Schedule of Accreditation issued by United Kingdom Accreditation Service 2 Pine Trees, Chertsey Lane, Staines-upon-Thames, TW18 3HR, UK

Transcription

1 Schedule of ccreditation United Kingdom ccreditation Service 2 Pine Trees, Chertsey Lane, Staines-upon-Thames, TW18 3HR, UK LS Life Sciences Limited ccredited to Units 7 & 8 Hawarden usiness Park Manor Road Off Manor Lane Hawarden Deeside CH5 3US Contact: Ian lackburne Tel: +44 (0) Fax: +44 (0) Ian.lackburne@alsglobal.com Website: Testing performed at the above address only Laboratory locations: s covered by the organisation and their relevant activities details ctivity code ddress Units 7 & 8 Hawarden usiness Park Manor Road Off Manor Lane Hawarden Deeside CH5 3US Local contact Ian lackburne Tel: +44 (0) Fax: +44 (0) Ian.lackburne@alcontrol.com Testing Chemical Microbiological Physical sbestos ddress c/o Persley Waste Water Treatment Works Woodside Persley berdeen 22 8Q Local contact: Jonathan ladon Tel: +44 (0) Jonathan.ladon@alsglobal.com Testing Chemical ssessment Manager: JL1 Page 1 of 33

2 Schedule of ccreditation United Kingdom ccreditation Service LS Life Sciences Limited ccredited to DETIL OF CCREDITTION Health and Hygiene SESTOS IN ULK MTERILS Identification of: mosite Chrysotile Crocidolite Fibrous ctinolite Fibrous nthophyllite Fibrous Tremolite HSG 248:2005 sbestos: The analysts guide for sampling, analysis and clearance procedures, by Documented In-House Method TM048 using stereo-microscopy, polarised light microscopy and dispersion staining SESTOS IN SOILS and GGREGTES (fibre screening, identification) sbestos fibre screening, identification of asbestos content: mosite Chrysotile Crocidolite Fibrous ctinolite Fibrous nthophyllite Fibrous Tremolite Documented In-House Method TM 048 using stereo microscopy, polarised light optical microscopy, phase contrast microscopy and dispersion staining SESTOS IN SOILS (fibre screening, identification and quantification) sbestos fibre screening, identification and quantification of asbestos content: mosite Chrysotile Crocidolite Fibrous ctinolite Fibrous nthophyllite Fibrous Tremolite Documented In-House Method TM 048 and TM 304 using stereo microscopy, polarised light optical microscopy, phase contrast microscopy and dispersion staining ssessment Manager: JL1 Page 2 of 33

3 Schedule of ccreditation United Kingdom ccreditation Service LS Life Sciences Limited ccredited to Chemical Tests Documented In-House Methods in the series TM 000 NTURL GS Monoethylene Glycol (MEG) in distributed Natural Gas TM 121 by Thermal desorption and GC-FID MIENT IR Volatile Organic Compounds, TM 330 based upon US EP TO-15 specifically: y GC-MS 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,2,3-Trimethylbenzene 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromoethane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,2-Dichlorotetrafluoroethane 1,3,5-Trimethylbenzene 1,3-utadiene 1,4-Dichlorobenzene 1-Propanol 2-utanone (MEK) 2-Hexanone 2-Pentanone 3-Hexanone 3-Pentanone 4-Methyl-2-pentanone cetone + Propanal cetonitrile crolein enzene enzyl Chloride romodichloromethane romoform ssessment Manager: JL1 Page 3 of 33

4 Schedule of ccreditation United Kingdom ccreditation Service LS Life Sciences Limited ccredited to Chemical Tests (cont d) Documented In-House Methods in the series TM 000 MIENT IR (cont d) Volatile Organic Compounds (cont d), specifically: TM 330 based upon US EP TO-15 by GC-MS romomethane utanal Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-dichloroethene cis-1,3-dichloropropene Cyclohexane Dichlorodifluoromethane Difluorochloromethane Ethylbenzene Hexanal Hexane Iodomethane Isobutene Isoprene m/p-xylene Methylacrolein Methylene Chloride MTE o-xylene Pentanal Pentane Styrene Tetrachloroethene Toluene trans-1,2-dichloroethene trans-1,3-dichloropropene Trichloroethene Trichlorofluoromethane Trichlorotrifluoroethane Vinyl cetate Vinyl Chloride ssessment Manager: JL1 Page 4 of 33

5 Schedule of ccreditation United Kingdom ccreditation Service ccredited to LS Life Sciences Limited SOILS Chemical Tests Exchangeable mmonium TM 024 by steam distillation and titration Water Soluble nions (2:1), specifically: Chloride romide Nitrate Sulphate TM 019 by Ion Chromatography (IC) Water soluble nions (2:1), specifically: Chloride Sulphate TM 243 by Kone analyser Total Cyanide Easily Liberated/Free Cyanide Thiocyanate TM 153 by segmented flow analyser based on WW/PH 20 th Edition - Method 4500 Extractable Phophorus TM 229 by Kone analyser (Olsen s Phosphorus) based upon The nalysis of gricultural Materials, MFF, Third edition, 1986 SOILS and SEWGE SLUDGE Hexavalent Chromium TM 151 by Kone analyser SOILS and SLUDGE cid Extractable Fluroide TM397 by ion selective electrode ssessment Manager: JL1 Page 5 of 33

6 Schedule of ccreditation United Kingdom ccreditation Service LS Life Sciences Limited ccredited to SOILS (cont d) Chemical Tests (cont d) Metals: TM 181 by ICP-OES ntimony rsenic arium eryllium oron Cadmium Cobalt Chromium Copper Iron Lead Manganese Mercury Molybdenum Nickel Selenium Strontium Thallium Tin Vanadium Zinc Water Soluble oron (10:1) TM 222 by ICP-OES Loss on ignition TM 018 by gravimetry cid Extractable Sulphate TM 221 by ICP-OES Gasoline Range Hydrocarbons: enzene Toluene Ethylbenzene o-xylene m/p-xylene MTE Petroleum Hydrocarbons in the range C8 - C40 TM 089 by Headspace and GC-FID based on USEP Methods 8020 and 602 TM 154 by Flash - GC-FID ssessment Manager: JL1 Page 6 of 33

7 Schedule of ccreditation United Kingdom ccreditation Service ccredited to LS Life Sciences Limited SOILS (cont d) Chemical Tests (cont d) Elemental Sulphur TM 136 by HPLC Sulphide TM 180 by ion selective electrode Polychlorinated iphenyls (PCs) as rochlor 1254 TM 070 by GC-MS (Ref:Modified USEP Method 8250 and 625) Volatile Hydrocarbons: TM 116 by Headspace Dichlorodifluoromethane GC-MS based on Chloromethane USEP Methods 8240, 8120, Vinyl Chloride 8020, 624, 610 and 602 romomethane Chloroethane Trichlorofluoromethane Trans-1,2-dichloroethene Dichloromethane Chloroform 1,1,1-trichloroethane 1,1-dichloropropene enzene carbon tetrachloride dibromomethane 1,2-dichloropropane bromodichloromethane trichloroethene cis-1,3dichloropropene 1,1,2-trichloroethane Toluene 1,3-dichloropropane dibromochloromethane tetrachloroethene 1,1,1,2-tetrachloroethane chlorobenzene ethylbenzene m/p-xylene romoform o-xylene 1,2,3-trichloropropane isopropylbenzene bromobenzene 2-chlorotoluene propylbenzene 4-chlorotoluene ssessment Manager: JL1 Page 7 of 33

8 Schedule of ccreditation United Kingdom ccreditation Service ccredited to LS Life Sciences Limited SOILS (cont d) Chemical Tests (cont d) Volatile Hydrocarbons: (cont d) TM 116 by Headspace 1,2,4-trimethylbenzene GC-MS based on 1,3-dichlorobenzene USEP Methods 8240, 8120, 1,4-dichlorobenzene 8020, 624, 610 and 602 sec-butylbenzene Carbon disulphide 1,1-dichloroethene 1,1-dichloroethane cis-1,2-dichloroethene bromochloromethane 2,2-dichloropropane 1,2-dibromoethane Styrene 4-isopropyltoluene 1,3,5-trimethylbenzene tert-butylbenzene 1,2-dichlorobenzene 1,2-dibromo-3-chloropropane 1,2,4-trichlorobenzene naphthalene 1,2,3-trichlorobenzene Tert-butyl methyl ether 1,2-Dichloroethane Tert-amyl methyl ether 1,1,2,2-Tetrachloroethane ph Monohydric Phenols (sum of the following): phenol cresols xylenols 2,3,5-trimethyl phenol 2-isopropylphenol Dichloromethane Extractable Compounds TM 133 using a GL ph Meter (Ref: Modified S 1377:Part 3:1990) TM 062 by HPLC TM 004 by Solvent Extraction pparatus ssessment Manager: JL1 Page 8 of 33

9 Schedule of ccreditation United Kingdom ccreditation Service ccredited to LS Life Sciences Limited SOILS (cont d) Chemical Tests (cont d) Total Organic Carbon (TOC) TM 132 by combustion method Total Carbon TM 132 by combustion method Extractable Petroleum Hydrocarbons >C10 - C40 lso: TM 061 by GC-FID based on Determination of EPH, Massachusetts Dept of EP, 1988 Polynuclear romatic TM 218 by microwave digestion Hydrocarbons (PH): and GC-MS Naphthalene 1,2 cenaphthylene 2 cenaphthene 2 Fluorene 2 Phenanthrene 1,2 nthracene 1,2 Fluoranthene 1,2 Pyrene 2 benz(a)anthracene 1,2 Chrysene 1,2 enzo(b)fluoranthene 2 enzo(k)fluoranthene 1,2 enzo(a)pyrene 1,2 Indeno(123cd)pyrene 1,2 Dibenzo(ah)anthracene 2 enzo(ghi)perylene 1,2 Sum of Dutch 10 PHs (annotated 1 ) Sum of EP 16 PHs (annotated 2 ) ssessment Manager: JL1 Page 9 of 33

10 Schedule of ccreditation United Kingdom ccreditation Service LS Life Sciences Limited ccredited to SOILS (cont d) Chemical Tests (cont d) PC congeners: TM 168 using GC-MS PC 28 PC 52 PC 77 PC 81 PC 101 PC 105 PC 114 PC 118 PC 123 PC 126 PC 138 PC 153 PC 156 PC 157 PC 167 PC 169 PC 180 PC 189 SOILS Chemical Tests Documented In-House Method to meet the requirements of the Environment gency MCERTS Performance Standard - chemical testing of soil Total cyanide Easily liberated/free cyanide Thiocyanate TM 153 by segmented flow analyser based on WW/PH 20 th Edition - Method 4500 Water Soluble oron (10:1) TM 222 by ICP-OES ssessment Manager: JL1 Page 10 of 33

11 Schedule of ccreditation United Kingdom ccreditation Service LS Life Sciences Limited ccredited to SOILS (cont d) Chemical Tests (cont d) Documented In-House Method to meet the requirements of the Environment gency MCERTS Performance Standard - chemical testing of soil (cont d) Water Soluble nions (2:1), specifically: Chloride Nitrite romide Nitrate Sulphate TM 019 by Ion Chromatography (IC) Elemental Sulphur TM 136 by HPLC rsenic eryllium Cadmium Cobalt Chromium Copper Manganese Mercury Nickel Lead Zinc Exchangeable mmonium TM 181 by ICP-OES TM 024 by steam distillation and titration ph TM 133 by automated ph probe Loss on ignition TM 018 by gravimetry cid Extractable Sulphate TM 221 by ICP-OES Sulphide TM 180 by ion selective electrode Total Organic Carbon (TOC) TM 132 by combustion method Hexavalent Chromium TM 151 by Kone analyser ssessment Manager: JL1 Page 11 of 33

12 Schedule of ccreditation United Kingdom ccreditation Service ccredited to LS Life Sciences Limited SOILS (cont d) Chemical Tests (cont d) Documented In-House Method to meet the requirements of the Environment gency MCERTS Performance Standard - chemical testing of soil (cont d) Extractable Petroleum Hydrocarbons >C10 - C40 TM 061 by GC-FID based on Determination of EPH, Massachusetts Dept of EP, 1988 Polynuclear romatic TM 218 by microwave digestion Hydrocarbons (PH): and GC-MS Naphthalene 1,2 cenaphthylene 2 cenaphthene 2 Fluorene 2 Phenanthrene 1,2 nthracene 1,2 Fluoranthene 1,2 Pyrene 2 enz(a)anthracene 1,2 Chrysene 1,2 enzo(b)fluoranthene 2 enzo(k)fluoranthene 1,2 enzo(a)pyrene 1,2 Indeno(123cd)pyrene 1,2 Dibenzo(ah)anthracene 2 enzo(ghi)perylene 1,2 Sum of Dutch 10 PHs (annotated 1 ) Sum of EP 16 PHs (annotated 2 ) ssessment Manager: JL1 Page 12 of 33

13 Schedule of ccreditation United Kingdom ccreditation Service ccredited to LS Life Sciences Limited SOILS (cont d) Chemical Tests (cont d) Documented In-House Method to meet the requirements of the Environment gency MCERTS Performance Standard - chemical testing of soil (cont d) Volatile Hydrocarbons: TM 116 by Headspace Dichlorodifluoromethane GC-MS based on USEP Vinyl Chloride Methods 8240, 8120, 8020, 624, romomethane 610 and 602 Chloroethane Trichlorofluoromethane Carbon Disulphide Tert-butyl methyl ether Trans-1,2-Dichloroethene 1,1-Dichloroethane Cis-1,2-Dichloroethene 2,2-Dichloropropane romochloromethane Chloroform 1,1,1-Trichloroethane 1,1-Dichloropropene Carbon tetrachloride 1,2-Dichloroethane enzene 1,2-Dichloropropane Dibromomethane romodichloromethane Cis-1,3-Dichloropropene Toluene 1,1,2-Trichloroethane 1,3-Dichloropropane Tetrachloroethene Dibromochloromethane 1,2-Dibromoethane Chlorobenzene 1,1,1,2-tetrachloroethane Ethylbenzene o-xylene 1,2,3-Trichloropropane Propylbenzene 1,3,5-Trimethylbenzene romoform romobenzene ssessment Manager: JL1 Page 13 of 33

14 Schedule of ccreditation United Kingdom ccreditation Service ccredited to LS Life Sciences Limited SOILS (cont d) Chemical Tests (cont d) Documented In-House Method to meet the requirements of the Environment gency MCERTS Performance Standard - chemical testing of soil (cont d) Volatile Hydrocarbons (cont d): TM 116 by Headspace 2-Chlorotoluene GC-MS based on USEP 4-Chlorotoluene Methods 8240, 8120, 8020, 624, Tert-utylbenzene 610 and Isopropyltoluene 1,3-Dichlorobenzene 1,4-Dichlorobenzene n-utylbenzene 1,2-Dichlorobenzene 1,2-Dibromo-3-Chloropropane Hexachlorobutadiene Naphthalene Gasoline Range Hydrocarbons: enzene Toluene Ethylbenzene o-xylene m/p-xylene Total Monohydric Phenols (sum of the following): phenol cresols xylenols 2,3,5-trimethyl phenol 2-isopropylphenol TM 089 Headspace GC-FID based on USEP Methods 8020 and 602 TM 062 by HPLC based on MEWM ook /Second Site Property, March 2003, Method 17.7 PC congeners: TM 168 using GC-MS PC 28 PC 52 PC 77 PC 81 PC 101 PC 105 PC 114 PC 118 PC 123 ssessment Manager: JL1 Page 14 of 33

15 Schedule of ccreditation United Kingdom ccreditation Service LS Life Sciences Limited ccredited to SOILS (cont d) Chemical Tests (cont d) Documented In-House Method to meet the requirements of the Environment gency MCERTS Performance Standard - chemical testing of soil (cont d) PC congeners (cont d): TM 168 using GC-MS PC 126 PC 138 PC 153 PC 156 PC 157 PC 167 PC 169 PC 180 PC 189 WTERS Chemical Tests Documented In-House Method Potable water (nonregulatory), Ground water, Saline water, treated and untreated sewages and trade effluent Hexavalent Chromium TM 241 by Kone nalyser Surface Water Gasoline Hydrocarbons: enzene Toluene Ethyl enzeneo-xylene m/p-xylene MTE TME TM 245 by Headspace GC-FID based on USEP Methods 8020 and 602 Ground water and Final effluent anded and Total Gasoline Hydrocarbons: C5 - C12 including bands >C6-C8 >C8-C10 >C10-C12 TM 245 by Headspace GC-FID based on USEP Methods 8020 and 602 Groundwater Total Polychlorinated iphenyl (PC) as rochlor 1254 TM 198 by GC-MS based on USEP 3535, 625 and 8250 ssessment Manager: JL1 Page 15 of 33

16 Schedule of ccreditation United Kingdom ccreditation Service ccredited to LS Life Sciences Limited WTERS (cont d) Chemical Tests (cont d) Documented In-House Method Ground water, treated and Dissolved Metals: TM 152 by ICP-MS untreated sewages, luminium trade effluent rsenic arium eryllium ismuth oron Cadmium Chromium Cobalt Copper Lead Lithium Molybdenum Nickel Manganese Phosphorus Selenium Strontium Titanium Vanadium Zinc Surface water, treated and Total Metals: TM 191 by ICP-MS untreated sewage effluents luminium and trade effluent ntimony rsenic arium eryllium ismuth oron Cadmium Chromium ssessment Manager: JL1 Page 16 of 33

17 Schedule of ccreditation United Kingdom ccreditation Service ccredited to LS Life Sciences Limited WTERS (cont d) Chemical Tests (cont d) Documented In-House Method Surface water, treated and Total Metals (cont d): TM 191 by ICP-MS untreated sewage effluents Cobalt and trade effluent (cont d) Copper Lead Lithium Manganese Molybdenum Nickel Phosphorus Selenium Strontium Thallium Tin Titanium Vanadium Zinc Surface water, treated and untreated sewage effluents and trade effluent Major Cations: Iron Magnesium Calcium Sodium Potassium Total Hardness as CaCO 3 TM 228 by ICP-OES Saline Water ntimony TM 270 by ICP-MS rsenic luminium oron Cadmium Copper Iron Lead Manganese Mercury Nickel Selenium Vanadium Zinc ssessment Manager: JL1 Page 17 of 33

18 Schedule of ccreditation United Kingdom ccreditation Service ccredited to LS Life Sciences Limited WTERS (cont d) Chemical Tests (cont d) Documented In-House Method Saline Water Major Cations: Iron Magnesium Calcium Potassium Total Hardness as CaCO 3 TM 228 by ICP-OES Surface Water, treated sewage effluent and trade effluent Total Petroleum Hydrocarbons TM 235 by Infra-red Potable water (nonregulatory), Ground water, Surface waters and Final effluent Extractable Petroleum Hydrocarbons C10 - C40 TM 172 by GC-FID Surface Waters, Ground Waters Semi-Volatile Organic Compounds (SVOCs), specifically: is(2-chloroethyl)ether 2-Chlorophenol 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene 2-Methylphenol N-nitrosodi-n-propylamine Hexachloroethane 4-Methylphenol Nitrobenzene Isophorone 2-Nitrophenol 2,4-Dimethylphenol is(2-chloroethoxy)methane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene Hexachlorobutadiene 4-Chloro-3-methylphenol 2-Methylnaphthalene 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol 2-Chloronaphthalene 2-Nitroaniline TM 176 by GC-MS ssessment Manager: JL1 Page 18 of 33

19 Schedule of ccreditation United Kingdom ccreditation Service ccredited to LS Life Sciences Limited WTERS (cont d) Chemical Tests (cont d) Surface Waters, Ground Waters (cont d) Semi-Volatile Organic Compounds (SVOCs), specifically (cont d) Dimethyl phthalate cenaphthylene 2,6-Dinitrotoluene 3-Nitroaniline cenaphthene Dibenzofuran 2,4-Dinitrotoluene Fluorene Diethyl phthalate 4-Chlorophenylphenylether 4-Nitroaniline zobenzene 4-romophenylphenylether Hexachlorobenzene Phenanthrene nthracene Carbazole Di-n-butylphthalate Fluoranthene Pyrene utylbenzylphthalate enz(a)anthracene Chrysene is(2-ethylhexyl)phthalate Di-n-octylphthalate enzo(b)fluoranthene enzo(k)fluoranthene enzo(a)pyrene Indeno(1,2,3-cd)pyrene Dibenzo(a,h)anthracene enzo(ghi)perylene TM 176 by GC-MS Surface water, Groundwater Treated and Untreated Sewages, Trade Effluent, Landfill Leachate Volatile Hydrocarbons: TM 208 by Headspace GC-MS Chloromethane Vinyl Chloride Chloroethane Dichloromethane 1,1-dichloroethane tert-butyl methyl ether ssessment Manager: JL1 Page 19 of 33

20 Schedule of ccreditation United Kingdom ccreditation Service ccredited to LS Life Sciences Limited WTERS (cont d) Chemical Tests (cont d) Surface water, Groundwater Treated and Untreated Sewages, Trade Effluent, Landfill Leachate (cont d) Volatile Hydrocarbons: (cont d) TM 208 by Headspace GC-MS cis-1,2-dichloroethene bromochloromethane chloroform 1,2-dichloroethene 1,1,1-trichloroethane 1,1-dichloropropene benzene dibromomethane trichloroethene 1,1,2-trichloroethane toluene 1,3-dichloropropane 1,2-dibromoethane tetrachloroethene chlorobenzene m/p-xylene styrene o-xylene 1,2,3-trichloropropane isopropylbenzene bromobenzene 2-chlorotoluene propylbenzene 4-chlorotoluene n-butylbenzene naphthalene Dichlorofluoromethane Trans-1,2-dichloroethene ethylbenzene 1,2-dichloropropane bromomethane Tert-amyl methyl ether Trichlorofluoromethane 1,1-dichlorethene Carbon disulphide Carbon tetrachloride romodichlormethane trans-1,3-dichloropropene Dibromchloromethane 1,1,1,2-tetrachloroethane romoform ssessment Manager: JL1 Page 20 of 33

21 Schedule of ccreditation United Kingdom ccreditation Service ccredited to LS Life Sciences Limited WTERS (cont d) Chemical Tests (cont d) Surface water, Groundwater Treated and Untreated Sewages, Trade Effluent, Landfill Leachate (cont d) Volatile Hydrocarbons: (cont d) TM 208 by Headspace GC-MS 1,3,5-trimethylbenzene Tert-butylbenzene 1,2,4-trimethylbenzene Sec-butylbenzene 4-isopropyltoluene 1,3-dichlorobenzene 1,4-dichlorobenzene 1,2,4-trichlorobenzene 1,2-dichloroethane 1,1,2,2-tetrachloroethane 1,2-dichlorobenzene Cis-1,3-dichloropropene Hexachlorobutadiene 1,2,3-trichlorobenzene 2,2-dichloropropane Groundwater, Surface Water, Landfill Leachate, Treated and Untreated Sewages, Trade Effluents, Saline Waters, Potable Waters (non-regulatory) ph TM 256 using a GL ph Meter based on S 1377:Part 3:1990 Groundwater, Landfill leachate, Treated and Untreated Sewages, Trade Effluents Dissolved Oxygen TM 187 by titration (including autotitrator) Groundwater, Landfill Leachate, Treated and Untreated Sewages, Trade Effluents, Dissolved Mercury TM 183 by Cold Vapour tomic Fluorescence Spectroscopy Ground Water, Landfill Leachate, Treated and Untreated Sewages, Trade Effluent, Potable Water (non-regulatory) Total Mercury TM 183 by Cold Vapour tomic Fluorescence Spectroscopy ssessment Manager: JL1 Page 21 of 33

22 Schedule of ccreditation United Kingdom ccreditation Service ccredited to LS Life Sciences Limited WTERS (cont d) Chemical Tests (cont d) Groundwater, Surface Water, Landfill Leachate, Treated and Untreated Sewages, Trade Effluents Chemical Oxygen Demand (COD) TM 107 using Dr Lange Kit Groundwater, Surface Water, Landfill Leachate, Treated and Untreated Sewages, Trade Effluents iochemical Oxygen Demand (OD) TM 045 based on MEWM OD5 2 nd Edition 1988/WW/ PH 20 th Edition - Method 5210 Groundwater, Surface Water, Landfill Leachate, Treated and Untreated Sewages, Trade Effluents nions: romide Chloride Fluoride Nitrate Nitrate as N and NO 3 Nitrite Nitrite as N and NO 2 Phosphate Sulphate TM 226 by ion chromatography Groundwater, Surface Water, Landfill Leachate, Treated and Untreated Sewages, Trade Effluents and Saline water lkalinity TM 043 by titration and auto-titrator based on WW/PH 20 th Edition - Method 2320/ S 2690:Part 109:1984 (Ref: S 2690) Groundwater, Surface Water, Saline water, Treated and Untreated Sewages, Trade Effluents mmonium mmoniacal Nitrogen as N and NH 3 TM 099 by Kone nalyser based on S 2690 Part 7:1968/ S 6068:Part 2.11:1984 Ground water, surface water, Untreated Sewage, Treated Sewage, Trade Effluent Total Inorganic Nitrogen TM 099 by Kone analyser (by calculation) Groundwater, Surface Water, Treated and Untreated Sewages, Trade Effluents nions: Total Oxidised Nitrogen (TON) TON as N and NO 3 TM 184 by automated discrete analyser (Kone) ssessment Manager: JL1 Page 22 of 33

23 Schedule of ccreditation United Kingdom ccreditation Service LS Life Sciences Limited ccredited to WTERS (cont d) Chemical Tests (cont d) Groundwater, Surface Water, Saline Water, Treated and Untreated Sewages, Trade Effluents Nitrite Nitrite as N and NO 2 TM 184 by Kone analyser Saline Water Total Oxidised Nitrogen (TON) TON as N and NO 3 TM 281 by Kone analyser Surface Water Nitrate as N and NO 3 TM 184 by automated discrete analyser (Kone) Groundwater, Surface Water, Saline waters, Treated and Untreated Sewages, Trade Effluents Phosphate Phosphate as P and PO 4 TM 184 by automated discrete analyser (Kone) Groundwater, Surface Water, Treated and Untreated Sewages, Trade Effluents, Chloride TM 184 by automated discrete analyser (Kone) Groundwater, Surface Water, Saline waters, Treated and Untreated Sewages, Trade Effluents, Sulphate Sulphate as S and SO 4 TM 184 by automated discrete analyser (Kone) Groundwater, Landfill Leachate, Treated and Untreated Sewages, Trade Effluents, Saline water, Potable Water (non-regulatory) Electrical Conductivity at 20 C TM 120 using a Digital Conductivity Meter based on S 2690:Part 119:1981 Ground water, surface water, Landfill leachate, Untreated Sewage, Treated Sewage, Trade Effluent Total Nitrogen TM 212 by Skalar ssessment Manager: JL1 Page 23 of 33

24 Schedule of ccreditation United Kingdom ccreditation Service LS Life Sciences Limited ccredited to WTERS (cont d) Chemical Tests (cont d) Surface Waters Electrical Conductivity at 20 C TM 120 using a Digital Conductivity Meter based on S 2690:Part 119:1981 Groundwater, Surface Water, Treated and Untreated Sewages, Trade Effluents, Saline water, Potable Water (non-regulatory) Total Suspended Solids TM 022 by Gravimetric Determination based on S 2690:Part 120:1981 Groundwater, Landfill Leachate, Treated and Untreated Sewages, Trade Effluents Total Inorganic Carbon TM 090 by TOC nalyser Groundwater, Surface Water Total Organic Carbon (low level) TM 295 by TOC nalyser Groundwater, Potable Water (non-regulatory), Landfill Leachate, Treated and Untreated Sewage Effluents Total Organic Carbon TM 090 by TOC nalyser Groundwater, Surface Water, Landfill Leachate, Treated and Untreated Sewages, Trade Effluents, Total Dissolved Solids TM 021 by Gravimetric Determination based on S 2690:Part 121:1981 or TM 123 by conductivity meter Untreated Sewage, Treated Sewage, Trade Effluent Dry Matter at 105ºC Total sh at 550ºC Documented In-House Method TM 236 The Determination of the Dry Solids residue at 105ºC and The Total sh after ignition at 550ºC ssessment Manager: JL1 Page 24 of 33

25 Schedule of ccreditation United Kingdom ccreditation Service LS Life Sciences Limited ccredited to WTERS (cont d) Chemical Tests (cont d) Trade Effluent Volatile Fatty cids: cetic acid Propionic cid Isobutyric cid utyric cid Isovaleric cid Valeric cid Caproic cid Heptanoic cid TM 201 by GC-FID Groundwater, Landfill Leachate, Treated and Untreated Sewages, Trade Effluents, Total Monohydric Phenols (sum of the following): Phenol Cresols Xylenols TM 259 by HPLC Groundwater, Surface Water Ferrous Iron TM 125 using colorimetry Groundwater, Potable Water (non-regulatory), Landfill Leachate, Treated and Untreated Sewages, Trade Effluents Total Cyanide Easily Liberated (Free) Cyanide Thiocyanate TM 227 by Segmented Flow nalyser Ground Water, Surface Water, Landfill Leachate Easily Liberatable (Free) Cyanide Total Cyanide TM 279 by SF colorimetry Groundwater, Potable Water (non-regulatory), Treated and Untreated Sewages, Trade Effluents, Fluoride TM 104 by Kone nalyser Groundwater, Potable Water (non-regulatory), Saline Water, Treated and Untreated Sewages, Trade Effluents Sulphide TM 101 by automated discrete analyser (KONE) ssessment Manager: JL1 Page 25 of 33

26 Schedule of ccreditation United Kingdom ccreditation Service ccredited to LS Life Sciences Limited WTERS (cont d) Chemical Tests (cont d) Surface Water, Ground Polynuclear romatic TM 178 by GC-MS Water, Saline Water Hydrocarbons (PH s): Naphthalene 1,2 cenaphthylene 2 cenaphthene 2 Fluorene 2 Phenanthrene 1,2 nthracene 1,2 Fluoranthene 1,2 Pyrene 2 enz(a)anthracene 1,2 Chrysene 1,2 enzo(b)fluoranthene 2 enzo(k)fluoranthene 1,2 enzo(a)pyrene 1,2 Indeno(1,2,3-cd)pyrene 1,2 Dibenzo(a,h)anthracene 2 enzo(g,h,i)perylene 1,2 Sum of Dutch 10 PHs (annotated 1 ) Sum of EP 16 PHs (annotated 2 ) Surface and Saline waters Volatile Hydrocarbons: TM 265 by Headspace GC-MS Vinyl Chloride 1,1,1,2-tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene ssessment Manager: JL1 Page 26 of 33

27 Schedule of ccreditation United Kingdom ccreditation Service ccredited to LS Life Sciences Limited WTERS (cont d) Chemical Tests (cont d) Surface and Saline waters Volatile Hydrocarbons: (cont d) TM 265 by Headspace GC-MS (cont d) 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2-Chlorotoluene 4-Chlorotoluene 4-Isopropyltoluene enzene romobenzene romochloromethane romodichloromethane romoform Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Cis-1,2-Dichloroethene Cis-1,3-Dichloropropene Dibromochloromethane Dibromomethane Ethylbenzene Hexachlorobutadiene Isopropylbenzene Naphthalene n-utylbenzene o-xylene p/m-xylene Propylbenzene Sec-utylbenzene Styrene Tert-utylbenzene Tetrachloroethene Toluene Trans-1,2-Dichloroethene Trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane ssessment Manager: JL1 Page 27 of 33

28 Schedule of ccreditation United Kingdom ccreditation Service ccredited to LS Life Sciences Limited WSTE WTERS Chemical Testing Untreated Sewage, Treated Sewage, Trade Effluent (Settled Samples) iochemical Oxygen Demand (OD) TM 045, PM 210 Chemical Oxygen Demand (COD) TM 107, PM 210 Total suspended solids TM 022, PM 210 WTERS & WSTE WTERS Total neutralised suspended solids TM 022, PM 210 Ground Water, Surface Water, Untreated Sewage, Treated Sewage, Trade Effluent Volatile suspended solids at 500 C Non-volatile suspended solids at 500 C TM 022 by gravimetric Determination based on S 2690:1981 part 120 Turbidity TM 195 by nephelometry WSTE WTERS Chemical Testing Documented In-House Method to meet the requirements of the Environment gency MCERTS Performance Standard - sampling and chemical testing of untreated sewage, treated sewage effluents and trade effluents Untreated Sewage Total Suspended Solids TM 022 by Gravimetry Treated Sewage Effluent Trade Effluent Electrical Conductivity TM 120 by Conductivity meter mmonia mmoniacal Nitrogen as N and NH 3 TM 099 by discrete colorimetric analyser ph TM 256 by ph meter Chemical Oxygen Demand (COD) TM 107 by tube test ssessment Manager: JL1 Page 28 of 33

29 Schedule of ccreditation United Kingdom ccreditation Service ccredited to LS Life Sciences Limited WSTE WTERS (cont d) Chemical Testing (cont d) Documented In-House Method to meet the requirements of the Environment gency MCERTS Performance Standard - sampling and chemical testing of untreated sewage, treated sewage effluents and trade effluents (cont d) iochemical Oxygen Demand (OD) TM 045 by DO meter Total Nitrogen TM 212 by Skalar Trade Effluent Easily Liberated (Free) Cyanide Total Cyanide TM 279 by SF colorimetry Easily Liberated (Free) Cyanide Total Cyanide Thiocyanate TM 227 by SF colorimetry Trade Effluent nions: TM 226 by Ion Chromatography Treated Sewage Effluent romide Untreated Sewage Chloride Fluoride Nitrate Nitrate as N and NO 3 Nitrite Nitrite as N and NO 2 Total Oxidised Nitrogen (TON) as N Phosphate Sulphate Untreated Sewage, Treated Sewage, Trade Effluent Dissolved Metals, specifically: luminium rsenic Cadmium Chromium Cobalt Copper Iron Lead TM 377 by ICP-MS with Kinetic Energy Discrimination (KED) ssessment Manager: JL1 Page 29 of 33

30 Schedule of ccreditation United Kingdom ccreditation Service ccredited to LS Life Sciences Limited WSTE WTERS (cont d) Chemical Testing (cont d) Documented In-House Method to meet the requirements of the Environment gency MCERTS Performance Standard - sampling and chemical testing of untreated sewage, treated sewage effluents and trade effluents (cont d) Untreated Sewage, Dissolved Metals, specifically: TM 377 by ICP-MS with Kinetic Treated Sewage, Nickel Energy Discrimination (KED) Trade Effluent Phosphorus Selenium Zinc Documented In-house methods Groundwater and Treated Sewage Effluent Perfluorinated substances (PFS): Perfluoro-n-butanoic acid Perfluoro-n-pentanoic acid Perfluoro-n-hexanoic acid Perfluoro-n-butanesulfonate Perfluoro-n-heptanoic acid 6:2 fluorotelomer sulfonate Perfluoro-n-pentanesulfonate Perfluoro-n-octanoic acid Perfluoro-n-hexanesulfonate Perfluoro-n-nonanoic acid Perfluoro-n-heptanesulfonate Perfluoro-n-decanoic acid Perfluoro-n-octanesulfonate - linear Perfluorooctane sulfonatebrached Perfluoro-n-undecanoic acid Perfluoro-n-dodecanoic acid Perfluorooctanesulfonamide Sum of 16 PFS - not including PFPS or PFDS TM 337 by LC-MS/MS ssessment Manager: JL1 Page 30 of 33

31 Schedule of ccreditation United Kingdom ccreditation Service LS Life Sciences Limited ccredited to WTERS Microbiology Testing: Enumeration of: Wastewater (Surface water, treated sewage and recreational (sea)) Total coliforms, presumptive E.coli, presumptive TM 367 based on The Microbiology of Drinking Water Part 4 (2009) and The Microbiology of Recreational Waters (2000) using membrane filtration onto MLG Wastewater (Surface water, treated sewage and recreational (sea)) Enterococci, presumptive TM 371 based on The Microbiology of Drinking water part 5 (2012) and The Microbiology of Recreational Water (2000) using membrane filtration onto S& SLUDGE Caked sewage sludge Total coliforms, confirmed E.coli, confirmed TM 368 based on The Microbiology of Sewage Sludge part 3 (2003) using Colilert ssessment Manager: JL1 Page 31 of 33

32 Schedule of ccreditation United Kingdom ccreditation Service LS Life Sciences Limited ccredited to WTERS: (cont d) Chemical nalysis Documented In-House Methods based on published procedures in the HMSO series Methods for the Examination of Waters and ssociated Materials, (MEWM), referenced by the ISN number and year or alternative reference as below: Treated Sewage Untreated Sewage, Trade Effluent and Land Leachate iochemical Oxygen Demand (OD) S5.1 based on HMSO 1988, ISN Chemical Oxygen Demand (COD) S5.2 based on ISO 15705:2002 ph S3.6.2 based on HMSO 1978, ISN lkalinity Suspended solids, Settleable and Particulate Non-Settleable Solids Test No S4.1 based on HMSO1981, ISN S3.8 based on HMSO 1980, ISN X Conductivity S3.3 based on HMSO 1978, ISN Dissolved Oxygen S3.2 based on HMSO 1979, ISN mmoniacal Nitrogen Chloride Nitrite (NO2) S2.0 and S2.3 based on HMSO 1989 (2nd Ed 1980), ISN S2.0 and S2.4 based on HMSO 1989 (1st Ed 1980), ISN S2.0 and S2.6 based on HMSO 1989, ISN ssessment Manager: JL1 Page 32 of 33

33 Schedule of ccreditation United Kingdom ccreditation Service LS Life Sciences Limited ccredited to WTERS: (cont d) Chemical nalysis (cont d) Documented In-House Methods based on published procedures in the HMSO series Methods for the Examination of Waters and ssociated Materials, (MEWM), referenced by the ISN number and year or alternative reference as below: Treated Sewage Untreated Sewage, Trade Effluent and Land Leachate (cont d) Total Oxidised Nitrogen (TON) Orthophosphate S2.0 and S2.7 based on HMSO 1989 (1st Ed 1980), ISN S2.0 and S2.8 based on HMSO 1981, ISN Nitrate (TON-NO2) S2.0, calculated parameter from methods S2.6 and 2.7 Total Dissolved Solids at 180 C S11.2 based on HMSO 1980, ISN X SLUDGE Chemical Tests Documented In-House Methods Dry Matter at 105 C S11.1 based on ISO EN 12880:1998 Potable water (nonregulatory), Groundwater and Surface water ph S3.6.2 based on HMSO 1978, ISN Potable water (nonregulatory) Chloride S2.0 and S2.4 based on HMSO 1989 (1st Ed 1980), ISN END ssessment Manager: JL1 Page 33 of 33