Systems for Mӧssbauer Spectroscopy
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1 Systems for Mӧssbauer Spectroscopy CRYO Industries of America, Inc.
2 CRYO Systems for Mӧssbauer Spectroscopy Cryo Industries of America, Inc. has numerous designs for Mӧssbauer Spectroscopy. In the most common designs, the sample is placed in exchange gas which results in ultra low vibrations at the sample! The cooling is provided by a Gifford-McMahn (GM) or pulse tube closed cycle refrigerator for long term cryogenic operation. No liquid cryogens are needed! In order to ensure that vibrations from the coldhead are not transmitted to the sample, the coldhead is isolated from the sample via a flexible bellows assembly. This flexible bellows assembly is placed between the refrigerator and a sample support flange. For additional vibration dampening the support flange is mounted to a vibration isolation stand. By working with our team of physicists and engineers, Cryo Industries is able to custom design a system that will meet all your experimental needs.
3 CRYO Model: REF-399-D22 CRYO s most popular system for Mӧssbauer Spectroscopy is the Top Loading Sample in Exchange Gas (REF-399-D22). This system is available with an integrated 10 K or 4 K coldhead. REF-399-D22 features exchange gas cooling of low thermal conductive samples. Samples can be changed in seconds without shutting off or warming the refrigerator. An independent sample mount heater results in fast thermal response. Ultra-stable variable temperature operation. The Model REF-399-D22 (Mossbauer) features low vibration through bellows, spacer and exchange gas isolation. A vibration isolation stand is included. All REF-399-D22 Systems Feature: Model: REF-399-D22 Vibration isolation bellows assembly Low Vibration Support Stand Exchange gas manifold Sample probe with rotational and linear adjustments T-style optical sample holder Clear type D mylar windows (0.010 thick) Heaters installed on coldhead and sample mount Silicon diode temperature sensor installed on sample mount Matching silicon diode temperature sensor installed on 2nd stage refrigerator 10-pin electrical sample feedthrough Sample exchange gas valve with safety pressure relief Evacuation valve with safety pressure relief
4 CRYO Model: REF-399-D22 (cont.) Pure Fe Foil 300 K, Refrigerator off FWHM = mm/s 10 K REF System Specs: <15K to 325K operating temperature range 2 Stage (GM) coldhead Model K 2nd stage cooling power K 1st stage cooling power CTI Model 8200 Water cooled compressor 18 K, Refrigerator on FWHM = mm/s Velocity (mm/s) 4 K REF System Specs: Above: Fe thin foil spectra. The line widths are at 300 K (without refrigerator) and with refrigerator. Virtually no refrigerator induced vibrations. <5K to 325K operating temperature range 2 Stage (GM) coldhead Model SRDK 408D K 2nd stage cooling power K 1st stage cooling power Water cooled compressor
5 THE INFORMATION CONTAINED IN THIS DRAWING IS THE SOLE PROPERTY OF CRYO INDUSTRIES OF AMERICA, INC., S WILLOW STREET MANCHESTER, N.H ANY REPRODUCTION IN PART OR WHOLE WITHOUT THE WRITTEN PERMISSION OF CRYO INDUSTRIES IS STRICTLY PROHIBITED Model: CF-2497-MOS Cryogen Free Superconducting Mӧssbauer Magnet System CRYO Cryo Industries innovative Cryogen Free Superconducting Magnet Mӧssbauer System is a true performance by design system. The system offers either a 5 Tesla magnet horizontal field split pair at 4.2 K with active null field positioned in each horizontal port or a 10 Tesla magnet with active null field positioned in the axial ports. The system can be configured to your experimental needs! Systems Features: HIGH CURRENT LEADS (1) BLANK PORT SAMPLE POSITION ADJUSTER SAMPLE POSITIONER ASS'Y WITH PROVISION FOR VIBRATION FREE EXTERNAL SUPPORT (1) 10 PIN ELECTRICAL FEEDTHROUGH 3-WAY EXCHANGE GAS VALVE WITH 0.37" DIA. TUBE ADAPTER AND NW25 FLANGE Cryogen Free Superconducting Magnet System with integrated optical variable temperature insert VIBRATION ISOLATED FLANGE PULSE TUBE REFRIGERATOR COLD HEAD B CONCENTRICITY SPACER FREE EXTERNAL SUPPORT VIBRATION ISOLATION SAFETY PRESSURE BELLOWS RELIEF B SECTION B-B PROVISION FOR T/C VACUUM GUAGE NOTE: THIS PORT IS ROTATED INTO VIEW (GAS INLET PORT FOR CONDENSING CHAMBER) O.D. 5 Tesla magnet horizontal field split pair at 4.2 K with active null field positioned in each horizontal port (optional 10T with active null fields positioned in axial ports) O.D. 2 K to 325 K variable temperature range CONDENSING CHAMBER + 0.5% homogeneity over central 1 cm DSV ADJUSTABLE THERMAL LINK Stray field <600 gauss at 20 cm from center 1.75 O.D. SAMPLE TUBE COPPER SAMPLE MOUNT WITH HEATER, PROVISION FOR TEMP. SENSOR AND TAPPED HOLES FOR SAMPLE MOUNTING Ø1.62 Ø2.81 (4) window ports, parallel to the magnetic field and at right angles to the magnetic field with aluminized mylar windows EPOXY SEALED MYLAR WINDOWS (4) SETS 90 APART SUPERCONDUCTING MAGNET HTS magnet current leads K pulse tube refrigerator for magnet cooling DWG. NO. CF-2497-MOS PROPRIETARY INFORMATION CRYO INDUSTRIES of America Inc S. Willow St., Manchester N.H TITLE: CRYOGEN FREE SUPER-CONDUCTING MAGNET SYSTEM Water cooled compressor
6 Cryo Industries of America, Inc South Willow Street Manchester, NH Ph: (603) Fax: (603)
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