypyr-1-methyl heptyl ester Prodiamine Spirotetramat MCPB Prohexadione Calcium Sulfentrazone Trisulfuron-methyl Propamocarb Sulfosulfuron Picloram Propaquizafop Tebuconazole Fluopyram Propiconazole Tepraloxydim Halauxifen Methyl Propyzamide Terbutylazine Maleic Hydrazide Proquinazid Thiabendazole Triclopyr Prosulfocarb Thiacloprid Prothioconazole Thiamethoxan Pymetrozine Thifensulfuron (- methyl) Pyraclostrobin Thiophanate-methyl Pyrethrins Tralkoxydim Pyridate Tribenuron (-methyl) Pyrimethanil Trifloxystrobin Pyraflufen-Ethyl Trifluralin Pyroxsulam Trinexapac ethyl Quinmerac Triticonazole Quizalofop-P-ethyl ,4-DB Rimsulfuron ,4 D Silthiofam ,4-D-ethyl hexyl ester Spinosad Triclopyr butoxyethyl ester (BEE) Flexible Scope: Additional substances may be added and ranges extended in accordance with the laboratory s approved and documented procedures. For details refer to the laboratory s master list of flexible scope changes, available from the laboratory. Edition 29, 13/04/ T Page 33 of 35

34 ANNEX 3 List of Quaternary ammonium salts and other pesticides SOP 113 Fruit and Vegetables Chlormequat LC Cyromazine LC Daminozide LC Mepiquat LC Paraquat LC Flexible Scope: Additional substances may be added and ranges extended in accordance with the laboratory s approved and documented procedures. For details refer to the laboratory s master list of flexible scope changes, available from the laboratory. ANNEX 4 List of Glyphosate and Co Compounds SOP 116 AMPA (metabolite of Glyphosate) LC Ethephon LC Glufosinate LC N-acetyl Glufosinate (metabolite of Glufosinate) LC Glyphosate LC Flexible Scope: Additional substances may be added and ranges extended in accordance with the laboratory s approved and documented procedures. For details refer to the laboratory s master list of flexible scope changes, available from the laboratory. Edition 29, 13/04/ T Page 34 of 35

35 ANNEX 5 Dithiocarbamates SOP 110 Dithiocarbamates (as CS 2 ) LC Fruit and Vegetables On Formula Flexible Scope: Additional matrices may be added and ranges extended in accordance with the laboratory s approved and documented procedures. For details refer to the laboratory s master list of flexible scope changes, available from the laboratory. Amitraz and Metabolites ANNEX 6 Amitraz and its Metabolites SOP 114 Fruit, Vegetables and Honey Amitraz LC DMF LC DMPF LC Flexible Scope: Additional matrices may be added and ranges extended in accordance with the laboratory s approved and documented procedures. For details refer to the laboratory s master list of flexible scope changes, available from the laboratory. Edition 29, 13/04/ T Page 35 of 35