Investigating Copper Metallurgy Effects for Sort Process and Cleaning Performance Metrics

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1 Jan Martens NXP Semiconductors Germany Simon Allgaier Feinmetall GmbH Jerry Broz, Ph.D. International Test Solutions Investigating Copper Metallurgy Effects for Sort Process and Cleaning Performance Metrics June 7-10, San Diego, CA USA

2 Content Motivation Joint Venture Overview FM: ViProbe ITS: Lab Capabilities NXP: Engineering Environment Contact Resistance and Fritting Theory Experimental Data Production Data Results & Future Work Martens, Allgaier,, Broz IEEE SW Test Workshop 2

3 Motivation Joint Venture Overview FM: ViProbe ITS: Lab Capabilities NXP: Engineering Environment Contact Resistance and Fritting Theory Experimental Data Production Data Results & Future Work Martens, Allgaier,, Broz IEEE SW Test Workshop 3

4 Motivation Public knowledge of bare copper probing is limited and industry rumors suggest difficult process control. Sort floors are often resource limited for performing fundamental characterization studies. Testing with full-build probe cards is expensive and often not feasible, particularly with large array probe cards. Assessing combinations of key performance parameters performed quickly under known and controlled conditions. Martens, Allgaier,, Broz IEEE SW Test Workshop 4

5 Motivation Joint Venture Overview FM: ViProbe ITS: Lab Capabilities NXP: Engineering Environment Contact Resistance and Fritting Theory Experimental Data Production Data Results & Future Work Martens, Allgaier,, Broz IEEE SW Test Workshop 5

6 Feinmetall ViProbe Contacting on Copper Contacting on bare copper is becoming more important for the semiconductor industry. Feinmetall is faced with different costumers and different types copper based technologies. Aluminium vs. copper seems to be two different worlds for wafer test. Martens, Allgaier,, Broz IEEE SW Test Workshop 6

7 Feinmetall ViProbe Trivar HC SWTW2008 Tests on aluminium with 3 mil beams 800 ma maximum current. SWTW2009 Tests on copper with 2 mil beams 300 ma current minimum beam pitch: 75 µm To decrease the pitch and make the next technology step Feinmetall has introduced a new fine pitch beam: 1.6 mil diameter 200 ma max. current 59 µm minimum needle pitch Martens, Allgaier,, Broz IEEE SW Test Workshop 7

8 ViProbe Testvehicle Smallest ViProbe test head ever designed and built 1.6 mil, 2 mil, 2.5 mil and 3 mil ViProbe compatibility 25-PIN D-Sub Connector Probe Head Electrical Connection Beams Connector Martens, Allgaier,, Broz IEEE SW Test Workshop 8

9 Controlled Test Conditions Bench-top instrument for material characterization and probe performance testing. NI LabVIEW Motion Control Data Acquisition Precision Stages ITS LTU Probe-Gen System Testing System Details Variable z-speed and z-acceleration. Low gram load cell measurements. Synchronized load vs. overtravel vs. CRES data acquisition. High resolution video imaging and still image capture. Current forcing and measurement with Keithley 2400 source-meter. Micro-stepping capable to maximize number of touchdowns. Multi-zone cleaning functionalities. Martens, Allgaier,, Broz IEEE SW Test Workshop 9

10 Bench Top Testing ViProbe with 50 gram load cell Synchronized DAQ Load vs. overtravel vs. CRES Probe Polish 70 Cleaning Zone Electrical Test Zone Probe / Material Interaction and Buckling Visualization Martens, Allgaier,, Broz IEEE SW Test Workshop 10

11 NXP Testcenter Hamburg Engineering Environment Engineering site for automotive and identification business, digital, and mixed signal products. Applications with high multisite factors and small pad pitch. Capability to collect contact resistance data within production like environment Martens, Allgaier,, Broz IEEE SW Test Workshop 11

12 Multi Probing Within Pads to Maximize Touchdowns Pin to Pin CRES 4-wire Measurement Martens, Allgaier,, Broz IEEE SW Test Workshop 12

13 Motivation Joint Venture Overview FM: ViProbe ITS: Lab Capabilities NXP: Engineering Environment Contact Resistance and Fritting Theory Experimental Data Production Data Results & Future Work Martens, Allgaier,, Broz IEEE SW Test Workshop 13

14 Contact Resistance (CRES) CRES is considered the most CRITICAL parameters in wafer sort CRES Fundamentals CRES occurs between two bodies in contact Creates losses in electrical and thermal systems Current flow is constricted to the inter-metallic contacts Localized joule heating Martens, Allgaier,, Broz IEEE SW Test Workshop 14

15 Contact Resistance (CRES) Contact Resistance is a combination two main parameters Localized physical mechanisms metallic contact Non-conductive contribution film resistance Model for CRES has two main factors C RES probe 4 pad H P film P H pad, probe, film = resistivity values H = hardness of softer material P = contact pressure METALLIC CONTACT Contact pressure (P) applied force normalized by true contact area FILM RESISTANCE Unstable CRES is dominated by the film contribution term due to the accumulation of non-conductive materials Martens, Allgaier,, Broz IEEE SW Test Workshop 15

16 Key Factors that affect CRES Presence of contamination eventually dominates the magnitude and stability of the CRES. Probe shape and needle contact mechanics play an important role Displacing the contaminants from the true contact area Surface characteristics affect the a-spot density R. Martens, et. al, IEEE SW Test Workshop (2004) C. Manion, et. al, IEEE SW Test Workshop (2000) Pad hardness contributes to pad penetration and acummulation Softer Pads Better oxide break through but more debris Harder Pads Less debris but worse oxide break through Ehrler, et. al, IEEE SW Test Workshop (2007) Amplitude and directionality of the voltage or current applied. Voltage or current must be sufficient to breakdown the oxide J. Martens, et. al, IEEE SW Test Workshop (2008) J. Martens,, et. al, IEEE SW Test Workshop (2006) Martens, Allgaier,, Broz IEEE SW Test Workshop 16

17 Fritting Theory The vertical Probe tip touches the contact pad. Probe Tip Depending on the contact pressure the oxide film is broken partly and electrical bridges arise. The number and size of the bridges is equivalent to the C RES quality Contact Pad Martens, Allgaier,, Broz IEEE SW Test Workshop 17

18 Fritting Theory What happens, if bridges are only few and small? Probe tip Oxide film Contact pad Small bridge through oxide film. Before high current flow. Martens, Allgaier,, Broz IEEE SW Test Workshop 18

19 Fritting Theory Current must flow through small bridge. Bridge and neighborhood are heated up Contact Pad material migrates to the bridge. Probe tip Oxide film Contact pad High current flow situation: Black Lines of current flow. White Lines of equipotential surface. Martens, Allgaier,, Broz IEEE SW Test Workshop 19

20 Fritting Theory Bridge is widened C RES decreased Contact pad material migrated to the bridge and tip surface Probe tip Oxide film Contact pad Wide bridge through oxide film. After high current flow. Tip surface is contaminated. Martens, Allgaier,, Broz IEEE SW Test Workshop 20

21 Fritting What s that? Fritting is a kind of electrical breakdown at the contact surface between the probe tip and the contact pad of the IC. It improves the electrical contact by building or stabilizing bridges through the oxide film, if the film was not mechanically broken completely. After Fritting the probe tip is welded with the contact pad. After removing the contact residuals of the welding remain at the probe tip and will oxidize. Probe Tip Contact Pad Martens, Allgaier,, Broz IEEE SW Test Workshop 21

22 Motivation Joint Venture Overview FM: ViProbe ITS: Lab Capabilities NXP: Engineering Environment Contact Resistance and Fritting Theory Experimental Data Production Data Results & Future Work Martens, Allgaier,, Broz IEEE SW Test Workshop 22

23 Description DOE 1 CRES vs. Overtravel (OT) characteristic on several pad materials Rhodium plate (reference) Rh plate Blanket aluminum wafer ( 08 data) Al Wafer Blanket galvanic copper wafer (10µm) Cu Wafer NXP internally processed product NXP source A 1mA pin to pin 6TDs each material up to 75µm OT Measuring CRES and Probe force Martens, Allgaier,, Broz IEEE SW Test Workshop 23

24 Probe Force Result DOE1 8 Probe force for 2 beams on Cu Wafer Probe Force [cn] nd Touch Probe force increasing Probe force decreasing Hysteresis caused by plastic deformation 2 1 st Touch OT [µm] Martens, Allgaier,, Broz IEEE SW Test Workshop 24

25 CRES Results DOE Rh Plate Al Wafer Cu Wafer NXP Source A Contact Resistance Cres [Ohm] Thin Copper Oxides Film Resistance 1 Metallic Contact OT [µm] Martens, Allgaier,, Broz IEEE SW Test Workshop 25

26 Description DOE 2 CRES vs. Overtravel (OT) characteristic on several pad materials Rhodium plate (reference) Rh plate Blanket aluminum wafer ( 08 data) Al Wafer Blanket galvanic copper wafer (10µm) Cu Wafer NXP internally processed products NXP source A and B Current from 1mA to 300mA 6TDs each material up to 75µm OT Data taken from 20µm OT (forcing fritting by bad mechanical scrub through oxide) Martens, Allgaier,, Broz IEEE SW Test Workshop 26

27 CRES Results DOE Cu 1mA Cu 300mA Contact Resistance Cres [Ohm] Fritting OT [µm] Martens, Allgaier,, Broz IEEE SW Test Workshop 27

28 CRES Results DOE2 Contact Resistance Cres [Ohm] Thin oxide Less Fritting CRES decrease Because of Fritting AL Wafer (2008 data) Cu Wafer NXP Source B NXP Source A Rh Plate Measurement Current [ma] Martens, Allgaier,, Broz IEEE SW Test Workshop 28

29 Description DOE 3 Long term test (LTT) with up to 20k TDs Blanket aluminium wafer ( 08 data) Al Wafer Blanket galvanic copper wafer (10µm) Cu Wafer NXP internally processed products NXP source A and B Pin to Pin Current 150mA on Cu OT at 20µm (forcing fritting by bad mechanical scrub through oxide) Different cleaning settings No cleaning to establish baseline CRES trending Frequent cleaning Cleaning interval 128 TDs with 32 cleaning TDs at 75µm OT ITS Probe Polish 70 Infrequent cleaning Cleaning interval 1k TDs with 128 cleaning TDs at 75µm OT ITS Probe Polish 70 Martens, Allgaier,, Broz IEEE SW Test Workshop 29

30 Cu Wafer LTT without cleaning 100% Cumulative Probability 80% 60% 40% Metallic contact Film resistance Fast CRES increase 20% 64 TDs 256 TDs 1k TDs 4k TDs 20k TDs 0% 2 2,5 3 3,5 4 4,5 5 Contact Resistance [Ohm] 64 TDs 256 TDs 1k TDs 4k TDs 20k TDs Martens, Allgaier,, Broz IEEE SW Test Workshop 30

31 Al Wafer LTT without cleaning ( 08)( 100% 80% Fast CRES increase Cumulative Probability 60% 40% 20% 64 TDs 256 TDs 1k TDs 4k TDs 20k TDs 0% 1,5 2 2,5 3 3,5 4 4,5 5 Contact Resistance [Ohm] 64 TDs 256 TDs 1k TDs 4k TDs 20k TDs Martens, Allgaier,, Broz IEEE SW Test Workshop 31

32 NXP Source B LTT without cleaning 100% 80% Cumulative Probability 60% 40% Needs frequent Cleaning 20% 64 TDs 256 TDs 1k TDs 4k TDs 10k TDs 0% 2 2,5 3 3,5 4 4,5 5 Contact Resistance [Ohm] 64 TDs 256 TDs 1k TDs 4k TDs 10k TDs Martens, Allgaier,, Broz IEEE SW Test Workshop 32

33 NXP Source B LTT with frequent cleaning 100% 80% Cumulative Probability 60% 40% Frequent Cleaning Improves CRES 20% 64 TDs 256 TDs 1k TDs 4k TDs 10k TDs 0% 2 2,5 3 3,5 4 4,5 5 Contact Resistance [Ohm] 64 TDs 256 TDs 1k TDs 4k TDs 10k TDs Martens, Allgaier,, Broz IEEE SW Test Workshop 33

34 NXP Source A LTT without cleaning 100% Cumulative Probability 80% 60% 40% Needs infrequent Cleaning 20% 64 TDs 256 TDs 1k TDs 4k TDs 10k TDs 0% 2 2,5 3 3,5 4 4,5 5 Contact Resistance [Ohm] 64 TDs 256 TDs 1k TDs 4k TDs 10k TDs Martens, Allgaier,, Broz IEEE SW Test Workshop 34

35 NXP Source A LTT with infrequent cleaning 100% Cumulative Probability 80% 60% 40% Infrequent Cleaning improves CRES 20% 64 TDs 256 TDs 1k TDs 4k TDs 10k TDs 0% 2 2,5 3 3,5 4 4,5 5 Contact Resistance [Ohm] 64 TDs 256 TDs 1k TDs 4k TDs 10k TDs Martens, Allgaier,, Broz IEEE SW Test Workshop 35

36 SEM pictures after 20k LTT without any cleaning NXP Source A Al Wafer Blanket Cu Wafer Contact surface visibly contaminated Contact surface appears less contaminated NXP Source B Martens, Allgaier,, Broz IEEE SW Test Workshop 36

37 Motivation Joint Venture Overview FM: ViProbe ITS: Lab Capabilities NXP: Engineering Environment Contact Resistance and Fritting Theory Experimental Data Production Data Results & Future Work Martens, Allgaier,, Broz IEEE SW Test Workshop 37

38 Production CRES Measurement Evaluation of NXP Source A and aluminium reference. Probecard with 16 Kelvin contacts (3mil beams). Rebuild for pin to pin and 4-wire CRES measurement 3.5k test runs to identify contact performance. Fritting study with 300mA current between CRES measurements of 3mA. No cleaning to differentiate the CRES performance. Martens, Allgaier,, Broz IEEE SW Test Workshop 38

39 Production CRES Comparison 100% 80% Better CRES Performance on Copper Less Fritting on Copper Cumulative Probability 60% 40% 20% 0% Consistent result! 2 2,5 3 3,5 4 4,5 5 Contact Resistance [Ohm] NXP Alu before Fritting NXP Alu after Fritting NXP Cu Source A before Fritting NXP Cu Source A after Fritting Martens, Allgaier,, Broz IEEE SW Test Workshop 39

40 Production CRES Comparison 100% ITS Lab LTT NXP Production LTT 80% Cumulative Probability 60% 40% Consistent result! 20% 0% 2 2,5 3 3,5 4 4,5 5 Contact Resistance [Ohm] Martens, Allgaier,, Broz IEEE SW Test Workshop 40

41 Motivation Joint Venture Overview FM: ViProbe ITS: Lab Capabilities NXP: Engineering Environment Contact Resistance and Fritting Theory Experimental Data Production Data Results & Future Work Martens, Allgaier,, Broz IEEE SW Test Workshop 41

42 Results / Discussion Several copper source analysed and fritting was observed on all sources detected. NXP sources perform better than reference blanket copper wafer. Thinner oxides on copper compared to aluminum reduce the effect of Fritting because of better oxide penetration. Copper debris on contact surfaces are barely detectable by optical inspection. Martens, Allgaier,, Broz IEEE SW Test Workshop 42

43 Results / Discussion FM ViProbe with 2 mil beams show consistent probe force and CRES performance. Production and lab data fit consistently for proof of this analysis strategy. NXP copper sources qualified and ranked and cost effective cleaning recipes optimized. Martens, Allgaier,, Broz IEEE SW Test Workshop 43

44 Future Work (many interesting studies!) Copper at different temperatures (high AND low). FM ViProbe 1.6 mil beam performance. Extended long long term tests (> 20K TDs). Analyse background of copper performance differences. Investigating the effects and repercussions of the fritting mechanisms Temperature Frequency Fab materials Martens, Allgaier,, Broz IEEE SW Test Workshop 44

45 Acknowledgements Feinmetall Engineering Development and Design Teams ITS Applications Engineering Team Andrea Haag (Engineering Technician) Martens, Allgaier,, Broz IEEE SW Test Workshop 45

46 Men At Work Martens, Allgaier,, Broz IEEE SW Test Workshop 46

47 Thank you! Questions?

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