Low temperature hydrogen production from 2 nd generation biomass
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1 Low temperature hydrogen production from 2 nd generation biomass HyTIME Pieternel Claassen Food & Biobased Research Click to add title
2 PROJECT OVERVIEW SP1-JTI-FCH Hydrogen production Jan 2012-July 2015 Total budget M 2.92; FCH-JU grant M 1.32 The target of HyTIME is the production of 1-10 kg H 2 /day by fermentation of biomass. The process is derived from Anaerobic Digestion but is novel in the decoupling of hydrogen production from methane production in dedicated bioreactors. Hydrogen is harvested and biogas from the effluent of the H 2 reactor is used to cover the energy demand.
3 PROJECT TARGETS AND ACHIEVEMENTS Programme objective/ target Project objective/ target Project achievements to-date Final achieve ment AIP Efficient biological systems for digestion of 2 nd generation biomass Supply of biomass. Mobilisation of fermentable components Optimized protocols for straw and grass (steam ex, chemical, enzymatic). Energy demand, reduction of enzymes 100% Low temperature H 2 production process Efficient H 2 fermentation in dedicated reactors Grass : 90% yield at 5.7 L. Larger scale: 25-30% yield at L scale 35% Development of bioh 2 production systems Optimisation of gas upgrading, AD, process monitoring and system integration MC successful, AD potential sufficient, new devices for online control, mass and energy balances, technoeconomics overall process Circa 75%
4 Validation of pretreatment Wheat straw 1. Steam explosion or acid impregnation 2. Enzymatic hydrolysis 3. Hydrogen fermentation in 35 L CSTR: 4. Anaerobic digestion in 250 L CSTR: Hydrolysate/ inoculum T reactor HRT(h) % H 2 H 2 in g/day C+E/Anaerobic sludge S+E/C. saccharolyticus C+E/C. saccharolyticus
5 Dedicated bioreactors and upscaling Cell retention 1 m 3 grass hydrolysate: 4.7 m 3 H m 3 CH 4 at 6 g H 2 /day Verge grass Packed bed reactor (5.7 L)
6 Final scale: 225 L
7 Results of upscaling in dedicated reactors Feedstock Volume L Type reactor T reactor HRT (h) Yield % % H 2 H 2 in g/day Straw(C) 35 CSTR n.d Grass(C) 5.7 PB/GD Sucrose 58 PB/GD Molasses 58 PB/GD Glucose 225 PB/GD
8 Biohydrogen production system Cleaned off-gas Inlet fermenter off-gas Absorption unit Cooling Membrane modules for CO 2 removal Heating Desorption Visualisation software for remote process control
9 Techno-economic analysis
10 Objective: 1-10 kg H 2 /day Achieved: 109 g H 2 /day Yield only 25% instead of 90% (contamination) Reactor size 225 L instead of 500 L (defaulting partner) Low organic loading (lack of time) Main contingency plans: Exploration new bacteria Carbohydrate vs lignocellulose -derived biomass
11 SYNERGIES WITH OTHER PROJECTS AND INITIATIVES Co-funding by Dutch ministry of Economic Affairs: Topsector AgriFood FCH JU interactions: UNIfHY (HyGEAR), FITUP (ENVIPARK), HYPROFESSIONALS (ENVIPARK), ENE.FIELD (ENVIPARK), FLUMABACK (ENVIPARK), Knowhy (ENVIPARK) EU interactions: SAHYOG (DLO-FBR), Ambigas (RWTH), TMFB (RWTH) International-level projects: SEBE (ENVIPARK), BioH2 regional (ENVIPARK), HySTREM (ENVIPARK), H2MemClean (TUW), Biomethair (ENVIPARK), Thai-German Seed Fund (RWTH) HyTIME is a direct continuation of FP 5 BIOHYDROGEN (Proof of principle) and FP 6 HYVOLUTION (increase of H 2 yield); Coordinated by DLO-FBR
12 HORIZONTAL ACTIVITIES Training activities 2 practical training of students, 1 workshop, 3 training courses on production of BioH 2 and AD (ENVIPARK) 1 PhD, 2 Masters, 1 Bachelor student (TUW) 1-4 Masters, 2 Bachelors, 1 Diplom student and 15 undergraduates (RWTH) 1 PhD student, external training (DLO-FBR)
13 DISSEMINATION ACTIVITIES ( ) Conferences with presentations: PRES, Prague 2014 DECHEMA, Aachen 2014 Fuels of the Future, Berlin 2014 Beyond Biogas, Wageningen 2014 EBCE, Vienna 2015 PRES, Kuching 2015 Bioethanol & Bioconversion Technology, Detmold 2015 Hypothesis XI, Toledo 2015
14 EXPLOITATION PLAN/EXPECTED IMPACT Change in FCHJU technology development panorama: Fermentation is a realistic approach to sustainable hydrogen production Exploitations: A hydrogen sensor system with an electrochemical and a thermal conductivity sensor Communication and visualisation software Remote control for advanced support Main RTD results beyond international State-of-Art: Prolonged continuous hydrogen fermentation with fitting mass balance at large scale Integration of fermentation and gas upgrading Evaluation of biohydrogen production costs Current RTD results for industrial application/follow up: Biomass suitability and pretreatment protocols Test of biohydrogen production potential Integration and simulation models for biorefinery processes for biobased chemicals
HyTIME (278855) Pieternel Claassen DLO-Food and Biobased Research
HyTIME (278855) Pieternel Claassen DLO-Food and Biobased Research Project & Partnership description General Overview Full title: Low temperature hydrogen production from 2 nd generation biomass Duration:
PROJECT FINAL REPORT
PROJECT FINAL REPORT ("Publishable") FCH JU Grant Agreement number: 278855 Project acronym: Project title: Funding Scheme: HYTIME Low temperature hydrogen production from 2 nd generation biomass Collaborative
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