VULCAN - Fusion Technology

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Walter Hines
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1 - Fusion Technology 6MA Tools: Fusion machine Flux Flux mixtures for specific applications Platinum ware Applications Sample storage

Fusion technology is used to prepare samples to be analyzed with an X-ray fluorescence machine. It is also used to improve precision compared to pressed powder technology.

MA Automatic version No manual adjustment of the flames Full microprocessor control Applications with variable temperature settings possible High flexibility for all types of applications Storage of

2 Fusion technology is used to prepare samples to be analyzed with an X-ray fluorescence machine. It is also used to improve precision compared to pressed powder technology. Using your in combination with the extractor hood will ensure that every bead is produced under the same constant conditions! MA Automatic version No manual adjustment of the flames Full microprocessor control Applications with variable temperature settings possible High flexibility for all types of applications Storage of 0 different programs 2MA, 4MA, 6MA Technical Data 2MA 4MA 6MA Stations: 2 XRF 4 XRF 6 XRF Voltage: 0 V/60 Hz 0 V/60 Hz 0V/60 Hz 230V/50 Hz Power: 70 W 20 W 20 W Temperatures: C C C Permiss. air pressure: 6 bar 6 bar 6 bar Permiss. natural gas press.: 250 mbar 250 mbar 250 mbar Permiss. propane gas press.: 250 mbar 250 mbar 250 mbar Permiss. oxygen gas press.: 2 bar 2 bar 2 bar Air consumption: max. m3/hr max. 2 m3/hr max. 3 m3/hr Oxygen consumption: max. 0.5 m3/hr at 3 bar max. m3/hr at 3 bar max..5 m3/hr at 3 bar Natural gas consumption: max m3/hr max..2 m3/hr max..8 m3/hr Or LPG* liquefied petroleum gas max. 0.5 m3/hr at 3 bar max. 0.6 m3/hr at 3 bar max. 0.7 m3/hr at 3 bar Length: 530 mm 530 mm 530 mm Width: 530 mm 700 mm 700 mm Height: 300 mm 300 mm 300 mm Weight: ~ 40 kg ~ 45 kg ~ 50 kg Samples per h: * LPG, bottled gas Other versions on request. Please ask for installation requirements!

Feed and mould control Easy fitting and lifting of the moulds It is not possible to forget the moulds No contact with the fusion chamber Longer durability of the moulds Cover function for crucibles

contamination of the sample ICP/AAS Automatic version Available as pure ICP device with 4 or 6 stations Also available as a mix of XRF and ICP stations, for e.g.

22MA/ICP, 4MA/ICP, 6MA/ICP Technical Data 22MA/ICP 4MA/ICP 6MA/ICP Stations: 2 XRF / 2ICP 4 ICP 6 Peroxide Voltage: 0 V/60 Hz 0 V/60 Hz 0 V/60 Hz Power: 20 W 20 W 20 W Temperatures: 0-.600 C 0-.

3 Feed and mould control Easy fitting and lifting of the moulds It is not possible to forget the moulds No contact with the fusion chamber Longer durability of the moulds Cover function for crucibles Higher temperature in the crucible (excellent for materials that do not dissolve at low temperatures) Higher thermal stability in the crucible Lower energy consumption (gases) Protection against contamination of the sample ICP/AAS Automatic version Available as pure ICP device with 4 or 6 stations Also available as a mix of XRF and ICP stations, for e.g. 2 MA, 22 MA, 3 MA, 32 MA, 4 MA and 42 MA (first number indicates the XRF-stations, the second the ICP-stations) Speed of the magnetic stirrer is adjustable Other versions on request. 22MA/ICP, 4MA/ICP, 6MA/ICP Technical Data 22MA/ICP 4MA/ICP 6MA/ICP Stations: 2 XRF / 2ICP 4 ICP 6 Peroxide Voltage: 0 V/60 Hz 0 V/60 Hz 0 V/60 Hz Power: 20 W 20 W 20 W Temperatures: C C C Permiss. air pressure: 6 bar 6 bar 6 bar Permiss. natural gas press.: 250 mbar 250 mbar 250 mbar Permiss. propane gas press.: 250 mbar 250 mbar 250 mbar Permiss. oxygen gas press.: 2 bar 2 bar - Air consumption: max. 2 m3/hr max. 2 m3/hr max. 3 m3/hr Oxygen consumption: max. m3/hr at 3 bar max. m3/hr at 3 bar - Natural gas consumption: max..2 m3/hr * max. 0.9 m3/hr * max..35 m3/hr * Or LPG* liquefied petroleum gas max. 0.5 m3/hr at 3 bar max m3/hr at 3 bar max m3/hr at 3 bar Length: 530 mm 530 mm 530 mm Width: 700 mm 700 mm 700 mm Height: 300 mm 300 mm 300 mm Weight: ~ 45 kg ~ 45 kg ~ 50 kg Samples per h: * LPG, bottled gas Other versions on request. Please ask for installation requirements!

New: Peroxid Automatic version No manual adjustment of flames Full control microprocessor Applications with variable temperature settings possible High

: VU-0007) capacity 500 ml height 20 mm, diameter 75 mm Options VU-005 VU-006 Automation bar for dosing of release agent Zircon crucible for peroxide fusion

conditions, like temperature, circulation of air, stability of the flames!

4 New: Peroxid Automatic version No manual adjustment of flames Full control microprocessor Applications with variable temperature settings possible High flexibility for all types of applications Storage of 0 different programs PTFE-Cup PTFE-Cup for ICP/AAS (Item no.: VU-0007) capacity 500 ml height 20 mm, diameter 75 mm Options VU-005 VU-006 Automation bar for dosing of release agent Zircon crucible for peroxide fusion VU-0007 ACCESSORIES The extractor hood Using your in combination with the extractor hood will ensure that every bead is produced under the same constant conditions, like temperature, circulation of air, stability of the flames! The extractor hood removes all vapors and fumes, which develop during the fusion; protecting your health and extending the durability of your. Aluminium profile rack; high-grade steel cover and drain Heat resistant glass Constant circulation (no slanting of the flames) Height 298 mm, width 900 mm, depth 700 mm Motor (/90 ma) continuously variable to 2760 r.p.m; 0 V version also available. The table Together with the and the hood this table forms a professional setup The table has an integrated drawer for all needed accessories Manufactured of robust steel Height 750 mm, width 90 mm, depth 760 mm

5 Flux Borate flux with guaranteed purity from our own production. All fluxes are delivered with a certificate of analysis. Anhydrous homogeneous pre-fused fluxes with a low loss on ignition and defined granulometry. With these fluxes, the sample is completely dissolved in a borate glass with a perfect surface. Non-hygroscopic Dust < % Special fluxes on request > 99,98% Item No. Description Quantity in kg FX-X00-2 Lithium tetraborate 2 FX-X00-25N Lithium tetraborate 25 FX-X80-2 Lithium tetraborate : Lithium metaborate 80:20 2 FX-X80-2LiBr Lithium tetraborate : Lithium metaborate 80: % LiBr 2 FX-X65-2 Lithium tetraborate : Lithium metaborate 66:34 2 FX-X65-25N Lithium tetraborate : Lithium metaborate 66:34 25 FX-X50-2 Lithium tetraborate : Lithium metaborate 50:50 2 FX-X50-25N Lithium tetraborate : Lithium metaborate 50:50 25 FX-X20-2 Lithium tetraborate : Lithium metaborate 20:80 2 FX-X20-25N Lithium tetraborate : Lithium metaborate 20:80 25 FX-X35-2 Lithium tetraborate : Lithium metaborate 35.3:64.7.2:2.2 2 FX-X00-2 Lithium metaborate 2 Special Additives Item No. Description Quantity FX-ADD3 Single Additive Non Wetting Agent Pack = 50g FX-CAT8 Single catalyst for FeTi, FeCr, FeV Pack = 000g FX-OXY6 Single oxidizer for ferroalloys and metals Pack = 250g FX-OXY7 Single oxidizer for slags, ferroalloys, oxides Pack = 250g FX-SUL Borate flux for sulfide ores Pack = 000g FX-SUL2 Borate flux for sulfide ores Pack = 000g FX-SUL3 Internal standard tungsten oxide Pack = 00g FX-SUL4 Single oxidizer for sulfides Pack = 250g

Platinum Ware for We supply platinum ware made from platinum/gold 95/5 for fusion machines and laboratory needs.

This surface finishing increases the lifetime of your crucibles and moulds. Please ask for a quote. Item No.

8 0.8 3 FS-OA438 Mould 36 34 3.8 0.8 45 FS-OA439 Mould 4 39 3.8 0.8 46 For your order in platinum FKS, just add 'FKS' to the part no!

5 g Pt Ultrasonic bath with heating, Vol. ca.

6 Platinum Ware for We supply platinum ware made from platinum/gold 95/5 for fusion machines and laboratory needs. We accept old platinum ware for recycling as credit against your next order. We also offer all platinum ware in FKS. This surface finishing increases the lifetime of your crucibles and moulds. Please ask for a quote. Item No. Description OD mm ID mm Height mm Bottom mm Weight g FS-OT866 Crucible FS-OT867 Crucible FS-OA434 Mould FS-OA877 Mould FS-OA438 Mould FS-OA439 Mould For your order in platinum FKS, just add 'FKS' to the part no! Other sizes on request. Tools Item No. Description Quantity FS-OZ327 VU-US.9kit Crucible tongs, platinum shoes, length 230 mm, ca. 5 g Pt Ultrasonic bath with heating, Vol. ca..9 l for cleaning WZ-0004 Suction tool for beads and pellets VU-Tiegel_Al2O3 Aluminium oxide crucible for determination of LOI (loss on ignition). Inexpensive and very robust alternative for platinum VU-Tiegel_Al2O3 VU-US.9kit Applications We offer ready-to-go calibration packages for x-ray fluorescence analysis. Please see our application flyer for further information.

Sample Storage BX-000-24 It is important to keep reference materials prepared as beads or pellets in a dust-free and dry environment.

Description Compartments Qty/Set BX-000-8 Box 20 x 20 x 35 mm with lid 8 x max 32mm pellets/cups BX-000-24 Box 330 x 220 x 53 mm with lid 24 x max 52mm pellets/cups BX-0002-5 BX-0003-5 Drawer cabinet

42 mm) 20 x max 34mm pellets 25 x max 42mm pellets BX-0004-39 Box for single pellet H 5 mm max 34mm pellets BX-0004-46 Box for single pellet H 6 mm max 42mm pellets BX-0004-46-6 Box for single pellet

dry pearls, tray for dry pearls and hygrometer to combine with storage case x BX-0002-5 or x BX-0003-5 or 3x BX-000-24 BX-00 Desiccator W 640 x H 550 x D 40 mm incl.

drawers to add to the cabinet are available in various colors. Other dimensions on request.

7 Sample Storage BX It is important to keep reference materials prepared as beads or pellets in a dust-free and dry environment. There is a wide range of boxes and containers for single or multiple samples and standards for XRF. BX-000 BX-00 BX Item No. Description Compartments Qty/Set BX Box 20 x 20 x 35 mm with lid 8 x max 32mm pellets/cups BX Box 330 x 220 x 53 mm with lid 24 x max 52mm pellets/cups BX BX Drawer cabinet with 5 drawers, each with 42 partitions for D max 34 mm, H 7 mm (ideal for pellets D max 34 mm) Drawer cabinet with 5 drawers, each with 25 partitions for D max 42 mm, H 7 mm (ideal for pellets D max 42 mm) 20 x max 34mm pellets 25 x max 42mm pellets BX Box for single pellet H 5 mm max 34mm pellets BX Box for single pellet H 6 mm max 42mm pellets BX Box for single pellet H 6 mm max 46mm pellets BX Box for single pellet H 25 mm max 50mm pellets BX-0006-P Plastic tweezers for beads BX-000 Desiccator W 350 x H 334 x D 40 mm incl. dry pearls, tray for dry pearls and hygrometer to combine with storage case x BX or x BX or 3x BX BX-00 Desiccator W 640 x H 550 x D 40 mm incl. dry pearls, tray for dry pearls and hygrometer to combine with storage case 4x BX or 4x BX or 2x BX WZ-0004 Handling tool for glass beads and pellets Additional, individual drawers to add to the cabinet are available in various colors. Other dimensions on request. For storing your beads and pellets we would recommend: BX / BX : Boxes to store your individual samples. BX / BX / BX / BX : Store 32 mm (40 mm) samples in these transparent boxes with sealed lid. BX , BX : Drawer cabinets suitable for direct storage of non-hygroscopic samples. BX-000, BX-00: Desiccators to store your sensible calibration and monitor samples. Ideal in combination with BX , BX or BX Tip: Use our tool WZ-0004 to handle your pellets and beads and avoid finger contact.

8 FLUXANA GmbH & Co. KG Borschelstr. 3, 4755 Bedburg-Hau, Germany Tel.: +49 (0) Fax: +49 (0) Amtsgericht Kleve: HR-A 2935, HR-B 82 Ust-IdNr.: DE , Steuer-Nr. 6/5755/0442 Finanzamt Kleve Official agent FXMM

Vulcan - Fusion Technology

Vulcan - Fusion Technology Your supplier for XRF Application Solutions ELEKTRONIK Fusion machines - Fusion Technology VULCAN 4MA Tools: Fusion machine Flux Flux mixtures for specific applications Platinum ware Applications Sample