Sample ID: NTF (Byproduct - Water) Sampled: 06/24/10 10:00 General Chemistry Parameters
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1 ANALYTICAL REPORT Result Flag Units Dilution Analysis MRL Factor Date/Time Method Batch Sample ID: NTF (Byproduct - Water) Sampled: 06/24/10 10:00 General Chemistry Parameters Acidity 1530 H mg/l /14/10 08:05 SM2310 B 10G1670 Total Suspended Solids 63.0 mg/l /01/10 22:35 SM2540 D 10G0146 Arsenic ND mg/l /29/10 00:16 SW /6010B 10F4821 Barium ND mg/l /29/10 00:16 SW /6010B 10F4821 Cadmium 2.50 mg/l /29/10 00:16 SW /6010B 10F4821 Chromium 72.6 mg/l /29/10 00:16 SW /6010B 10F4821 Lead ND mg/l /29/10 00:16 SW /6010B 10F4821 Mercury ND mg/l /28/10 14:59 SW /7470A 10F4689 Selenium ND mg/l /29/10 00:16 SW /6010B 10F4821 Silver ND mg/l /29/10 00:16 SW /6010B 10F4821 Page 2 of 12
2 SAMPLE EXTRACTION DATA Parameter Batch Lab Number Wt/Vol Extracted Extracted Vol Date Analyst Extraction Method TCLP Extraction by EPA 1311 SW F4518 NTF /25/10 15:45 KLA EPA 1311 SW / F4518 NTF /25/10 15:45 KLA EPA 1311 SW /7470A 10F4689 NTF /28/10 12:20 LCB EPA 7470 Page 3 of 12
3 PROJECT QUALITY CONTROL DATA Blank Blank Value Q Units Q.C. Batch Lab Number Analyzed Date/Time General Chemistry Parameters 10G0146-BLK1 Total Suspended Solids <0.500 mg/l 10G G0146-BLK1 07/01/10 22:35 10G1670-BLK1 Acidity 2.60 mg/l 10G G1670-BLK1 07/14/10 08:05 10F4689-BLK1 Mercury < mg/l 10F F4689-BLK1 06/28/10 14:14 10F4821-BLK1 Arsenic Barium Cadmium Chromium Lead Selenium Silver < mg/l 10F F4821-BLK1 06/28/10 13:52 < mg/l 10F F4821-BLK1 06/28/10 13:52 < mg/l 10F F4821-BLK1 06/28/10 13:52 < mg/l 10F F4821-BLK1 06/28/10 13:52 < mg/l 10F F4821-BLK1 06/28/10 13:52 < mg/l 10F F4821-BLK1 06/28/10 13:52 < mg/l 10F F4821-BLK1 06/28/10 13:52 Page 4 of 12
4 PROJECT QUALITY CONTROL DATA Duplicate Orig. Val. Duplicate Q Units RPD Limit Batch Sample Duplicated % Rec. Analyzed Date/Time General Chemistry Parameters 10G0146-DUP1 Total Suspended Solids mg/l G0146 NTF /01/10 22:35 10G0146-DUP2 Total Suspended Solids mg/l G0146 NTF /01/10 22:35 10G1670-DUP1 Acidity mg/l G1670 NTF /14/10 08:05 Page 5 of 12
5 PROJECT QUALITY CONTROL DATA LCS Target Known Val. Analyzed Val Q Units % Rec. Range Batch Analyzed Date/Time General Chemistry Parameters 10G0146-BS1 Total Suspended Solids mg/l 93% G /01/10 22:35 10G1670-BS1 Acidity ug/ml 98% G /14/10 08:05 10F4689-BS1 Mercury mg/l 97% F /28/10 14:21 10F4821-BS1 Arsenic Barium Cadmium Chromium Lead Selenium Silver mg/l 95% F /28/10 13: mg/l 101% F /28/10 13: mg/l 96% F /28/10 13: mg/l 97% F /28/10 13: mg/l 99% F /28/10 13: mg/l 96% F /28/10 13: mg/l 94% F /28/10 13:59 Page 6 of 12
6 PROJECT QUALITY CONTROL DATA LCS Dup Orig. Val. Duplicate Q Units Spike Conc % Rec. Target Range RPD Limit Batch Sample Duplicated Analyzed Date/Time 10F4689-BSD1 Mercury mg/l % F /28/10 14:23 10F4821-BSD1 Arsenic Barium Cadmium Chromium Lead Selenium Silver 1.87 mg/l % F mg/l % F mg/l % F mg/l % F mg/l % F mg/l % F mg/l % F4821 Page 7 of 12
7 PROJECT QUALITY CONTROL DATA Matrix Spike Orig. Val. MS Val Q Units Spike Conc % Rec. Target Range Batch Sample Spiked Analyzed Date/Time 10F4689-MS1 Mercury ND mg/l % F4689 NTF /28/10 14:32 10F4821-MS1 Arsenic Barium Cadmium Chromium Lead Selenium Silver ND 1.99 mg/l % F4821 NTF /28/10 14: mg/l % F4821 NTF /28/10 14:11 ND 2.00 mg/l % F4821 NTF /28/10 14:11 ND 9.84 mg/l % F4821 NTF /28/10 14: mg/l % F4821 NTF /28/10 14:11 ND 2.00 mg/l % F4821 NTF /28/10 14:11 ND 1.89 mg/l % F4821 NTF /28/10 14:11 Page 8 of 12
8 PROJECT QUALITY CONTROL DATA Matrix Spike Dup Orig. Val. Duplicate Q Units Spike Conc % Rec. Target Range RPD Limit Batch Sample Duplicated Analyzed Date/Time 10F4689-MSD1 Mercury ND mg/l % F4689 NTF /28/10 14:35 10F4821-MSD1 Arsenic Barium Cadmium Chromium Lead Selenium Silver ND 1.97 mg/l % F4821 NTF /28/10 14: mg/l % F4821 NTF /28/10 14:14 ND 2.02 mg/l % F4821 NTF /28/10 14:14 ND 9.89 mg/l % F4821 NTF /28/10 14: mg/l % F4821 NTF /28/10 14:14 ND 2.01 mg/l % F4821 NTF /28/10 14:14 ND 1.90 mg/l % F4821 NTF /28/10 14:14 Page 9 of 12
9 TestAmerica Nashville Method Matrix CERTIFICATION SUMMARY AIHA Nelac Tennessee SM2310 B Water X SM2540 D Water X SW /6010B Water N/A X N/A SW /6010 Water SW /7470A Water N/A X N/A SW Water N/A X N/A Page 10 of 12
10 TCLP REGULATORY LIMITS Regulatory Limit Arsenic 5 Barium 100 Cadmium 1 Chromium 5 Lead 5 Mercury 0.2 Selenium 1 Silver 5 Page 11 of 12
11 H ND Sample analysis performed past method-specified holding time. DATA QUALIFIERS AND DEFINITIONS Not detected at the reporting limit (or method detection limit if shown) METHOD MODIFICATION NOTES Page 12 of 12
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