ANALYTICAL SUMMARY REPORT

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1 ANALYTICAL SUMMARY REPORT August 11, Washington Cottage Grove, OR Work Order: G Quote ID: G433 - Soil/Product Mix Project Name: Energy Laboratories Inc. Gillette WY received the following 6 samples for on 7/22/2014 for analysis. Lab ID Client Sample ID Collect Date Receive Date Matrix Test G Brine - Equal Parts 07/21/14 9:30 07/22/14 Soil Conductivity DRO-Ultrasonic Extraction Diesel Range Organics Hydrocarbons, Total Petroleum Anions by Ion Chromatography Moisture PAINT FILTER LIQUIDS TEST Saturated Paste Extraction Oil & Gas Commission Ext. Solids, Total Dissolved G Brine - 1 gallon brine/1/2 gallon product G Envert - 1 gallon envert/1/2 gallon product G Envert - 1 gallon product/1/4 gallon product The analyses presented in this report were performed by Energy Laboratories, Inc., 400 W. Boxelder Rd., Gillette, WY 82718, unless otherwise noted. As appropriate, any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these tests results, please call. 07/21/14 9:30 07/22/14 Soil Same As Above 07/21/14 7:50 07/22/14 Soil Same As Above 07/21/14 7:50 07/22/14 Soil Same As Above G Brine 07/21/14 9:19 07/22/14 Soil Moisture G Envert 07/21/14 7:50 07/22/14 Soil Same As Above Report Approved By: Page 1 of 15

2 CLIENT: Project: Report Date: 08/11/14 Work Order: G CASE NARRATIVE Tests associated with analyst identified as ELI-H were subcontracted to Energy Laboratories, 3161 E. Lyndale Ave., Helena, MT, EPA Number MT Tests associated with analyst identified as ELI-B were subcontracted to Energy Laboratories, 1120 S. 27th St., Billings, MT, EPA Number MT Page 2 of 15

3 LABORATORY ANALYTICAL REPORT Project: Report Date: 08/11/14 Client Sample ID: Brine - Equal Parts Collection Date: 07/21/14 09:30 Location: Date Received: 07/22/14 Samp FRQ/Type: Matrix: Soil Lab ID: G Sampled By: Bob Gonzales Analyses Result Units RL Qualifier Method Analysis Date / By WASTE ANALYSIS Paint Filter Liquids Test ND ml/100g 1.0 SW9095B 07/30/14 06:27 / eli-b PHYSICAL CHARACTERISTICS Moisture (As Received) 19.8 wt% 0.2 D /23/14 16:18 / djb WOGCC LEACHATE Solids, Total Dissolved 180 C Total Petroleum Hydrocarbons A2540 C E1664A 07/28/14 08:26 / blb 07/28/14 13:51 / mav NON-METALS 25 C umhos/cm 10 A2510 B 07/28/14 14:12 / blb PETROLEUM HYDROCARBONS-SEMI-VOLATILE Diesel Range Organics (DRO) mg/kg 1000 Total Extractable Hydrocarbons mg/kg 1000 Surr: o-terphenyl 0 %REC O - te 1: Diesel Range Organics are defined as all hydrocarbons eluting between C10 and C28. - te 2: Total Extractable Hydrocarbons are defined as the total hydrocarbon response regardless of elution time. 07/28/14 12:11 / eli-b 07/28/14 12:11 / eli-b 07/28/14 12:11 / eli-b SATURATED PASTE EXTRACT Chloride D E300.0 Chloride, sat. paste 1720 meq/l 4 D E /07/14 13:14 / eli-h 08/07/14 13:14 / eli-h Report Definitions: QCL - Quality control limit. D - RL increased due to sample matrix. MCL - Maximum contaminant level. O - Diluted out. Page 3 of 15

4 LABORATORY ANALYTICAL REPORT Project: Report Date: 08/11/14 Client Sample ID: Brine - 1 gallon brine/1/2 gallon product Collection Date: 07/21/14 09:30 Location: Date Received: 07/22/14 Samp FRQ/Type: Matrix: Soil Lab ID: G Sampled By: Bob Gonzales Analyses Result Units RL Qualifier Method Analysis Date / By WASTE ANALYSIS Paint Filter Liquids Test ND ml/100g 1.0 SW9095B 07/30/14 06:27 / eli-b PHYSICAL CHARACTERISTICS Moisture (As Received) 19.6 wt% 0.2 D /23/14 16:21 / djb WOGCC LEACHATE Solids, Total Dissolved 180 C Total Petroleum Hydrocarbons A2540 C E1664A 07/28/14 08:26 / blb 07/28/14 13:50 / mav NON-METALS 25 C umhos/cm 10 A2510 B 07/28/14 14:12 / blb PETROLEUM HYDROCARBONS-SEMI-VOLATILE Diesel Range Organics (DRO) mg/kg 1000 Total Extractable Hydrocarbons mg/kg 1000 Surr: o-terphenyl 0 %REC O - te 1: Diesel Range Organics are defined as all hydrocarbons eluting between C10 and C28. - te 2: Total Extractable Hydrocarbons are defined as the total hydrocarbon response regardless of elution time. 07/28/14 12:55 / eli-b 07/28/14 12:55 / eli-b 07/28/14 12:55 / eli-b SATURATED PASTE EXTRACT Chloride D E300.0 Chloride, sat. paste 2220 meq/l 4 D E /07/14 13:25 / eli-h 08/07/14 13:25 / eli-h Report Definitions: QCL - Quality control limit. D - RL increased due to sample matrix. MCL - Maximum contaminant level. O - Diluted out. Page 4 of 15

5 LABORATORY ANALYTICAL REPORT Project: Report Date: 08/11/14 Client Sample ID: Envert - 1 gallon envert/1/2 gallon product Collection Date: 07/21/14 07:50 Location: Date Received: 07/22/14 Samp FRQ/Type: Matrix: Soil Lab ID: G Sampled By: Bob Gonzales Analyses Result Units RL Qualifier Method Analysis Date / By WASTE ANALYSIS Paint Filter Liquids Test ND ml/100g 1.0 SW9095B 07/30/14 06:27 / eli-b PHYSICAL CHARACTERISTICS Moisture (As Received) 8.9 wt% 0.2 D /23/14 16:23 / djb WOGCC LEACHATE Solids, Total Dissolved 180 C Total Petroleum Hydrocarbons A2540 C E1664A 07/28/14 08:26 / blb 07/28/14 13:53 / mav NON-METALS 25 C umhos/cm 10 A2510 B 07/28/14 14:13 / blb PETROLEUM HYDROCARBONS-SEMI-VOLATILE Diesel Range Organics (DRO) mg/kg 2000 Total Extractable Hydrocarbons mg/kg 2000 Surr: o-terphenyl 0 %REC O - te 1: Diesel Range Organics are defined as all hydrocarbons eluting between C10 and C28. - te 2: Total Extractable Hydrocarbons are defined as the total hydrocarbon response regardless of elution time. 07/27/14 18:37 / eli-b 07/27/14 18:37 / eli-b 07/27/14 18:37 / eli-b SATURATED PASTE EXTRACT Chloride D E300.0 Chloride, sat. paste 2050 meq/l 4 D E /07/14 13:36 / eli-h 08/07/14 13:36 / eli-h Report Definitions: QCL - Quality control limit. D - RL increased due to sample matrix. MCL - Maximum contaminant level. O - Diluted out. Page 5 of 15

6 LABORATORY ANALYTICAL REPORT Project: Report Date: 08/11/14 Client Sample ID: Envert - 1 gallon product/1/4 gallon product Collection Date: 07/21/14 07:50 Location: Date Received: 07/22/14 Samp FRQ/Type: Matrix: Soil Lab ID: G Sampled By: Bob Gonzales Analyses Result Units RL Qualifier Method Analysis Date / By WASTE ANALYSIS Paint Filter Liquids Test ND ml/100g 1.0 SW9095B 07/30/14 06:27 / eli-b PHYSICAL CHARACTERISTICS Moisture (As Received) 11.4 wt% 0.2 D /23/14 16:26 / djb WOGCC LEACHATE Solids, Total Dissolved 180 C Total Petroleum Hydrocarbons A2540 C E1664A 07/28/14 08:26 / blb 07/28/14 13:48 / mav NON-METALS 25 C umhos/cm 10 A2510 B 07/28/14 14:13 / blb PETROLEUM HYDROCARBONS-SEMI-VOLATILE Diesel Range Organics (DRO) mg/kg 2000 Total Extractable Hydrocarbons mg/kg 2000 Surr: o-terphenyl 0 %REC O - te 1: Diesel Range Organics are defined as all hydrocarbons eluting between C10 and C28. - te 2: Total Extractable Hydrocarbons are defined as the total hydrocarbon response regardless of elution time. 07/27/14 19:21 / eli-b 07/27/14 19:21 / eli-b 07/27/14 19:21 / eli-b SATURATED PASTE EXTRACT Chloride D E300.0 Chloride, sat. paste 2720 meq/l 4 D E /07/14 13:47 / eli-h 08/07/14 13:47 / eli-h Report Definitions: QCL - Quality control limit. D - RL increased due to sample matrix. MCL - Maximum contaminant level. O - Diluted out. Page 6 of 15

7 LABORATORY ANALYTICAL REPORT Project: Report Date: 08/11/14 Client Sample ID: Brine Collection Date: 07/21/14 09:19 Location: Date Received: 07/22/14 Samp FRQ/Type: Matrix: Soil Lab ID: G Sampled By: Bob Gonzales Analyses Result Units RL Qualifier Method Analysis Date / By PHYSICAL CHARACTERISTICS Moisture (As Received) 28.2 wt% 0.2 D /23/14 16:28 / djb Report Definitions: QCL - Quality control limit. MCL - Maximum contaminant level. Page 7 of 15

8 LABORATORY ANALYTICAL REPORT Project: Report Date: 08/11/14 Client Sample ID: Envert Collection Date: 07/21/14 07:50 Location: Date Received: 07/22/14 Samp FRQ/Type: Matrix: Soil Lab ID: G Sampled By: Bob Gonzales Analyses Result Units RL Qualifier Method Analysis Date / By PHYSICAL CHARACTERISTICS Moisture (As Received) 10.8 wt% 0.2 D /23/14 16:29 / djb Report Definitions: QCL - Quality control limit. MCL - Maximum contaminant level. Page 8 of 15

9 Project: QA/QC Summary Report Report Date: 08/11/14 Work Order: G Analyte Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: A2510 B Batch: _1_COND-PROBE-W Lab ID: ICV1-1_ Initial Calibration Verification Standard Run: COND1-G_140728A 07/28/14 13:54 25 C 100 umhos/cm Lab ID: ICV2-1_ Initial Calibration Verification Standard Run: COND1-G_140728A 07/28/14 13:54 25 C 5140 umhos/cm Lab ID: ICV3-1_ Initial Calibration Verification Standard Run: COND1-G_140728A 07/28/14 13:56 25 C umhos/cm Lab ID: ICV4-1_ Initial Calibration Verification Standard Run: COND1-G_140728A 07/28/14 13:56 25 C umhos/cm Lab ID: MBLK-1_ Method Blank Run: COND1-G_140728A 07/28/14 13:58 25 C 1 umhos/cm 0.2 Lab ID: G ADUP Sample Duplicate Run: COND1-G_140728A 07/28/14 14:13 25 C umhos/cm Qualifiers: Page 9 of 15

10 Project: QA/QC Summary Report Report Date: 08/11/14 Work Order: G Analyte Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: A2540 C Batch: TDS140728A Lab ID: MB-1_140728A Method Blank Run: BAL-MET-AE_140728A 07/28/14 08:23 Solids, Total Dissolved 180 C ND 4 Lab ID: LCS-2_140728A Laboratory Control Sample Run: BAL-MET-AE_140728A 07/28/14 08:23 Solids, Total Dissolved 180 C Lab ID: G A MS Sample Matrix Spike Run: BAL-MET-AE_140728A 07/28/14 08:24 Solids, Total Dissolved 180 C Lab ID: G A DUP Sample Duplicate Run: BAL-MET-AE_140728A 07/28/14 08:27 Solids, Total Dissolved 180 C Qualifiers: Page 10 of 15

11 Project: QA/QC Summary Report Report Date: 08/11/14 Work Order: G Analyte Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: E1664A Batch: A Lab ID: MBLK Method Blank Run: BAL-ACCU-124_140728A 07/28/14 08:48 Total Petroleum Hydrocarbons ND 0.8 Lab ID: LCS Laboratory Control Sample Run: BAL-ACCU-124_140728A 07/28/14 08:52 Total Petroleum Hydrocarbons Lab ID: LCSD Laboratory Control Sample Duplicate Run: BAL-ACCU-124_140728A 07/28/14 08:54 Total Petroleum Hydrocarbons Lab ID: G FMS Sample Matrix Spike Run: BAL-ACCU-124_140728A 07/28/14 08:55 Total Petroleum Hydrocarbons Qualifiers: Page 11 of 15

12 Project: QA/QC Summary Report Prepared by Billings, MT Branch Report Date: 08/01/14 Work Order: G Analyte Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: Batch: Lab ID: LCS Laboratory Control Sample Run: GCFID-HP2-B_140725D 07/28/14 04:06 Diesel Range Organics (DRO) 445 mg/kg Total Extractable Hydrocarbons 463 mg/kg Surr: o-terphenyl Lab ID: MB Method Blank Run: GCFID-HP2-B_140725D 07/28/14 04:50 Diesel Range Organics (DRO) ND mg/kg 10 Total Extractable Hydrocarbons ND mg/kg 10 Surr: o-terphenyl Lab ID: B BMS Sample Matrix Spike Run: GCFID-HP2-B_140725D 07/28/14 06:18 Diesel Range Organics (DRO) 504 mg/kg Total Extractable Hydrocarbons 530 mg/kg Surr: o-terphenyl Lab ID: B BMSD Sample Matrix Spike Duplicate Run: GCFID-HP2-B_140725D 07/28/14 07:02 Diesel Range Organics (DRO) 432 mg/kg Total Extractable Hydrocarbons 456 mg/kg Surr: o-terphenyl Method: Analytical Run: R Lab ID: CCV_0725HP252r Continuing Calibration Verification Standard 07/27/14 09:06 Total Extractable Hydrocarbons 506 mg/kg Surr: o-terphenyl Method: Analytical Run: R Lab ID: CCV_0725HP284r Continuing Calibration Verification Standard 07/28/14 08:30 Total Extractable Hydrocarbons 520 mg/kg Surr: o-terphenyl Qualifiers: Page 12 of 15

13 Project: QA/QC Summary Report Prepared by Helena, MT Branch Report Date: 08/08/14 Work Order: G Analyte Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual Method: E300.0 Batch: Lab ID: LCS Laboratory Control Sample Run: IC102-H_140804A 08/04/14 21:07 Chloride, sat. paste 2.77 meq/l Lab ID: MB Method Blank Run: IC102-H_140804A 08/04/14 21:19 Chloride, sat. paste ND meq/l Method: E300.0 Batch: Lab ID: G BMS Sample Matrix Spike Run: IC102-H_140806A 08/06/14 16:47 Chloride, sat. paste 2150 meq/l A Method: E300.0 Analytical Run: IC102-H_140807A Lab ID: ICV Initial Calibration Verification Standard 08/07/14 09:43 Chloride Lab ID: CCV Continuing Calibration Verification Standard 08/07/14 12:52 Chloride Method: E300.0 Batch: Lab ID: G BDUP Sample Duplicate Run: IC102-H_140807A 08/07/14 13:58 Chloride, sat. paste 2820 meq/l Qualifiers: A - The analyte level was greater than four times the spike level. In accordance with the method % recovery is not calculated. Page 13 of 15

14 Workorder Receipt Checklist G Login completed by: Reviewed by: Reviewed Date: Amanda Alley BL2000\kscottruff 7/23/2014 Date Received: 7/22/2014 Received by: tla Carrier name: Hand Del Shipping container/cooler in good condition? t Present Custody seals intact on all shipping container(s)/cooler(s)? t Present Custody seals intact on all sample bottles? t Present Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as ph, DO, Res Cl, Sulfite, Ferrous Iron, etc.) Temp Blank received in all shipping container(s)/cooler(s)? t Applicable Container/Temp Blank temperature: 12.6 C On Ice - From Field Water - VOA vials have zero headspace? VOA vials submitted Water - ph acceptable upon receipt? t Applicable Standard Reporting Procedures: Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as ph, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Contact and Corrective Action Comments: COC has the wrong collection date. The bottles are marked 07/21/2014. tla 8/11/2014 Page 14 of 15

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ANALYTICAL SUMMARY REPORT

ANALYTICAL SUMMARY REPORT ANALYTICAL SUMMAY EPOT vember 01, 2018 201 1st Ave N Lewistown, MT 59457-1725 Work Order: Project Name: B18101757 MT0001229 Energy Laboratories Inc Billings MT received the following 1 sample for on 10/19/2018