Performance Maintenance Protocol
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1 Performance Maintenance Protocol ACQUITY UPLC and H-Class System Sample Organizer Serial Number /Firmware Version Sample Organizer SN: Sample Organizer Firmware: Date Performer 2011 WATERS CORPORATION. ALL RIGHTS RESERVED. * * *C*
2 Performance maintenance Goal This performance maintenance protocol is a guide to performing maintenance tasks on your system. Packaged as part of the performance maintenance kit, it is intended to ensure optimum performance and an uninterrupted period of trouble-free operation. Schedule Waters recommends that performance maintenance visits be performed once a year. Systems under heavy use or using aggressive solvents will need more frequent maintenance. For detailed maintenance schedules, refer to the appropriate operator s guide(s) located on the Waters web site. Failure to follow the maintenance schedules as described in the operator s guides may result in unreliable operation and inaccurate laboratory results. For some protocols, optional tests can be performed by Waters field service engineers for added confidence and reliability. Safety considerations Some protocols may involve removing instrument covers, exposing the performer to high voltages, high currents, and moving parts. This presents risks of electric shock and/or damage to the instrument. To reduce these risks, Waters recommends that these protocols be conducted by certified Waters field service engineers, who have access to the latest information on Waters products. Waters does not advise and is not responsible for an unqualified performer initiating actions that they do not understand. If there is any doubt on the part of the performer, a Waters certified field service engineer should conduct the performance maintenance activity. Waters Quality Parts Waters designs and manufactures Waters Quality Parts to the same strict regulatory standards (ISO 9001:2000, ISO 13485:2003, and CGMP) as your high-performance Waters systems. Waters recommends using Waters Quality Parts for all maintenance activities. Failure to use Waters Quality Parts may compromise laboratory results and reliability. Customer education Waters offers several operation and maintenance courses for ACQUITY UPLC, Alliance HPLC and MS systems as well as courses designed to help you maintain professional competency and further your knowledge in Chromatography, UPLC, Informatics and Mass Spectrometry. For more information on available training courses from Waters Educational Services please visit the Waters web site. Compliance services Waters Compliance Services help you achieve and maintain the regulatory compliance of your LC and MS instruments and software with a combination of expertise, compliant-ready systems and software, and a portfolio of services to ensure that you have quality data, consistently. To learn more about these services, please visit the Waters web site. ACQUITY UPLC and H-Class Sample Organizer Performance Maintenance Protocol Page 2 of 11
3 General tasks Use the following guidelines when conducting performance maintenance visits. This information is intended to be a guide only. For example: If a particular module has been recently serviced, it may need only testing and replacement of fewer parts. Not all procedures apply to all instruments (specify NA in the Comments section if the procedure does not apply). If the instrument fails to perform adequately during initial inspection, initialization diagnostics or after post-maintenance tests, further service may be required beyond the scope of this protocol. Such service may incur additional parts and labor charges. The following table lists the general tasks to be performed during a performance maintenance visit. For detailed instructions and a list of the necessary tools, refer to the Operator s Guide located on the Waters web site. Inspect Maintenance Tasks Post Performance Maintenance Tasks Firmware Version 1 Air Intake Filter Initialization Diagnostics Fans Battery 3 Verify Shelf Sensor Amplifier Threshold Settings 3 & 7 Internal Air Regulator Pressure 3 IGUS E-Z Readychain Cable (replace every 2 yrs) 3 Verify/Adjust Z Initialization Sensor Height 5 Shelf Sag 8 Pneumatic Regulator Filter 4 Verify/Adjust XTS/YTS Hard Stops 3 Storage Shelf Retainer X/Y Transfer Shuttle Speed 2 Verify Plate Transfer Create Log Entry Shelf Sensor Amplifier Threshold Settings 3 & 6 Plate Over-travel Sensor Amplifier Threshold Settings 3 Error Logs 1 Firmware upgrades, if required, should be performed by a Waters field service engineer prior to beginning performance maintenance. Firmware upgrades may require re-qualification of the upgraded instrument if it is in a regulated environment. 2 Adjusted only by a Waters field service engineer, but can be checked in Console. 3 Checked/adjusted/replaced only by a Waters field service engineer. 4 The pneumatic regulator filter should be replaced when necessary. This filter is not included in the PM Kit. 5 Verified by Waters field service engineers only. Certain serial numbers require use of the Z tool. Adjust if necessary. 6 Perform this inspection if not replacing the IGUS E-Z Readychain. If replacing the Readychain cable, verify the settings as part of the post performance maintenance tasks. 7 Perform this post performance maintenance task only after replacing the IGUS E-Z Readychain cable. 8 Does not apply to ACQUITY H-Class Sample Organizers. ACQUITY UPLC and H-Class Sample Organizer Performance Maintenance Protocol Page 3 of 11
4 Inspect Firmware version 1. Confirm what firmware version is installed, and note it on the cover page. 2. Update if required. Firmware check complete... Fans Power supply fan 1. Observe the power supply fan on the rear of the Sample Organizer. 2. Ensure that the fan grate is clear of debris and dust. The fan should be blowing outward. 3. Clean if necessary. Power supply fan check complete... Circulating fan 1. Open the Sample Organizer door. 2. Observe the circulating fan found at the rear of the Sample Organizer compartment to see if it is turning. 3. Clean if necessary. Circulating fan check complete... ACQUITY UPLC and H-Class Sample Organizer Performance Maintenance Protocol Page 4 of 11
5 Internal air regulator pressure NOTE: The internal air regulator pressure must read 75 psi. Adjust if necessary. Internal air regulator pressure check complete... Shelf sag NOTE: Applies only to ACQUITY UPLC Sample Organizers, not H-Class. 1. Open the Sample Organizer door. 2. Observe the shelves to see that they are completely horizontal and aligned with one another. Shelf sag check complete... Storage shelf retainer Alignment of the transfer mechanisms are dependant on a LED and sensor self-alignment. This is highly dependant on the reflective metallic edge of the storage shelf retainer (spring metal device) on the back side of the shelf. 1. Remove the shelves form the Sample Organizer. 2. Locate the reflective area of the storage shelf retainer. NOTE: A good storage shelf retainer will be flush with the black shelf plate. NOTE: A damaged storage shelf retainer will have a gap between it and the black shelf plate. Any amount of gap constitutes a damaged shelf. Do not use any shelf with a damaged storage shelf retainer. Storage shelf retainer check complete... ACQUITY UPLC and H-Class Sample Organizer Performance Maintenance Protocol Page 5 of 11
6 X/Y transfer shuttle speed From the ACQUITY Console: 1. In the System tree click Sample Organizer > Interactive display. 2. Click the Control icon on the right-side of the display. 3. Click either the X or Y shuttle in the display. The X or Y motor shuttle window appears. 4. In the shuttle window, move the shuttle away and click OK. Observe the time on the timer controls. The travel time should be one to two seconds. 5. Click the shuttle icon again and bring the shuttle to its Home position. Observe the travel time. It should be between 1 and 2 seconds 6. Repeat the process for the other shuttle. X/Y transfer shuttle speed check complete... Pass Fail Shelf sensor amplifier threshold settings NOTE: It is not necessary to verify shelf sensor threshold settings prior to replacing the IGUS E-Z Readychain. If replacement is part of the performance maintenance, verify the settings as part of the post performance maintenance tasks. Amplifier threshold settings for shelf sensor are verified... Plate over-travel sensor amplifier threshold settings Amplifier threshold settings for plate over-travel sensor are verified... ACQUITY UPLC and H-Class Sample Organizer Performance Maintenance Protocol Page 6 of 11
7 Error logs 1. From the Run Samples window in Empower or the Inlet Editor window in MassLynx, click the ACQUITY Console icon in the Sample Manager control editor. 2. In the system tree click ACQUITY UPLC System. 3. Click on Logs to review error logs. Review error logs complete... ACQUITY UPLC and H-Class Sample Organizer Performance Maintenance Protocol Page 7 of 11
8 Maintenance tasks Air intake filter 1. Remove the drain tube from the air intake filter frame. 2. Pull the filter frame over the drain of the filter drain assembly. 3. Slide a new air filter and frame over the drain on the filter drain assembly. Air intake filter replaced... Battery Battery replaced... Replacing the IGUS E-Z readychain cable NOTE: Replace the IGUS E-Z Readychain cable every two years regardless of which style chain is in place. IGUS E-Z readychain replaced... Replacing the pneumatic regulator filter NOTE: Replace the pneumatic regulator as required. Pneumatic regulator filter replaced... ACQUITY UPLC and H-Class Sample Organizer Performance Maintenance Protocol Page 8 of 11
9 Post performance maintenance tasks Initialization diagnostics Initialization diagnostic checks complete.... Pass Fail Verify shelf sensor amplifier threshold settings NOTE: Perform only if the IGUS E-Z Readychain cable was replaced. Amplifier threshold settings for shelf sensor verified... Verify/adjust Z initialization sensor height NOTE: On Sample Organizers with serial numbers lower than A07UPO57M, you must replace the metal flag controlling the bottom Z sensor using the Z sensor and hard stop gauge kit (PN ). NOTE: On Sample Organizers with serial numbers lower than A07UPO57M, you must replace the upper and lower worm gear screws using the Z sensor and hard stop gauge kit (PN ). Z initialization sensor height verified... Verify/adjust XTS/YTS hard stops NOTE: The hard stop settings determine the proper distance between the XTS and YTS. This ensures proper transfer of sample plates from the Sample Organizer to the sample manager. NOTE: After setting the hard stops, you must verify proper transfer of the sample plates from the Sample Organizer to the sample manager. ACQUITY UPLC and H-Class Sample Organizer Performance Maintenance Protocol Page 9 of 11
10 Verifying/adjusting the hard stops complete... Verify plate transfer (get/put to sample manager test) 1. Power on the ACQUITY UPLC System. 2. Stock the Sample Organizer shelves with plates. NOTE: Be certain that all plates conform to SBS standards. Using non-conforming plates will jam the Sample Organizer. Also, all samples must be covered with Waters approved covers. 3. Enable control in the Interactive Display. 4. Scan and store the shelf layout. 5. From the Console, transfer a tray from the Sample Organizer shelf to the Sample Manager. 6. From the Console, transfer the tray from the Sample Manager back to the Sample Organizer. 7. Repeat the process for the remaining shelves. Plate transfer check complete.... Pass Fail Create log entries 1. In the ACQUITY UPLC Console, click on Sample Organizer in the system tree. 2. From the menu bar, click Maintain > Create log entry. The Create Log Entry dialog box appears. 3. Enter the operator s name, the date of the performance maintenance, the date the IGUS E-Z Readychain was last replaced, and any other comments. Create log entries complete... ACQUITY UPLC and H-Class Sample Organizer Performance Maintenance Protocol Page 10 of 11
11 Performance maintenance confirmation I confirm on behalf of Company Name that the performance maintenance protocol has been satisfactorily completed on: Serial Number Signed: Customer Date: I certify that the performance maintenance protocol has been successfully completed. Signed: Date: Performer Waters Global Services Waters Global Services focuses on optimizing Waters products with superior service, support, upgrades, training, and Waters Quality Parts. For more information, go to Waters Corporation 34 Maple Street Milford, MA U.S.A. Waters, ACQUITY UPLC and Waters Quality Parts are registered trademarks of Waters Corporation. The Science of What s Possible is a trademark of Waters Corporation. All other trademarks are property of their respective owners. ACQUITY UPLC and H-Class Sample Organizer Performance Maintenance Protocol Page 11 of 11
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