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1 NEW Wilmad Sets the Standard for NMR Consumables a bridge between your experiments and our products Table of Contents: Page General Select-A-Tube Guide 1 Economy and Precision Tube Comparison Sheet 2 for NMR Caps for MAS Caps for Small Volume NMR for Gas-Tight Tubes Quality Manufactured in the USA ISO 9001:2008 Certified An SP Industries Company ORDER TODAY Call: or Fax: or On Line: cs@wilmad-labglass.com Wilmad-LabGlass 1172 N.W. Blvd. Vineland NJ USA
2 Page 1
3 Wilmad-LabGlass Economy and Precision Tube Comparison Sheet Economy Precision (Glass) Precision (Quartz) Precision (Suprasil) Material Impact on shimming quality by paramagnetic ASTM Type 1 Class B Borosilicate Glass (commercial name N51A) Medium (>1200 ppm impurities 1 Fe 2 O 3 ) ASTM Type 1 Class A Borosilicate Glass (commercial name Pyrex) Small (400 ppm Fe 2 O 3 ) Clear Fused Quartz Synthetic Quartz None (0.5 ppm Fe 2 O 3 ) None (<0.005 ppm Fe 2 O 3 ) Rapid cooling/heating No Yes, within 120 C Yes, within 300 C Yes, within 300 C Max. working temperature Ambient 230 C 1300 C 1300 C Sample volume 2 10% 0.5% 0.5% 0.5% reproducibility Cut-off wavelength 320 nm 320 nm 265 nm 190 nm Note 1: Impact on shimming quality varies upon magnetic field strength. Economy tube is recommended for 1D low field experiments. Note 2: Sample volume reproducibility refers to the maximum volume fluctuation when filling different NMR tubes to the same sample height. This number correlates to the reproducibility of time domain signal amplitude between different runs. Page 2
4 Gas-tight seal for air sensitive sample? Wilmad-LabGlass for NMR Caps Syringe access to the sample? Resonance frequency 600 MHz? Serum Cap Polyethylene Superior Pressure Cap Using Chloroform? PTFE NMR Tube Cap Disposable NMR Tube Caps Bruker 2.5 mm Rotor? Wilmad-LabGlass for MAS Caps Vespel Cap 13 C NMR? Macor Cap Variable temperature experiment? Torlon Cap 1 H NMR? Kel-F Cap Torlon Cap Page 3
5 Using small volume NMR probe, such as MicroProbe from Bruker? Wilmad-LabGlass for Small Volume NMR Using 4 inch long tube for automatic sample changer system? Looking for susceptibility matched product, such as Shigemi tubes? Requiring O.D. of the tube top to be 5 mm? 8 long Bruker MicroProbe /MicroCryoProbe Sample Tubes Doty Susceptibility Plugs Varying sample/external reference solution ratio? Varian and Bruker Automatic Sample Changer Tubes Bruker MATCH and SampleJet Capillary Sample Tubes Coaxial Insert Variable temperature experiment? Stem Coaxial Insert Microcell Insert Page 4
6 Wilmad-LabGlass for Gas-Tight Tubes Use Universal Solvent Jet NMR Tube Washer WG (J2) to wash Low Pressure/Vacuum Tube and Screw-Cap NMR Tube. Use Universal Solvent Jet NMR Tube Washer WG (J1) to wash Quick Pressure Valve Tube and Omni-Fit NMR Tube. Use Hamilton Syringe plus PTFE Needle to wash Pressure/Vacuum Tube. Pressure 1 atmosphere? Low quality vacuum seal (> 10-4 torr) for rough degasification? Connecting tube directly to metal (stainless steel or brass) gas/vacuum line with Swagelok Adaptor? Screw-Cap NMR Tube Introducing additional chemicals into the sealed sample without glove box? Pressure/Vacuum Tube 1 Quick Pressure Valve Tube 2 Omni-Fit NMR Tube Requiring high quality vacuum seal for < 10-6 torr? Constricted NMR Tube Requiring permanent seal? Low Pressure/Vacuum Note 1: Please check the maximum pressure for Quick Pressure Valve Tube and Pressure/Vacuum NMR Tube. Note 2: For any experiment with NH 3 gas or other corrosive gas, we recommend Quick Pressure Valve Tube with Kalrez O-ring Page 5
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