WASHINGTON STATE DEPARTMENT OF ECOLOGY
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1 WASHINGTON STATE DEPARTMENT OF ECOLOGY ENVIRONMENTAL LABORATORY ACCREDITATION PROGRAM SCOPE OF ACCREDITATION AmTest Laboratories Kirkland, WA is accredited for the analytes listed below using the methods indicated. Full accreditation is granted unless stated otherwise in a note. EPA is the U.S. Environmental Protection Agency. SM is "Standard Methods for the Examination of Water and Wastewater." SM refers to EPA approved method versions. ASTM is the American Society for Testing and Materials. USGS is the U.S. Geological Survey. AOAC is the Association of Official Analytical Chemists. Other references are described in notes. Drinking Water Turbidity EPA 180.1_2_1993 Bromide Chloride Fluoride Nitrate Nitrite Sulfate Cyanide, Total EPA 335.4_1_1993 Nitrate EPA 353.2_2_1993 Color SM 2120 B-2011 Alkalinity SM 2320 B-2011 Specific Conductance SM 2510 B-2011 Solids, Total Dissolved SM 2540 C-2011 Cyanide, Total SM 4500-CN E-2011 Nitrite SM 4500-NO2 B-2011 Orthophosphate SM 4500-P E-2011 Total Organic Carbon SM 5310 B-2011 UV Absorbing Organics SM 5910 B-00 Calcium Hardness, Total (as CaCO3) Iron Page 1 of 19
2 Drinking Water Magnesium Manganese Silica Sodium Zinc Aluminum Antimony Arsenic Barium Beryllium Cadmium Chromium Copper Lead Manganese Nickel Selenium Silver Thallium Zinc Mercury Bromoacetic acid Bromochloroacetic acid Chloroacetic acid Dibromoacetic acid Dichloroacetic acid Total haloacetic acids (HAA5) Trichloroacetic acid Bromodichloromethane Bromoform Chlorodibromomethane Chloroform EPA 245.1_3_1994 EPA 552.2_1_1995 EPA 552.2_1_1995 EPA 552.2_1_1995 EPA 552.2_1_1995 EPA 552.2_1_1995 EPA 552.2_1_1995 EPA 552.2_1_1995 EPA 524.2_4.1_1995 EPA 524.2_4.1_1995 EPA 524.2_4.1_1995 EPA 524.2_4.1_1995 Page 2 of 19
3 Drinking Water Total Trihalomethanes Heterotrophic Bacteria Fecal coliform-count Total coliforms-count Total coli/e.coli - detect EPA 524.2_4.1_1995 SM 9215 B (PCA) SM 9222 B+9221 E1 (mendo/eccounts) SM 9222 B+9221 E1 (mendo/eccounts) SM 9222 B+9221 F (mendo/ec Mug- PA) Fecal coliform-count SM 9222 D (mfc) 06 Total coli/e.coli - detect SM9223 B Colisure (PA) Non-Potable Water n-hexane Extractable Material (O&G) EPA 1664A_1_1999 Turbidity EPA 180.1_2_1993 Bromide Chloride Fluoride Nitrate Nitrite Sulfate Cyanide, Total EPA 335.4_1_1993 Ammonia EPA 350.1_2_1993 Nitrogen, Total Kjeldahl EPA 351.2_2_1993 Nitrate + Nitrite EPA 353.2_2_1993 Chemical Oxygen Demand (COD) EPA 410.4_2_1993 Phenolics, Total EPA 420.4_1_1993 Color SM 2120 B-2011 Alkalinity SM 2320 B-2011 Specific Conductance SM 2510 B-2011 Solids, Total SM 2540 B-2011 Solids, Total Dissolved SM 2540 C-2011 Solids, Total Suspended SM 2540 D-2011 Chromium, Hexavalent SM 3500-Cr B-2011 Page 3 of 19
4 Non-Potable Water Cyanide, Total SM 4500-CN E-2011 Cyanides, Amenable to Chlorination SM 4500-CN G-2011 Nitrite SM 4500-NO2 B-2011 Dissolved Oxygen SM 4500-O C-2011 Orthophosphate SM 4500-P E-2011 Phosphorus, total SM 4500-P F-2011 Sulfide SM 4500-S2 D-2011 Biochemical Oxygen Demand (BOD) SM 5210 B-2011 Total Organic Carbon SM 5310 B-2011 Nonionic Surfactants as CTAS SM 5540 B-93 Anionic Surfactants (MBAS) SM 5540 C-2011 UV Absorbing Organics SM 5910 B-00 Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Hardness, Total (as CaCO3) Iron Lead Magnesium Manganese Molybdenum Nickel Potassium Selenium Page 4 of 19
5 Non-Potable Water Silica Silver Sodium Strontium Thallium Tin Titanium Vanadium Zinc Aluminum Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Manganese Molybdenum Nickel Selenium Silver Thallium Vanadium Zinc Mercury EPA 245.1_3_1994 4,4'-DDD EPA 608 4,4'-DDE EPA 608 4,4'-DDT EPA 608 Aldrin EPA 608 Page 5 of 19
6 Non-Potable Water alpha-bhc (alpha-hexachlorocyclohexane) EPA 608 alpha-chlordane EPA 608 Aroclor-1016 (PCB-1016) EPA 608 Aroclor-1221 (PCB-1221) EPA 608 Aroclor-1232 (PCB-1232) EPA 608 Aroclor-1242 (PCB-1242) EPA 608 Aroclor-1248 (PCB-1248) EPA 608 Aroclor-1254 (PCB-1254) EPA 608 Aroclor-1260 (PCB-1260) EPA 608 beta-bhc (beta-hexachlorocyclohexane) EPA 608 delta-bhc EPA 608 Dieldrin EPA 608 Endosulfan I EPA 608 Endosulfan II EPA 608 Endosulfan sulfate EPA 608 Endrin EPA 608 Endrin aldehyde EPA 608 Endrin ketone EPA 608 gamma-bhc (Lindane, gamma-hexachlorocyclohexane) EPA 608 Heptachlor EPA 608 Heptachlor epoxide EPA 608 Methoxychlor EPA 608 2,4,5-T EPA ,4-D EPA ,4-DB EPA Dalapon EPA Dicamba EPA Dichloroprop (Dichlorprop) EPA Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP) EPA MCPA EPA MCPP EPA Page 6 of 19
7 Non-Potable Water Silvex (2,4,5-TP) EPA ,1,1,2-Tetrachloroethane EPA 624 1,1,1-Trichloroethane EPA 624 1,1,2,2-Tetrachloroethane EPA 624 1,1,2-Trichloroethane EPA 624 1,1-Dichloroethane EPA 624 1,1-Dichloroethylene EPA 624 1,2,3-Trichloropropane EPA 624 1,2-Dibromo-3-chloropropane (DBCP) EPA 624 1,2-Dibromoethane (EDB, Ethylene dibromide) EPA ,2-Dichlorobenzene EPA 624 1,2-Dichloroethane (Ethylene dichloride) EPA 624 1,2-Dichloropropane EPA 624 1,3-Dichlorobenzene EPA 624 1,4-Dichlorobenzene EPA Butanone (Methyl ethyl ketone, MEK) EPA Hexanone EPA Methyl-2-pentanone (MIBK) EPA 624 Acetone EPA 624 Acrylonitrile EPA Benzene EPA 624 Bromochloromethane EPA 624 Bromodichloromethane EPA 624 Bromoform EPA 624 Carbon dioxide EPA 624 Carbon tetrachloride EPA 624 Chlorobenzene EPA 624 Chlorodibromomethane EPA 624 Chloroethane (Ethyl chloride) EPA 624 Chloroform EPA 624 cis-1,2-dichloroethylene EPA 624 cis-1,3-dichloropropene EPA 624 Page 7 of 19
8 Non-Potable Water Dibromomethane EPA Ethylbenzene EPA 624 Iodomethane (Methyl iodide) EPA 624 m+p-xylene EPA 624 Methyl bromide (Bromomethane) EPA 624 Methyl chloride (Chloromethane) EPA 624 Methylene chloride (Dichloromethane) EPA 624 o-xylene EPA 624 Styrene EPA 624 Tetrachloroethylene (Perchloroethylene) EPA 624 Toluene EPA 624 trans-1,2-dichloroethylene EPA 624 trans-1,3-dichloropropylene EPA 624 trans-1,4-dichloro-2-butene EPA 624 Trichlorofluoromethane (Freon 11) EPA 624 Vinyl acetate EPA 624 Vinyl chloride EPA ,2,4-Trichlorobenzene EPA 625 1,2-Dichlorobenzene EPA 625 1,2-Diphenylhydrazine EPA 625 1,3-Dichlorobenzene EPA 625 1,4-Dichlorobenzene EPA 625 2,4,5-Trichlorophenol EPA 625 2,4,6-Trichlorophenol EPA 625 2,4-Dichlorophenol EPA 625 2,4-Dimethylphenol EPA 625 2,4-Dinitrophenol EPA 625 2,4-Dinitrotoluene (2,4-DNT) EPA 625 2,6-Dinitrotoluene (2,6-DNT) EPA Chloronaphthalene EPA Chlorophenol EPA 625 Page 8 of 19
9 Non-Potable Water 2-Methylnaphthalene EPA Methylphenol (o-cresol) EPA Nitroaniline EPA Nitrophenol EPA 625 3,3'-Dichlorobenzidine EPA Nitroaniline EPA 625 4,6-Dinitro-2-methylphenol EPA Bromophenyl phenyl ether (BDE-3) EPA Chloro-3-methylphenol EPA Chloroaniline EPA Chlorophenyl phenylether EPA Methylphenol (p-cresol) EPA Nitroaniline EPA Nitrophenol EPA 625 Acenaphthene EPA Acenaphthylene EPA Aniline EPA 625 Anthracene EPA Azobenzene EPA 625 Benzidine EPA 625 Benzo(a)anthracene EPA Benzo(a)pyrene EPA Benzo(g,h,i)perylene EPA Benzo(k)fluoranthene EPA Benzo[b]fluoranthene EPA 625 Benzoic acid EPA 625 Benzyl alcohol EPA 625 bis(2-chloroethoxy)methane EPA 625 bis(2-chloroethyl) ether EPA 625 bis(2-chloroisopropyl) ether EPA 625 bis(2-ethylhexyl) phthalate (DEHP) EPA 625 Butyl benzyl phthalate EPA 625 Page 9 of 19
10 Non-Potable Water Carbazole EPA 625 Chrysene EPA Dibenz(a,h) anthracene EPA Dibenzofuran EPA 625 Diethyl phthalate EPA 625 Dimethyl phthalate EPA 625 Di-n-butyl phthalate EPA 625 Di-n-octyl phthalate EPA 625 Fluoranthene EPA Fluorene EPA Hexachlorobenzene EPA 625 Hexachlorobutadiene EPA 625 Hexachlorocyclopentadiene EPA 625 Hexachloroethane EPA 625 Indeno(1,2,3-cd) pyrene EPA Isophorone EPA 625 Naphthalene EPA Nitrobenzene EPA 625 N-Nitrosodimethylamine EPA 625 N-Nitroso-di-n-propylamine EPA 625 N-Nitrosodiphenylamine EPA 625 Pentachlorophenol EPA 625 Phenanthrene EPA Phenol EPA 625 Pyrene EPA Heterotrophic Bacteria Heterotrophic Bacteria Fecal coliform-count Total coliforms-count E.coli-count SM 9215 B (PCA) SM 9215 D (R2A) SM 9221 B+E1+C (LTB/BGB/EC- MPN) SM 9221 B+E1+C (LTB/BGB/EC- MPN) SM 9221 B+F+C (LTB/BGB/EC Mug- Page 10 of 19
11 Non-Potable Water Total coliforms-count Fecal coliform-count Fecal coliform-count Total coliforms-count E.coli-count Total coliforms-count MPN) SM 9221 B+F+C (LTB/BGB/EC Mug- MPN) SM 9221 E2+C (A1-MPN) SM 9222 B+9221 E1 (mendo/eccounts) SM 9222 B+9221 E1 (mendo/eccounts) SM 9222 B+G (mendo/na Mugambient water only) SM 9222 B+G (mendo/na Mugambient water only) Fecal coliform-count SM 9222 D (mfc) 06 Enterococci SM 9230 C3a (me-mf) Solid and Chemical Materials Chromium, Hexavalent EPA 7196A_1_1992 Cyanide, Total EPA 9012 B-04 Cyanide, Free EPA 9016 ph EPA 9045D_2002 Chloride EPA 9056A_(02/07) Fluoride EPA 9056A_(02/07) Sulfate EPA 9056A_(02/07) Total organic carbon EPA 9060A_1_2004 Phenolics, Total EPA 9065_1986 Cation Exchange Capacity EPA 9081 Solids, Total SM 2540 B-2011 Solids, Total, Fixed and Volatile SM 2540 G-2011 Cyanides, Amenable to Chlorination SM 4500-CN G-2011 Ammonia SM 4500-NH3 E-2011 Nitrite SM 4500-NO2 B-2011 Nitrate + Nitrite SM 4500-NO3 F Nitrogen, Total Kjeldahl SM 4500-Norg C-2011 Page 11 of 19
12 Solid and Chemical Materials Phosphorus, total SM 4500-P F-2011 Sulfide SM 4500-S2 D-2011 Aluminum Antimony Arsenic Barium Beryllium Boron Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Molybdenum Nickel Potassium Selenium Silica Silver Sodium Strontium Thallium Tin Titanium Vanadium Zinc Aluminum Antimony Page 12 of 19
13 Solid and Chemical Materials Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Lead Manganese Molybdenum Nickel Selenium Silver Thallium Vanadium Zinc Mercury 4,4'-DDD 4,4'-DDE 4,4'-DDT Aldrin alpha-bhc (alpha-hexachlorocyclohexane) alpha-chlordane beta-bhc (beta-hexachlorocyclohexane) Chlordane (tech.) delta-bhc Dieldrin Endosulfan I Endosulfan II Endosulfan sulfate EPA 7471B_(2/07) Page 13 of 19
14 Solid and Chemical Materials Endrin Endrin aldehyde Endrin ketone gamma-bhc (Lindane, gamma-hexachlorocyclohexane) Heptachlor Heptachlor epoxide Methoxychlor Aroclor-1016 (PCB-1016) EPA 8082A_(2/07) Aroclor-1221 (PCB-1221) EPA 8082A_(2/07) Aroclor-1232 (PCB-1232) EPA 8082A_(2/07) Aroclor-1242 (PCB-1242) EPA 8082A_(2/07) Aroclor-1248 (PCB-1248) EPA 8082A_(2/07) Aroclor-1254 (PCB-1254) EPA 8082A_(2/07) Aroclor-1260 (PCB-1260) EPA 8082A_(2/07) 2,4,5-T EPA 8151A_(1/98) 1 2,4-D EPA 8151A_(1/98) 1 2,4-DB EPA 8151A_(1/98) 1 5-Hydroxydicamba EPA 8151A_(1/98) 1 Dalapon EPA 8151A_(1/98) 1 DCPA di acid degradate EPA 8151A_(1/98) 1 Dicamba EPA 8151A_(1/98) 1 Dichloroprop (Dichlorprop) EPA 8151A_(1/98) 1 Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP) EPA 8151A_(1/98) 1 MCPA EPA 8151A_(1/98) 1 MCPP EPA 8151A_(1/98) 1 Silvex (2,4,5-TP) EPA 8151A_(1/98) 1 Diesel range organics (DRO) WDOE NWTPH-Dx_(1997) 2 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane Page 14 of 19
15 Solid and Chemical Materials 1,1-Dichloroethylene 1,2-Dibromo-3-chloropropane (DBCP) 1,2-Dichlorobenzene 1,2-Dichloroethane (Ethylene dichloride) 1,2-Dichloropropane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2-Butanone (Methyl ethyl ketone, MEK) 2-Hexanone 4-Methyl-2-pentanone (MIBK) Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane (Ethyl chloride) Chloroform cis-1,2-dichloroethylene cis-1,3-dichloropropene Ethylbenzene Iodomethane (Methyl iodide) m+p-xylene Methyl bromide (Bromomethane) Methyl chloride (Chloromethane) Methylene chloride (Dichloromethane) o-xylene Styrene Page 15 of 19
16 Solid and Chemical Materials Tetrachloroethylene (Perchloroethylene) Toluene trans-1,2-dichloroethylene trans-1,3-dichloropropylene trans-1,4-dichloro-2-butene Trichloroethene (Trichloroethylene) Trichlorofluoromethane (Freon 11) Vinyl acetate Vinyl chloride Xylene (total) 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,2-Diphenylhydrazine 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene (2,4-DNT) 2,6-Dinitrotoluene (2,6-DNT) 2-Chloronaphthalene 2-Chlorophenol 2-Methylnaphthalene 2-Methylphenol (o-cresol) 2-Nitroaniline 2-Nitrophenol 3,3'-Dichlorobenzidine 3-Nitroaniline 4,6-Dinitro-2-methylphenol 4-Bromophenyl phenyl ether (BDE-3) Page 16 of 19
17 Solid and Chemical Materials 4-Chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenyl phenylether 4-Methylphenol (p-cresol) 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Anthracene Azinphos-methyl (Guthion) Azobenzene Benzidine Benzo(a)anthracene Benzo(a)pyrene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzo[b]fluoranthene Benzoic acid Benzyl alcohol bis(2-chloroethoxy)methane bis(2-chloroethyl) ether bis(2-chloroisopropyl) ether Butyl benzyl phthalate Carbazole Chlorpyrifos Chrysene Di(2-ethylhexyl)phthalate Dibenz(a,h) anthracene Dibenzofuran Diethyl phthalate Dimethyl phthalate Page 17 of 19
18 Solid and Chemical Materials Di-n-butyl phthalate Di-n-octyl phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd) pyrene Isophorone Naphthalene Nitrobenzene N-Nitrosodimethylamine N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Phorate Pyrene Gasoline range organics (GRO) WDOE NWTPH-Gx_(1997) 2 Salmonella Fecal coliform-count Total coliforms-count E.coli-count Total coliforms-count Fecal coliform-count Particle Size Distribution Ignitability EPA 1682 Biosolids (MSRV) SM 9221 B+E1+C (LTB/BGB/EC- MPN) SM 9221 B+E1+C (LTB/BGB/EC- MPN) SM 9221 B+F+C (LTB/BGB/EC Mug- MPN) SM 9221 B+F+C (LTB/BGB/EC Mug- MPN) SM 9221 E2+C (A1-MPN) ASTM D422 EPA 1020B Page 18 of 19
19 Accredited Parameter Note Detail (1) Provisional accreditation pending submittal of acceptable MDL study. (2) Washington Department of Ecology Analytical Methods for Petroleum Hydrocarbons, Publication Number ECY , June (3) Includes accreditation for selective ion monitoring (SIM).(4) Provisional accreditation pending submittal of acceptable Proficiency Testing (PT) results (WAC ). 03/09/2018 Authentication Signature Rebecca Wood, Lab Accreditation Unit Supervisor Date Page 19 of 19
Cadmium B ug/l HRL Chromium B ug/l MCL 100
Appendix 4, Table A4-1 Inorganics/Metals Arsenic 7440-38-2 6010B ug/l 25 4.41 10 MCL 2 Barium 7440-39-3 6010B ug/l 10 1.04 2000 HRL Use Tier 2 5 (or hardnessspecific value if lower) Cadmium 7440-43-9 6010B
Anatek Labs, Inc - Spokane Spokane, WA
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Trace Metals mg/kg mg/kg SOLIDS 1000 Aluminum 1000 to 25000 Study Mean 0.1082 753.6118 100 SOLIDS 1005 Antimony 80 to 300 Study Mean 0.4385 8.1700 8.0 SOLIDS 1010 Arsenic 40 to 400 Study Mean 0.0915 1.0653
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STATE OF ILLINOIS ENVIRONMENTAL PROTECTION AGENCY NELAP - RECOGNIZED ENVIRONMENTAL LABORATORY ACCREDITATION. is hereby granted to
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Microbiology Misc. Analytes NPW Total Coliform, MF 2 CFU/100mL DW/NPW Acidity, as CaCO 8 3 * 585 mg/l NPW Fecal Coliform, MF 2 CFU/100mL NPW Color * 1.7 PC units NPW E.coli, MF 2 CFU/100mL DW/NPW Non-Filterable
Exact Scientific Services, Inc. Ferndale, WA
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STATE OF ILLINOIS ENVIRONMENTAL PROTECTION AGENCY NELAP - RECOGNIZED ENVIRONMENTAL LABORATORY ACCREDITATION. is hereby granted to
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Certificate of Accreditation
PERRY JOHNSON LABORATORY ACCREDITATION, INC. Certificate of Accreditation Perry Johnson Laboratory Accreditation, Inc. has assessed the Laboratory of: (Hereinafter called the Organization) and hereby declares
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