The University of South Africa invites suitably qualified service providers to participate in a. Public Tender Process to provide the University with

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1 The University of South Africa invites suitably qualified service providers to participate in a Public Tender Process to provide the University with CORRELATIVE XRM AND SEM MACHINES Tender Specification Document Tender Ref. No: PT2017/12 Date of Issue: August Tender Specification Correlative XRM/SEM 1

2 Table of contents 1. Overview 2. Proprietary and Confidential Information 3. Dealing with the University of South Africa 4. Registration and Compulsory information session 5. Mandatory Requirement 6. Other Requirements 7. Optional Pre-Screening 8. Tender submission closing date 9. Environmental Impact 10. Pricing 11. Value adding services/ Transformation Initiatives 12. Payment Terms 13. Sub-Contracting 14. Joint Arrangements 15. Tender Specifications 16. Evaluation Criteria 17. Annexures Pricing template A6 Supplier response template A8 Technical response template A Tender Specification Correlative XRM/SEM 2

3 1. OVERVIEW The Department of Mechanical and Industrial Engineering (DMIE) at UNISA is purchasing suitable lab equipment to meet the teaching and research requirement of the different fields in the department. In line with this DMIE has identified the need for correlative equipment comprising an XRM and an SEM machine for teaching and research in the areas of materials and manufacturing. The machines must work together in correlative research work to enable high resolution analysis of the surface and the interior of materials and engineering components. High resolution machines are required because of the application envisaged. The equipment configuration must have scope to incorporate other instruments including a FIB-SEM, Widefield microscope, and Helium Ion microscope correlative work in the future. 2. PROPRIETARY AND CONFIDENTIAL INFORMATION All material submitted in response to this tender shall become the property of Unisa. Any confidential information provided by a service provider in response to this Tender will be held in confidence and will only be used for the evaluation of this tender. 3. DEALING WITH THE UNIVERSITY OF SOUTH AFRICA Service providers must not contact any member of Unisa with respect to queries they may have with this tender. A compulsory information session will be held during which it is expected that any queries raised, will be answered. The service provider shall not disclose any such information or specification, whether explicit or implied, to any third party without the written consent from Unisa. 4. COMPULSORY REGISTRATION AND ADMITTANCE TO THE TENDER INFORMATION SESSION A non-refundable tender registration fee of R is payable by credit or debit card at the registration session. No cash payments will be accepted. Prospective tenderers must read the tender specification and bring a copy to the information session Only service provider representatives who are senior members of a relevant business unit, or are member(s) of the team responsible for tender responses, will be permitted to attend the compulsory Information session Registration Date: 01 September 2017 Registration Time: Venue: 12:00-12:30 (Latecomers will not be admitted) Unisa Science campus Boardroom NB Pityana Building Cnr Christiaan De Wet and Pioneer Avenue 2017 Tender Specification Correlative XRM/SEM 3

4 Florida Campus The above-mentioned time frames must be strictly adhered to; latecomers will not be registered and admitted to the information session. The information session will commence immediately after registration. 5. MANDATORY REQUIREMENTS Mandatory requirements will include the following and must be labelled and submitted in the following order. Failure to comply and submit any one of the documents will disqualify the submission: Annexure A1: Annexure A2: Annexure A3: Annexure A4: Attendance of compulsory information session. (Attach copy of the registration form received at the session.) Completed and signed Supplier List Application Form (F25) including the PSP form and bank account details from the bank. ( Resolution to sign on behalf of the tendering unit ( Current and valid original SARS Clearance Certificate Annexure A5: Copy of company registration documents indicating list of shareholders / Annexure A6: Annexure A7: members from CIPC / CIPRO Pricing template. (The pricing (6.1) and Bursary/Donation (6.2) templates must be completed) Financial Statements a. One set (2 years comparative figures) of the most recent audited Annual Financial Statements together with an Independent Auditor s Report or a signed letter from the Accounting Officer for Close Corporations must be submitted. The audited financial statement submitted must be within six months of the financial year-end to qualify for evaluation. A complete set of Annual Financial Statements including the following: Independent Auditor s Report (Letter from an External Accountant/Accounting Officer for Close Corporations) Statement of Comprehensive Income (Income Statement) Statement of Financial Position (Balance Sheet) Statement of Cashflows Statement of Changes in Equity Notes to the Financial Statements No summarized Financial Statements or Extracts of financial statements will be accepted. b. Where the financial statements of the holding company are submitted, a signed letter be included from the holding company, on their letterhead signed by the CEO/CFO, that they would be liable if the subsidiary defaulted. This must be attached to the financials being submitted. Failure to submit such signed letter will disqualify the tender submission. c. The financial statements should be submitted as a separate bound document. Annexure A8: Supplier Response template 2017 Tender Specification Correlative XRM/SEM 4

5 Annexure A9: Technical Response template must be completed. Annexure A10: Unisa Terms and Conditions must be completed 6. OTHER REQUIREMENTS Supplier documents and information Annexure B1: A valid B-BBEE certificate or proof of exemption from an accredited SANAS / IRBA verification agency / auditor. An affidavit certifying their total annual income and level of black ownership will be sufficient for EMEs and QSEs. Failure to submit the above will result in a zero score for B-BBEE. Annexure B2: Operating manual for the equipment being tendered on Annexure B3: Brochure for the equipment being tendered on Annexure B4: Draft service agreement Note: All documents submitted in support of this tender must be the documents of the tendering unit and may not pertain to different companies or units within a group. As an example, a tenderer cannot submit its own B-BBEE certificate, but the SARS certificate of its holding company. 7. OPTIONAL PRE-SCREENING OF MANDATORY SUPPORTING DOCUMENTATION A non-compulsory pre-screening opportunity will be available to assist service providers to ensure that their documentation meets the commercial mandatory requirements prior to the closing date of the tender responses. The pricing requirement does not form part of this opportunity and must only be submitted on the closing date. The Supply Chain Management Directorate will be available on: Date: 13 September 2017 Time: 12:00 14:00 Venue: NB Pityana Building. Second Floor, Room 2-19, Cnr Christiaan De Wet and Pioneer Avenue, Unisa Science Campus, Florida, Roodepoort 8. CLOSING DATE The original and a soft copy of the tender must be submitted into the official tender box in a sealed envelope located in the NB Pityana Building, Ground Floor, Roodepoort, Florida Campus, Christiaan De Wet and Pioneer Avenue. Please quote the tender reference number PT2017/12 on the sealed envelope. Closing date: 19 September Tenders submitted late will not be accepted or considered. Points will be awarded for Broad-Based Black Economic Empowerment. The decision of the UNISA Management Committee on awarding a tender is final. Unisa reserves the right to appoint, contract with and monitor the performance of any service provider it deems will offer the best service in line with its requirements, although it may not necessarily be the lowest Tenderer. Unisa also reserves the right, in its sole discretion, to re-advertise, not to retender or not to award the tender Tender Specification Correlative XRM/SEM 5

6 The tender awarded will be conditional and subject to successful negotiations and signing of a written contract, failing which Unisa reserves the right to withdraw the tender and to award the tender to another Tenderer without repeating the process. 9. ENVIRONMENTAL IMPACT Set out the detail of the environmental impact of the activities relating to the agreement/contract and the waste generated as a result thereof. Attach a detailed implementation plan by the contractor and/or the person(s) responsible for implementing the agreement/contract, indicating how the environmental impact and the waste generated will be minimized, mitigated and managed 10. PRICING The tenderer must state whether the price quoted is fixed for the duration of the agreement or whether the price is subject to escalation. In the absence of an indication in this regard the price will be considered as fixed for the full period of the agreement. All pricing must be quoted in South African Rand (ZAR) including VAT. Foreign exchange rate used to be indicated (if applicable). The pricing must remain valid for 90 days from the closing date of the tender. Pricing / costing template must be completed (Annexure A6) Any pricing not included in the pricing template will not be considered. Prices charged by the supplier for goods delivered and services performed under the contract shall not vary from the prices quoted by the supplier in his tender, and any variance will render the contract null and void. 11. VALUE-ADDING SERVICES/TRANSORMATION INITIATIVES Service providers are encouraged to indicate what other value adding services the University may reasonably expect to flow from their appointment. A monetary value needs to be associated to value add being proposed. The following are some examples of what can be provided / expected: student bursaries and/or donations to Unisa Foundation etc 12. PAYMENT TERMS The payment terms of the University are 30 days after receipt of goods and services and upon receipt of the required documentation. No upfront payments will be considered. 13. SUB-CONTRACTING No subcontracting will be considered for this tender 14. JOINT ARRANGEMENTS 2017 Tender Specification Correlative XRM/SEM 6

7 No joint venture arrangements will be considered for this tender 15. TENDER SPECIFICATION The correlative system must consist of an XRM machine and an SEM machine that are configured to work together in a correlative set-up. The XRM and SEM machines must be powerful standalone machines with very high resolution up to submicron levels. The research interests of the department of Mechanical and Industrial Engineering is mainly in the analysis of engineering materials, manufactured products and engineered components. The machines must be versatile with applications in the areas related to metals, metal alloys, super-alloys and advanced materials including ceramics, metal matrix composites, Nano composites and fibre-reinforced plastics. The tendering company must be responsible for supply the correlative machines (XRM and SEM) together with the correlative software and also to set up the machines for correlative work. The system must be able to work with images from different sources work with different environments from different sources incorporate the data from the different sources into a single image and process it for better presentation The correlative system provided must be able to incorporate other correlative instruments for further upgrades in the future when required. Other possible instruments that can be incorporated in the future include electron microscopes (FIB-SEM), light microscopes (Widefield, confocal and Helium Ion microscopes and optical microscopes (stereo microscope, inverted microscope and compound microscope). The analysis software associated with equipment must have multi-user licences. The system must have automatic data collection, analysis and reporting. The original Equipment Manufacturer must be ISO 9001 registered Only companies that are specialists in XRM and SEM equipment will be allowed to tender for this project. The company must have at least 1 local qualified technical service engineer/technician for both instruments (XRM and SEM) for maintenance of the machines. Additionally there may be any other number of engineers/technicians that are trained on either XRM or SEM only. There must be at least one locally based applications specialist for assistance in operating both machine and for support of the research efforts of the department. Installation and commissioning must be done at the UNISA Florida Campus. The specifications of the XRM and SEM instruments required are given in sections 12.1 and 12.2 below Tender Specification Correlative XRM/SEM 7

8 15.1. XRM Machine The XRM machine must be designed for correlation with SEM, FIB-SEM, light microscopes and capability of multiple contrast modes: 1) absorption, 2) phase propagation, 3) diffraction. It must be equipped with tools with ability to: maintain high resolution as the source is moved away from the sample in in-situ tests investigate fracture and other effects of in-situ heating, cooling, tension and compression on a sample distinguish between elements that are close on the periodic table and are difficult to distinguish with colour coding by using different imaging conditions in a single scan optionally operate at either, high resolution (image quality) or high speed (throughput) scan samples that is larger than the field of view of the instrument by combining high resolution scans of smaller views perform 4D analysis, that is evolution of 3D grain structure over time perform surface reconstruction for 2D 3D and 4D image analysis including visualisation and measurement of properties including areas, volumes, counts, distributions and orientations study of very wide range of sample sizes by use of geometric and optical magnification perform interactive labelling inspect multi-planar slices perform high quality surface rendering measure distances, angles, and paths, perform high definition volume rendering perform statistical analysis using histogram tools measure min, max, and mean intensity values and standard deviation study volume metrics including porosity, particle/ void analysis scan large images and to zoom on areas of interest for high resolution results employ image morphology manipulation including closing, opening, erosion, distance transform The machine must have capability, when fitted with the right tool configuration, to: load 10 or more samples and automatically running them one at a time 2017 Tender Specification Correlative XRM/SEM 8

9 perform non-destructive analysis through diffraction contrast tomography for studying 3D crystallographic grain orientation in materials including metals like steel and titanium Basic XRM operator training and advanced applications training should be provided together with further training on correlation between XRM and SEM. User guide and operation manuals must be provided. The company must give proof of correlative work done using the system proposed X-ray source High transmission sealed X-ray source: Power rating in the range: 8 W or more Voltage rating (higher voltage achievable): 150 kv or more AutoFilter changer; Number of filters: 10 or more filters Resolution Spatial resolution: 0.9 microns (0.9μm or 900 nm) or less Achievable Voxel size (nominal resolution or detail detectability): 90 nm (0.09μm) or less Sample stages The equipment should be able to load light to heavy samples and small to large samples. Relevant sample holders must be provided. Allowable heavy sample mass: 13 kg or more Allowable large sample dimensions (diameter x height): 200 mm x 50 mm or more In-situ thermo-mechanical testing stage There must be a stage(s) for testing samples under thermo-mechanical loads. The stage must allow heating, cooling, and application of tensile or compressive loads during the testing of the sample Tensile and compressive loading capacity: 4.5 kn or more Temperature range: 10 o C to 150 o C or greater range Resolution at 50 mm working distance for this stage: 1.2 μm or less Detector(s) The machine must come with several detectors including a camera and at least one detector 2017 Tender Specification Correlative XRM/SEM 9

10 Camera A large field of view camera should be provided A High contrast High resolution detector The detector should have one or more objectives giving the maximum resolution as in Provision to incorporate a flat panel detector Additionally the machine must either be supplied with a flat panel detector or must have the provision for incorporating a flat panel detector that is able to scan very large samples Provision for an Auto loading stage The system must have the capacity for an auto-loading stage for future upgrade. The number of samples that can be loaded at a time with the auto-loading stage must be 10 or more. This must be optionally supplied with the machine or be available for upgrade at a later stage. Number of samples that can be loaded at a time for automatic operation: 10 or more Software packages Mandatory software Data acquisition software 3D Tomography image reconstruction software 3D viewer software Wide field of view imaging software Correlative software between SEM and other equipment Software capability for later upgrade Diffraction /crystallographic phase orientation analysis Flat panel software for rapid scanning of flat surfaces and zooming on areas of interest 15.2 SEM machine The SEM required must be able to operate in High vacuum (HV), variable pressure (VP) up to at least 380 Pa and extended pressure modes. The system must be able to combine several images taken by different detectors into an interactive image with complementing information. The equipment must be 2017 Tender Specification Correlative XRM/SEM 10

11 fitted with co-planar EDS and EBSD systems with capability for simultaneous data collection from both systems. In addition a STEM detector must be supplied for transmission mode analysis. The system must be able to: allow different section of the image to be magnified compared to the rest the rest of the sample. A second monitor should be supplied to view different sections at different magnification allow a point or area to be brought into the main view define and free-form regions of interest (ROI) from batches of samples for unattended automated image acquisition recommend the best imaging conditions basing on sample type and to create interactive maps of sample. A FIB-SEM is required or the SEM must have the port for the FIB column for future upgrade. Training covering the each component of the SEM set-up including SEM, EDS, EBSD, STEM and on correlation between SEM and XRM is required Resolution Resolution at 30 kv SE: 3.2 nm or less Resolution at 30 kv SE with variable pressure: 3.6 nm or less Resolution at 3 kv SE: 12 nm or less Resolution at 1 kv SE: 22 nm or less Magnification range Magnification range: 15x to 900,000x (15x to 0.9Mx) or greater range Field of view at Analytic Working Distance: 6 mm Accelerating voltage and probe current: Accelerating voltage rating: 30 kv Probe current Current rating: 10 μa or less Pressure range: Variable Pressure range: up to 380 Pa 2017 Tender Specification Correlative XRM/SEM 11

12 Sample stage Load capacity: 0.5 kg or heavier Sample dimensions (Diameter x Height): 230 mm x 120 mm Detectors to be installed when the machine is supplied Secondary electron detector for detailing of surfaces in high vacuum modes Variable Pressure Secondary Electron Detector with enhanced contrast for imaging High Definition Backscattered Electron: High and low voltage surface detailing with enhanced topographical detail using shadow mode Integrated Cathodoluminescence Detector for characterisation for luminescence materials STEM detector for scanning and transmission modes EDS for Elemental analysis (elemental spectra, elemental maps, and phase maps) EBSD for Analyse the crystal structure analysis CHAMBERSCOPE CCD cameras for placement and observation of the sample in the chamber; with picture in picture presentation PC for SEM Large storage space is required due to the high resolution image data to be stored. It must have the following base specifications. Processor: Quad-core or better, 2 x 4 TB plus 480 GB SSD, 2GB video, 8GB RAM or better SEM software: SEM Software packages Data acquisition, processing, presentation, storage, reporting software EDS, EBSD, STEM software Correlative software between SEM and other equipment 2017 Tender Specification Correlative XRM/SEM 12

13 16. EVALUATION CRITERIA Stage 1 Functional evaluation: DESCRIPTION POINTS Phase 1- Technical Mandatory evaluation There must be 100 % compliance with the critical specifications as indicated in the Tender specification document. Phase 2- Technical evaluation Tenderers must score at least 75% or more to proceed to the next phase Phase 3 Capacity and training To be evaluated using response template Tenderers must score at least 75% or more to proceed to the next stage Stage 2: ITEMS POINTS 1. Price B-BBEE points will be awarded as follows: 25 B-BBEE Level (Certificate to be used) (10) B-BBEE/Transformation initiatives: Refer Annex 6.2 (15) 3. Technical (score to be carried from phase 2) Tender Specification Correlative XRM/SEM 13

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